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HomeMy WebLinkAbout1510 John Fitch Blvd - UST - Fire Marsha CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA 8260C is Soil Dichlorodifluoromethane CTNY Chloromethane CTNY Vinyl Chloride CTNY Bromomethane CTNY Chloroethane CTNY Trichlorofluoromethane CTNY Acetone CTNY Acrylonitrile CTNY Di-isopropyl ether CT t-Butanol CT Trichlorotrifluoroethane CTNY 1,1-Dichloroethene CTNY t-Butyl ethyl ether CT t-Butanol CTNY tert-Amyl methyl ether(TAME) CT Methylene Chloride CTNY Carbon Disulfide CTNY Methyl-t-Butyl Ether(MTBE) CTNY trans-1,2-Dichloroethene CTNY Di-isopropyl ether CT ],I-Dichloroethane CTNY t-Butyl ethyl ether CT 2-Butanone(MEK) CTNY 2,2-Dichloropropane CTNY cis-1,2-Dichloroethene CTNY Chloroform CTNY Tetrahydrofuran CT 1,1,1-Trichloroethane CTNY text-Amyl methyl ether(TAME) CT Carbon Tetrachloride CTNY 1,1-Dichloropropene CTNY Benzene CTNY 1,2-Dichloroethane CTNY Trichloroethene CTNY 1,2-Dichloropropane CTNY Dibromomethane CTNY Bromodichloromethane CTNY Methyl Isobutyl Ketone CTNY cis-1,3-Dichloropropene - CTNY Toluene CTNY trans-1,3-Dichloropropene CTNY 2-Hexanone CTNY 1,1,2-Trichloroethane C-f NY Tetrachloroethene CTNY 1,3-Dichloropropane CTNY Dibromochloromethane CTNY 1,2-Dibromoethane CTNY trans-1,4-Dichloro-2-Butene CTNY Chlorobenzene CTNY Page 35 of 37 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA 8260C in Soil 1,1,1,2-Tetrachloroethane CTNY Ethylbenzene CTNY m+p Xylenes CTNY o-Xylene CTNY Styrene CTNY Bromofomi CTNY Isopropylbenzene CTNY 1,1,2,2-Tetrachloroethane CTNY Bromobenzene CTNY 1,2,3-Trichloropropane CTNY n-Propylbenzene CTNY 2-Chlorotoluene CTNY 4-Chlorotoluene CTNY 1,3,5-Trimethylbenzene CTNY tert-Butylbenzene CTNY 1,2,4-Trimethylbenzene CTNY sec-Butylbenzene CTNY 1,3-Dichlorobenzene CTNY 4-Isopropyltoluene CTNY 1,4-Dichlorobenzene CTNY 1,2-Dichlorobenzene CTNY n-Butylbenzene CTNY 1,2-Dibromo-3-Chloropropane CTNY 1,2,4-Trichlorobenzene CTNY Hexachlorobutadiene CTNY Naphthalene CTNY 1,2,3-Trichlorobenzene CT Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires CT Connecticut Public Health PH0116 09/30/2016 NY New York Certification(NELAC) 11982 04/01/2016 Page 36 of 37 1111 EVIS ' L 6020397 0 INC ti co cu NVIROSHIELD, INC. 0- MOFFITT STREET PRIORITY LEVEL: BOX 1296 TRATFORD, CT 06615 _ CHAIN OF CUSTODY \OJEC Nr1ME'• PROJECT LOCATION; PURCHASE ORDER 7l'R1:6:CODES: w, WELL 0=OUTFALL WO=WASTE OIL RO=RUN OFF B=BOTTOM SEDIMENT SW=SEWAGE SG=SLUDGE 5—SOIL R=RIVER/STREAM LF=LANDFILL W W=WASTE WATER L=LAKE/OCEAN X=OTHER;SPECIFY lii'1 Sr\MI'1-E SOURCE CONT. CONT. CONT.. CONT. ANALYSISREQ UESTED `� 1•D• CODE NO. TYPE SIZE PRES. DATE TIME COMMENTS/"RCP"Required? pit:, ay 1-4 1 `i J_r �5 JCS Pc•5 .� �Ss ��3 c'iC �q�— �n i ON"I"\INEI:CODES: P=PLASTIC E=EPA VIAL G=GLASS A=AMBER GLASS B=BACTERIA BO;E-T]T- 'ItC%SEiRVATIVE CODES: I=ICED 1-1=HYDROCHLORIC ACID(HCI) S=SODIUM HYROXIDE(NaOH) Na=S�NUM BISULFATE OTHER;SPECIFY (AiahISQ4T Iv1=NIETI METHANOL(MeOH) 0= 1P1..ER'S SIGNAL URL AFFILIATION DATE TRNSF ITEM TRANSFERS ' `- (• NO. NO. RELINQUISHED BY ACCERTED B DATE TIME: `,l)I:)I'I-IONAI..C:OMMEN`1'S: F Data on server/templates/forms/chain of custody (revised July 2014) 80 Lupes Drive Tel:(203)377-9984 Stratford,CT 06615 Fax:(203)377-9952 e-mail:cetI@eetlabs.com COMRflf[WHOWN1111 WING,INC. Client: Mr.Tim Farrelly Enviroshield,Inc. P.O.Box 1296 Stratford, CT 06615 Analytical Report CET# 6020395 Report Date:February 26,2016 Project:County Distributors, 1510 John Fitch Blvd, PO Number:26476 Connecticut Laboratory Certificate:PH 0116 New York Certification: 11982 Massachusetts laboratory Certificate:M-CT903 .. Rhode Island Certification: 199 Page 1 of 23 CET#:6020395 SAMPLE SUMMARY The sample(s)were received at 2.9°C. This report contains analytical data associated with following samples only. Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date Waste Oil North 6020395-01 Soil 2/18/2016 02/22/2016 Waste Oil South 6020395-02 Soil 2/18/2016 02/22/2016 Waste Oil East 6020395-03 Soil 2/18/2016 02/22/2016 Waste Oil West 6020395-04 Soil 2/18/2016 02/22/2016 Waste Oil Bottom 6020395-05 Soil 2/18/2016 02/22/2016 Analyte: Total Solids [EPA 160.3 modified] Analyst:TWF Matrix: Soil Date/Time Laboratory ID Client Sample ID Result RL Units Dilution Batch Prepared Analyzed Notes 6020395-01 Waste Oil North 97 1.0 % 1 B6B2306 02/23/2016 02/23/2016 15:33 6020395-02 Waste Oil South 94 1.0 % 1 136B2306 02/23/2016 02/23/2016 15:33 6020395-03 Waste Oil East 94 1.0 % 1 B6B2306 02/23/2016 02/23/2016 15:33 6020395-04 Waste Oil West 94 1.0 % 1 B6B2306 02/23/2016 02/23/2016 15:33 6020395-05 Wastc Oil Bottom 95 1.0 % 1 B6B2306 02/23/2016 02/23/2016 15:33 Client Sample ID Waste Oil North Lab ID: 6020395-01 Conn.Extractable TPH Analyst: MR Method: CT ETPH Matrix: Soil Result RL Date/Time Analytc (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH 5100 52 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 10:32 R Surrogate:Octacosane 83.7% 50-150 B6B2338 02/23/2016 021241201610:32 R C18-C36 unknown Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 2 of 23 CET#:6020395 Client Sample ID Waste Oil South Lab ID: 6020395-02 Conn.Extractable TPH Analyst: MH Method: CT-ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH 2300 53 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 10:55 R Surrogate:Octacosane 56.5% 50-150 B6132338 02/23/2016 021241201610:55 R C18-06 unknown Client Sample ID Waste Oil East Lab ID: 6020395-03 Conn.Extractable TPH Analyst: MH Method: CT-ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH 4700 53 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 11:19 R Surrogate:Octacosane 94.7% 50-150 136B2338 02/23/2016 021241201611:19 R C18-C36 unknown Client Sample ID Waste Oil West Lab ID: 6020395-04 Conn.Extractable TPH Analyst: MH Method: CT-ETPH Matrix: Soil Result RL Datc/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH 1100 53 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 11:43 R Surrogate:Octacosane 86.3% 50-150 B6132338 02/23/2016 021241201611:43 R C18-C36 unknown Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 3 of 23 CET#:6020395 Client Sample ID Waste Oil Bottom Lab ID: 6020395-05 SPLP Metals Analyst: KP Method: EPA 602OA-1312 Matrix: Extract Result RL Date/Time Analyte (mg/L) (mg/L) Dilution Prep Method Batch Prepared Analyzed Notes Lead ND 0.013 1 EPA 3005A B6B2510 02/25/2016 02/25/2016 13:13 Selenium ND 0.010 1 EPA 3005A B6B2510 02/25/2016 02/25/2016 13:13 Cadmium ND 0.0050 1 EPA 3005A B6B2510 02/25/2016 02/25/2016 13:13 Chromium ND 0.050 1 EPA 3005A B6B2510 02/25/2016 02/25/2016 13:13 Arsenic ND 0.0090 1 EPA 3005A 136B2510 02/25/2016 02/25/2016 13:13 Barium ND 0.050 1 EPA 3005A B6B2510 02/25/2016 02/25/2016 13:13 Silver ND 0.020 1 EPA 3005A B6B2510 02/25/2016 02/25/2016 13:13 Mercury ND 0.0020 1 EPA 3005A 136B2510 02/25/2016 02/25/2016 13:13 Conn.Extractable TPH Analyst:MH Method: CT ETPH Matrix:Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH 1500 53 1 EPA 3550C B6132338 02/23/2016 02/24/2016 12:07 R Surrogate:Octacosane 94.6% 50-150 136B2338 02/23/2016 021241201612:07 R Cl8-C36 unknown PCBs by ASE Analyst:SJ Method: EPA 8082A Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes PCB-1016 ND 0.21 1 EPA 3545A B6132403 02/24/2016 02/24/2016 13:12 PCB-1221 ND 0.21 1 EPA 3545A 136132403 02/24/2016 02/24/2016 13:12 PCB-1232 ND 0.21 1 EPA 3545A B6132403 02/24/2016 02/24/2016 13:12 PCB-1242 ND 0.21 1 EPA 3545A B6B2403 02/24/2016 02/24/2016 13:12 PCB-1248 ND 0.21 1 EPA 3545A B6132403 02/24/2016 02/24/2016 13:12 PCB-1254 ND 0.21 1 EPA 3545A B6B2403 02/24/2016 02/24/2016 13:12 PCB-1260 ND 0.21 1 EPA 3545A B6B2403 02/24/2016 02/24/2016 13:12 PCB-1268 ND 0.21 1 EPA 3545A 136B2403 02/24/2016 02/24/2016 13:12 Surrogate:TCW 98.6% 30-150 B6132403 02/24/2016 021241201613:12 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 4 of 23 CET#:6020395 Client Sample ID Waste Oil Bottom Lab ID: 6020395-05 PCBs by ASE Analyst:Si Method: EPA 8082A Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Surrogate:DCB 90.8% 30-150 136132403 02/24/2016 021241201613:12 Semivolatile Organics Analyst:ALB Method: EPA 8270D Matrix:Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Naphthalene ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 2-Methyl Naphthalene ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 Acenaphthylene ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 Acenaphthene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/24/2016 17:14 Fluorene ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 Phcnanthrenc ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 Anthracene ND 320 1 EPA 3545A 136B2308 02/23/2016 02/24/2016 17:14 Fluoranthene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/24/2016 17:14 Pyrenc ND 320 1 EPA 3545A 136B2308 02/23/2016 02/24/2016 17:14 Benzo[a]anthraccne ND 320 1 EPA 3545A B6B2308 02/23/2016 02/24/2016 17:14 Chrysene ND 320 1 EPA 3545A 136B2308 02/23/2016 02/24/2016 17:14 Benzo[b]fluoranthene ND 320 1 EPA 3545A 136B2308 02/23/2016 02/24/2016 17:14 Benzo[k]fluoranthene ND 320 1 EPA 3545A 136132308 02/23/2016 02/24/2016 17:14 Benzo[a]pyrene ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 Indeno[1,2,3-cd]pyrene ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 Dibenz[a,h]anthracene ND 320 1 EPA 3545A 136132308 02/23/2016 02/24/2016 17:14 Benzo[g,h,i]perylene ND 320 1 EPA 3545A B6132308 02/23/2016 02/24/2016 17:14 Surrogate:Nitrobenzene-d5 41.9% 30-130 136B2308 02/23/2016 021241201617:14 Surrogate:2-Fluorobiphenyl 51.3% 30-130 136132308 02/23/2016 021241201617:14 Surrogate:Terphenyl-d14 56.1% 30-130 136B2308 02/23/2016 021241201617:14 Complete Environmental Testing,Inc. 80 Lupcs Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 5 of 23 CET ff:6020395 Client Sample ID Waste Oil Bottom Lab ID: 6020395-05 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 16 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 14:41 *F2 Chloromethane ND 10 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 *F2*C2 Vinyl Chloride ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 *F2*C2 Bromomethane ND 10 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 *F2*C2 Chloroethanc ND 10 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Trichlorofluoromethane ND 41 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Acetone ND 160 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Acrylonitrile ND 8.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Trichlorotrifluoroethane ND 41 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 1,1-Dichloroethene ND 5.2 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Methylene Chloride ND 52 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Carbon Disulfide ND 10 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Methyl-t-Butyl Ether(MTBE) ND 5.2 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 14:41 trans-1,2-Dichloroethene ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 1,1-Dichloroethane ND 5.2 1.97 EPA5035A-L B6132514 02/25/2016 02/25/2016 14:41 2-Butanone(MEK) ND 26 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 2,2-Dichloropropane ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 cis-1,2-Dichloroethene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Chloroform ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Tetrahydrofuran ND 26 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 1,1,1-Trichloroethane ND 5.2 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 14:41 Carbon Tetrachloride ND 5.2 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 14:41 1,1-Dichloropropene ND 5.2 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 14:41 Benzene ND 5.2 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 14:41 1,2-Dichloroethane ND 5.2 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 14:41 Trichloroethene ND 5.2 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 14:41 1,2-Dichloropropane ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Dibromomethane ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Bromodichloromethane ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Methyl Isobutyl Ketone ND 26 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 cis-1,3-Dichloropropene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Toluene ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 trans-1,3-Dichloropropene ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 2-Hexanonc ND 26 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 1,1,2-Trichloroethane ND 5.2 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Tetrachloroethenc ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 1,3-Dichloropropane ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Dibromochloromethane ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 1,2-Dibromoethane ND 5.2 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 14:41 trans-1,4-Dichloro-2-Butenc ND 26 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Chlorobenzene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 6 of 23 CET#:6020395 Client Sample ID Waste Oil Bottom Lab ID: 6020395-05 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix:Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes 1,1,1,2-Tetrachloroethane ND 5.2 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Ethylbenzene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 m+p Xylenes ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 o-Xylcne ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 Styrene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 *C2 Bromoform ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Isopropylbenzene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 1,1,2,2-Tetrachloroethane ND 5.2 1.97 EPA5035A-L B6132514 02/25/2016 02/25/2016 14:41 Bromobenzene ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 1,2,3-Trichloropropane ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 n-Propylbenzene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 2-Chlorotoluene ND 5.2 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 14:41 *C2 4-Chlorotoluene ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 *C2 1,3,5-Trimethylbenzene ND 5.2 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 14:41 *C2 tert-Butylbenzenc ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 1,2,4-Trimethylbenzene ND 5.2 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 14:41 sec-Butylbenzenc ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 1,3-Dichlorobenzene ND 5.2 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 14:41 *C2 4-Isopropyltoluene ND 5.2 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 14:41 1,4-Dichlorobenzene ND 5.2 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 14:41 1,2-Dichlorobenzene ND 5.2 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 14:41 *F2*C2 n-Butylbenzenc ND 5.2 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 14:41 *C2 1,2-Dibromo-3-Chloropropane ND 5.2 1.97 EPA5035A-L 136B2514 02/25/2016 02/25/2016 14:41 1,2,4-Trichlorobenzcne ND 5.2 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Hexachlorobutadiene ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 Naphthalene ND 5.2 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 14:41 1,2,3-Trichlorobenzene ND 5.2 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 14:41 Surrogate:1,2-Dichloroethane-d4 100% 70-130 136B2514 02/25/2016 021251201614:41 Surrogate:Toluene-d8 100% 70-130 B6B2514 02/25/2016 0212512016 14:41 Surrogate:4-Bromofluo obenzene 82.8% 70-130 B6B2514 02/25/2016 021251201614:41 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 7 of 23 CET#:6020395 QUALITY CONTROL SECTION Batch B6B2306-EPA 160.3 modifled Result RL Spike Source %Ree RPD Analyte (%) (%) Level Result %Rcc Limits RPD Limit Notes Duplicate(B6132306-DUPI) Source:6020395-05 Prepared:2/23/2016 Analyzed:2/23/2016 Total Solids 95 1.0 95 0.0290 200 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 8 of 23 CET#:6020395 Batch B6132308-EPA 8270D Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes BIank(B6B2308-BLK1) Prepared:2/23/2016 Analyzed:2/24/2016 Naphthalene ND 300 2-Methyl Naphthalene ND 300 Acenaphthylenc ND 300 Acenaphthene ND 300 Fluorene ND 300 Phenanthrenc ND 300 Anthracenc ND 300 Fluoranthenc ND 300 Pyrene ND 300 Benzo[a]anthracene ND 300 Chrysene ND 300 Benzo[b]fluoranthene ND 300 Benzo[k]fluoranthene ND 300 Benzo[a]pyrene ND 300 Indeno[1,2,3-cd]pyrene ND 300 Dibenz[a,h]anthracene ND 300 Benzo[g,h,i]perylene ND 300 Surrogate:Nitrobenzene-d5 53.4 30-130 Surrogate:2-Fluorobiphenyl 53.7 30-130 Surrogate:Terphenyl-d]4 55.3 30-130 LCS(B6B2308-BS1) Prepared:2/23/2016 Analyzed:2/24/2016 Naphthalene 2030 300 4,000.000 50.6 40-140 2-Methyl Naphthalene 2080 300 4,000.000 52.0 40-140 Acenaphthylene 2100 300 4,000.000 52.5 40-140 Acenaphthenc 2150 300 4,000.000 53.8 40-140 Fluorene 2250 300 4,000.000 56.3 40-140 Phenanthrene 2300 300 4,000.000 57.4 40-140 Anthracenc 2350 300 4,000.000 58.7 40-140 Fluoranthene 2360 300 4,000.000 58.9 40-140 Pyrene 2370 300 4,000.000 59.2 40-140 Benzo[a]anthracene 2410 300 4,000.000 60.2 40-140 Chrysene 2420 300 4,000.000 60.5 40-140 Benzo[b]fluoranthene 3210 300 4,000.000 80.2 40-140 Benzo[k]fluoranthene 3510 300 4,000.000 87.8 40-140 Benzo[a]pyrcnc 3550 300 4,000.000 88.7 40-140 Indeno[1,2,3-cd]pyrene 3680 300 4,000.000 92.0 40-140 Dibenz[a,h]anthracene 3610 300 4,000.000 90.3 40-140 Benzo[g,h,i]perylene 3680 300 4,000.000 92.1 40-140 Surrogate:Nitrobenzene-d5 51.4 30-130 Surrogate:2-Fluorobiphenyl 52.9 30-130 Surrogate:Terphenyl-d14 52.6 30-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 9 of 23 CET#:6020395 Batch B6B2338-CT-ETPH Result RL Spike Source %Rec RPD Analyte (mg/kg) (mg/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2338-BLKI) Prepared:2/23/2016 Analyzed:2/24/2016 ETPH ND 50 Surrogate:Octacosane 106 50-150 LCS(B6B2338-BSI) Prepared:2/23/2016 Analyzed:2/24/2016 ETPH 1270 50 1,500.000 84.6 60-120 Surrogate:Octacosane 94.6 50-150 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615-Tel:203-377-9984-Fax:203-377-9952-www.cetlabs.com Page 10 of 23 CET#:6020395 Batch B6B2403-EPA 8082A Result RL Spike Source %Rec RPD Analyte (mg/kg) (mg/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2403-BLKI) Prepared:2/24/20I6 Analyzed:2/24/2016 PCB-1016 ND 0.20 PCB-1221 ND 0.20 PCB-1232 ND 0.20 PCB-1242 ND 0.20 PCB-1248 ND 0.20 PCB-1254 ND 0.20 PCB-1260 ND 0.20 PCB-1268 ND 0.20 Surrogate:TCMX 102 30-150 Surrogate:DCB 93.3 30-150 LCS(B6B2403-BSI) Prepared:2/24/2016 Analyzed:2/24/2016 PCB-1016 0.985 0.20 1.000 98.5 50-150 PCB-1260 0.976 0.20 1.000 97.6 50-150 Surrogate:TCMX 95.9 30-150 Surrogate:DCB 87.6 30-150 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cettabs.com Page 1 CET#:6020395 Batch B6B2510-EPA 6020A Result RL Spike Source %Roc RPD Analyte (mg/L) (mg/L) Level Result %Rec Limits RPD Limit Notes Blank(B6B2510-BLKI) Prepared:2/25/2016 Analyzed:2/25/2016 Lead ND 0.013 Selenium ND 0.010 Cadmium ND 0.0050 Chromium ND 0.050 Arsenic ND 0.0090 Barium ND 0.050 Silver ND 0.020 Mercury ND 0.0020 LCS(B6B2510-BS1) Prepared:2/25/2016 Analyzed:2/25/2016 Lead 0.186 0.013 0.200 92.9 80-120 Selenium 0.386 0.010 0.400 96.6 80-120 Cadmium 0.188 0.0050 0.200 93.9 80-120 Chromium 0.184 0.050 0.200 92.2 80-120 Arsenic 0.192 0.0090 0.200 96.2 80-120 Barium 0.182 0.050 0.200 90.8 80-120 Silver 0.0970 0.020 0.100 97.0 80-120 Mercury 0.00459 0.0020 0.005 91.8 80-120 Duplicate(B6B2510-DUPI) Source:6020395-05 Prepared:2/25/2016 Analyzed:2/25/2016 Lead ND 0.013 ND 20 Selenium ND 0.010 ND 20 Cadmium ND 0.0050 ND 20 Chromium ND 0.050 ND 20 Arsenic ND 0.0090 ND 20 Barium ND 0.050 ND 20 Silver ND 0.020 ND 20 Mercury ND 0.0020 ND 35 Matrix Spike(B6B2510-MSI) Source:6020395-05 Prepared:2/25/2016 Analyzed:2/25/2016 Lead 0.187 0.013 0.200 ND 93.3 75-125 Selenium 0.397 0.010 0.400 ND 99.3 75-125 Cadmium 0.188 0.0050 0.200 ND 94.2 75-125 Chromium 0.188 0.050 0.200 ND 93.8 75-125 Arsenic 0.196 0.0090 0.200 ND 98.2 75-125 Barium 0.186 0.050 0.200 ND 93.0 75-125 Silver 0.0966 0.020 0.100 ND 96.6 75-125 Mercury 0.00642 0.0020 0.005 ND 128 75-200 Matrix Spike Dup(B6B2510-MSDI) Source:6020395-05 Prepared:2/25/2016 Analyzed:2/25/2016 Lead 0.186 0.013 0.200 ND 92.9 75-125 0.424 20 Selenium 0.391 0.010 0.400 ND 97.8 75-125 1.56 20 Cadmium 0.186 0.0050 0.200 ND 93.0 75-125 1.30 20 Chromium 0.185 0.050 0.200 ND 92.7 75-125 1.17 20 Arsenic 0.193 0.0090 0.200 ND 96.4 75-125 1.90 20 Barium 0.183 0.050 0.200 ND 91.7 75-125 1.45 20 Silver 0.0975 0.020 0.100 ND 97.5 75-125 0.861 20 Mercury 0.00650 0.0020 0.005 ND 130 75-200 1.19 20 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 12 of 23 CET#:6020395 Batch B6B2514-EPA 8260C Result RL Spike Source %Rec RPD Analytc (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes BIank(116112514-BLKl) Prepared:2/25/2016 Analyzed:2/25/2016 Dichlorodifluoromethane ND 7.5 Chloromethane ND 5.0 Vinyl Chloride ND 2.5 Bromomethane ND 5.0 Chloroethane ND 5.0 Trichlorofluoromethane ND 20 Acetone ND 75 Acrylonitrile ND 4.0 Trichlorotrifluoroethane ND 20 I,1-Dichloroethene ND 2.5 Methylene Chloride ND 25 Carbon Disulfide ND 5.0 Methyl-t-Butyl Ether(MTBE) ND 2.5 trans-1,2-Dichloroethene ND 2.5 IJ-Dichloroethane ND 2.5 2-Butanone(MEK) ND 13 2,2-Dichloropropane ND 2.5 cis-1,2-Dichloroethene ND 2.5 Chloroform ND 2.5 Tetralydrofuran ND 13 1,1,1-Trichlorocthane ND 2.5 Carbon Tetrachloride ND 2.5 1,1-Dichloropropene ND 2.5 Benzene ND 2.5 1,2-Dichloroethane ND 2.5 Trichloroethenc ND 2.5 1,2-Dichloropropane ND 2.5 Dibromomcthane ND 2.5 Bromodichloromethane ND 2.5 Methyl Isobutyl Ketone ND 13 cis-1,3-Dichloropropene ND 2.5 Toluene ND 2.5 trans-1,3-Dichloropropene ND 2.5 2-Hexanonc ND 13 1,1,2-Trichlorocthane ND 2.5 Tetrachloroethene ND 2.5 1,3-Dichloropropane ND 2.5 Dibromochloromethane ND 2.5 1,2-Dibromoethane ND 2.5 trans-1,4-Dichloro-2-Butene ND 13 Chlorobenzene ND 2.5 1,1,1,2-Tetrachloroethane ND 2.5 Ethylbenzene ND 2.5 m+p Xylenes ND 2.5 o-Xylenc ND 2.5 Styrene ND 2.5 Bromofonn ND 2.5 Isopropylbenzenc ND 2.5 1,1,2,2-Tetrachlorocthane ND 2.5 Bromobenzene ND 2.5 1,2,3-Tiichloropropanc ND 2.5 n-Propylbenzcne ND 2.5 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 13 of 23 CET#:6020395 Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2514-BLK1)-Continued Prepared:2/25/2016 Analyzed:2/25/2016 2-Chlorotoluene ND 2.5 4-Chlorotoluene ND 2.5 1,3,5-Trimethylbenzene ND 2.5 test-Butylbenzene ND 2.5 1,2,4-Trimethylbenzene ND 2.5 sec-Butylbenzene ND 2.5 1,3-Dichlorobenzene ND 2.5 4-Isopropyltoluene ND 2.5 1,4-Dichlorobenzene ND 2.5 1,2-Dichlorobenzene ND 2.5 n-Butylbenzene ND 2.5 1,2-Dibromo-3-Chloropropane ND 2.5 1,2,4-Trichlorobenzene ND 2.5 Hexachlorobutadiene ND 2.5 Naphthalene ND 2.5 1,2,3-Trichlorobenzene ND 2.5 Surrogate:1,2-Dichloroethane-d4 96.3 70-130 Surrogate:Toluene-d8 91.1 70-130 Surrogate:4-Bromofluorobenzene 84.3 70-130 LCS(B6B2514-BS1) Prepared:2/25/2016 Analyzed:2/25/2016 Dichlorodifluoromethane 70.0 7.5 50.000 140 70-130 g Chloromethane 85.3 5.0 50.000 171 70-130 g Vinyl Chloride 85.8 2.5 50.000 172 70-130 g Bromomethane 91.9 5.0 50.000 184 70-130 g Chloroethanc 60.0 5.0 50,000 120 70-130 Trichlorofluoromethanc 54.8 20 50.000 110 70-130 Acetone 97.4 75 100.000 97.4 70-130 Acrylonitrile 49.0 4.0 50.000 98.0 70-130 Trichlorotrifluoroethane 41.0 20 50.000 81.9 70-130 I,1-Dichloroethene 37.2 2.5 50.000 74.3 70-130 Methylene Chloride 42.3 25 50.000 84.6 70-130 Carbon Disulfide 37.6 5.0 50.000 75.2 70-130 Methyl-t-Butyl Ether(MTBE) 44.0 2.5 50.000 88.1 70-130 trans-1,2-Dichloroethene 42.5 2.5 50.000 84.9 70-130 1,1-Dichloroethane 51.7 2.5 50.000 103 70-130 2-Butanone(MEK) 102 13 100.000 102 70-130 2,2-Dichloropropane 54.4 2.5 50.000 109 70-130 cis-1,2-Dichloroctliene 55.2 2.5 50.000 110 70-130 Chloroform 50.4 2.5 50.000 101 70-130 Tetrahydrofuran 47.6 13 50.000 95.2 70-130 1,1,1-Trichloroethanc 53.9 2.5 50.000 108 70-130 Carbon Tetrachloride 47.0 2.5 50.000 93.9 70-130 I,1-Dichloropropcne 48.1 2.5 50.000 96.2 70-130 Benzene 51.3 2.5 50.000 103 70-130 1,2-Dichloroethane 53.5 2.5 50.000 107 70-130 Trichloroethene 46.1 2.5 50.000 92.2 70-130 1,2-Dichloropropane 52.9 2.5 50.000 106 70-130 Dibromomethane 50.3 2.5 50.000 101 70-130 Bromodichloromethane 52.5 2.5 50.000 105 70-130 Methyl Isobutyl Ketone 111 13 100.000 111 70-130 cis-1,3-Dichloropropene 51.3 2.5 50.000 103 70-130 Toluene 48.1 2.5 50.000 96.2 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 14 of 23 CET#:6020395 Result RL Spike Source %Rcc RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes LCS(B6B2514-BSI)-Continued Prepared:2/25/2016 Analyzed:2/25/2016 trans-1,3-Dichloropropene 55.4 2.5 50.000 111 70-130 2-Hexanone 120 13 100.000 120 70-130 1,1,2-Trichloroethane 53.0 2.5 50.000 106 70-130 Tetrachloroethene 48.1 2.5 50.000 96.2 70-130 1,3-Dichloropropane 52.1 2.5 50.000 104 70-130 Dibromochloromethane 56.9 2.5 50.000 114 70-130 1,2-Dibromoctliane 57.3 2.5 50.000 115 70-130 mans-1,4-Dicliloro-2-Butene 57.1 13 50.000 114 70-130 Chlorobenzene 56.6 2.5 50.000 113 70-130 1,1,1,2-Tetrachloroethane 56.9 2.5 50.000 114 70-130 Ethylbenzene 55.0 2.5 50.000 110 70-130 m+p Xylenes 118 2.5 100.000 118 70-130 o-Xylcnc 53.0 2.5 50.000 106 70-130 Styrene 57.0 2.5 50.000 114 70-130 Bromoform 51.9 2.5 50.000 104 70-130 Isopropylbenzene 56.7 2.5 50.000 113 70-130 1,1,2,2-Tetrachloroethane 57.8 2.5 50.000 116 70-130 Bromobenzene 62.0 2.5 50.000 124 70-130 1,2,3-Trichloropropane 59.0 2.5 50.000 118 70-130 n-Propylbenzene 63.0 2.5 50.000 126 70-130 2-Chlorotoluene 54.3 2.5 50.000 109 70-130 4-Chlorotoluene 56.0 2.5 50.000 112 70-130 1,3,5-Trimethylbenzene 54.5 2.5 50.000 109 70-130 tert-Butylbenzene 50.9 2.5 50.000 102 70-130 1,2,4-Trimethylbenzene 55.9 2.5 50.000 112 70-130 sec-Butylbenzene 56.2 2.5 50.000 112 70-130 1,3-Dichlorobenzene 59.8 2.5 50.000 120 70-130 4-Isopropyltoluene 58.6 2.5 50.000 117 70-130 1,4-Dichlorobenzene 60.6 2.5 50.000 121 70-130 1,2-Dichlorobenzene 66.3 2.5 50.000 133 70-130 g n-Butylbenzene 63.7 2.5 50.000 127 70-130 1,2-Dibromo-3-Chloropropane 54.4 2.5 50.000 109 70-130 1,2,4-Trichlorobenzene 60.4 2.5 50.000 121 70-130 Hexachlorobutadicne 49.8 2.5 50.000 99.6 70-130 Naphthalene 55.6 2.5 50.000 111 70-130 1,2,3-Trichlorobenzene 60.8 2.5 50.000 122 70-130 Surrogate:1,2-Dichloroethane-d4 102 70-130 Sm•rogate:Toluene-d8 9Z8 70-130 Surrogate:4-Brotnq luorobenzene 7. 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 15 of 23 CET#:6020395 Questions related to this report should be directed to David Ditta,Timothy Fusco,or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Report Comments: Sample Result Flags: E-The result is estimated,above the calibration range. H-The surrogate recovery is above the control limits. L-The surrogate recovery is below the control limits. B-The compound was detected in the laboratory blank. P-The Relative Percent Difference(RPD)of dual column analyses exceeds 40%. D-The RPD between the sample and the sample duplicate is high. Sample Homogenity may be a problem. +- The Surrogate was diluted out. *Cl-The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2-The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *FI-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I-The Analyte exceeds%RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result,or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 16 of 23 CET#:6020395 [VE 80 Lupes Drive Tel:(203)377-9984 Stratford,CT 06615 C PHIF IN IRONMENTA[TESTING,INC. Fax:(203)377-9952 email:cetl@cetlabs.com Quality Control Definitions and Abbreviations Internal Standard(IS) An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time,calculate relative response,and quantify analytes of interest. Surrogate Recovery The%recovery for non-tarer organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method,sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels(MDL)and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte foun in duplicate spikes including amount that was spike. Matrix Spike%Recovery %Recovery of spiked amount in sample. Matrix Spike Dup%Recovery %Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS%Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H- Recovery is above the control limits L- Recovery is below the control limits B- Compound detected in the Blank P- RPD of dual column results exceeds 40% #- Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 $ New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 17 of 23 REASONABLE CONFIDENCE PROTOCOL W LABORATORY ANALYSIS QA/QC CERTIFICATION FORM Laboratory Name: Complete Environmental Testing,Inc. Client: Enviroshield,Inc. Project Location: Tank Pull Project Number: Laboratory Sample ID(s): Sample Date(s): 6020395-01thru 6020395-05 02/18/2016 List RCP Methods Used.. CET#: 6020395 CT-ETPH,EPA 1312,EPA 6020A,EPA 8082A,EPA 8260C,EPA 8270D 1 For each analytical method referenced in this laboratory report package,were all specified QA/QC ❑Yes ❑ No performance criteria followed,including the requirement to explain any criteria falling outside of acceptable guidelines,as specified in the CTDEP method-specific Reasonable Confidence Protocol documents? IA Were the method specified preservation and holding time requirements met? ❑✓Yes ❑ No 113 VPH and EPH Methods only: Was the VPH and EPH method conducted without significant ❑Yes ❑ No modifications(see Section 11.3 of respective RCP methods)? ❑✓ N/A 2 Were all samples received by the laboratory in a condition consistent with that described on the Yes ❑ No associated chain-of-custody document(s)? 3 Were samples received at an appropriate temperature(<6 degrees C.)? ❑✓ Yes ❑ No ❑ N/A 4 Were all QA/QC performance criteria specified in the CT DEP Reasonable Confidence Protocol ❑Yes ❑✓ No documents achieved? 53 a)Were reporting limits specified or referenced on the chain-of-custody? ❑Yes ❑✓ No 5b b)Were these reporting limits met? ❑Yes ❑ No 6 For each analytical method referenced in this laboratory report package,were results reported for ❑Yes ❑✓ No all consiments identified in the method-specific analyte lists presented in the Reasonable Confidence Protocol documents? 7 Are project specific matrix spikes and laboratory duplicates included with this data set? ❑Yes ❑ No Notes:For all questions to which the response was"No"(with the exception of question#7),additional information must be provided in an attached narrative.If the answer to question#1,#1 A,or#1 B is"No",the data package does not meet the requirements for"Reasonable Confidence." This form may not be altered and all questions must be answered. I,the undersigned,attest under the pains and penalties of perjury that,to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report,such information is accurate and complete. Authorized Signature: Position:Laboratory Director Printed Name:David Ditta Date: 02/26/2016 Name of Laboratory:Complete Environmental Testing,Inc This certification form is to be used for RCP methods only. CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 18 of 23 RCP Case Narrative 4-See Exceptions Report Below 6-The client requested a subset of the CT8270 List and RCP Metals List. 4-Exceptions Report Recovery Batch/Sequence Analyte QC Type Exception Result RPD (%) Sample ID 1,2-Dichlorobenzene LCS High 133 B6B2514 Bromomethane LCS High 184 B6B2514 Chloromethane LCS High 171 B6B2514 Dichlorodifluoromethane LCS High 140 B6B2514 Vinyl Chloride LCS High 172 B6B2514 1,2-Dichlorobenzene CC High 72.7 145 S6B2602 1,3,5-Trimethylbenzene CC High 68.0 136 S6B2602 1,3-Dichlorobenzene CC High 68.6 137 S6B2602 2-Chlorotolucne CC High 69.3 139 S6B2602 4-Chlorotoluene CC High 70.0 140 S6B2602 Bromomethane CC High 71.5 143 S6B2602 Chloromethane CC High 68.1 136 S6B2602 n-Butylbenzene CC High 67.1 134 S6B2602 Styrene CC High 66.3 133 S6B2602 Vinyl Chloride CC High 65.0 130 S6B2602 QC Batch/Sequence Report Batch Sequence CET ID Sample ID Specific Method Matrix Collection Date B6B2338 6020395-01 Waste Oil North CT-ETPH Soil 02/18/2016 B6B2338 6020395-02 Waste Oil South CT-ETPH Soil 02/18/2016 B6B2338 6020395-03 Waste Oil East CT-ETPH Soil 02/18/2016 B6B2338 6020395-04 Waste Oil West CT-ETPH Soil 02/18/2016 B6B2338 6020395-05 Waste Oil Bottom CT-ETPH Soil 02/18/2016 B6B2410 6020395-05 Waste Oil Bottom EPA 1312 Soil 02/18/2016 B6B2510 S6B2510 6020395-05 Waste Oil Bottom EPA 6020A Soil 02/18/2016 B6B2403 S6B2502 6020395-05 Waste Oil Bottom EPA 8082A Soil 02/18/2016 B6B2514 S6B2602 6020395-05 Waste Oil Bottom EPA 8260C Soil 02/18/2016 B6B2308 S6B2509 6020395-05 Waste Oil Bottom EPA 8270D Soil 02/18/2016 CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 19 of 23 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications CT-ETPH in Soil ETPH CT EPA 6020A in Soil Lead CTNY Selenium CTNY Cadmium CTNY Chromium CTNY Arsenic CTNY Barium CTNY Silver CTNY Mercury CT EPA 8082A in Soil PCB-1016 CTNY PCB-1221 CTNY PCB-1232 CTNY PCB-1242 CTNY PCB-1248 CTNY PCB-1254 CTNY PCB-1260 CTNY PCB-1268 CT EPA 8260C in Soil Dichlorodifluoromethane CTNY Chloromethane CTNY Vinyl Chloride CTNY Bromomethane CTNY Chloroethane CTNY Trichlorofluoromethane CTNY Acetone CTNY Acrylonitrile CTNY Trichlorotrifluoroethane CTNY 1,1-Dichloroethene CTNY Methylene Chloride CTNY Carbon Disulfide CTNY Methyl-t-Butyl Ether(MTBE) CTNY trans-1,2-Dichloroethene CTNY 1,I-Dichloroethane CTNY 2-Butanone(MEK) CTNY 2,2-Dichloropropane CTNY cis-1,2-Dichloroethene CTNY Chloroform CTNY Tetrahydrofuran CT 1,1,1-Trichloroethane CTNY Carbon Tetrachloride CTNY 1,I-Dichloropropene CTNY Benzene CTNY 1,2-Dichloroethane CTNY Trichloroethene CTNY 1,2-Dichloropropane CTNY Dibromomethane CTNY Page 20 of 23 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications CPA 8260C in Soil Bromodichloromethane CTNY Methyl Isobutyl Ketone CTNY cis-1,3-Dichloropropene CTNY Toluene CTNY trans-1,3-Dichloropropene CTNY 2-Hexanone CTNY 1,1,2-Trichloroethane CTNY Terachloroethene CTNY 1,3-Dichloropropane CTNY Dibromochloromethane CTNY 1,2-Dibromoethane CTNY trans-1,4-Dichloro-2-Butene CTNY Chlorobenzene CTNY 1,1,1,2-Tetrachloroethane CTNY Ethylbenzene CTNY m+p Xylenes CTNY o-Xylene CTNY Styrene CTNY Bromofonn CTNY Isopropylbenzene CTNY 1,1,2,2-Tetrachloroethane CTNY Bromobenzene CTNY 1,2,3-Trichloropropane CTNY n-Propylbenzene CTNY 2-Chlorotoluene CTNY 4-Chlorotoluene CTNY 1,3,5-Trimethylbenzene CTNY tert-Butylbenzene CTNY 1,2,4-Trimethylbenzene CTNY sec-Butylbenzene CTNY 1,3-Dichlorobenzene CTNY 4-Isopropyltoluene CTNY 1,4-Dichlorobenzene CTNY 1,2-Dichlorobenzene CTNY n-Butylbenzene CTNY 1,2-Dibromo-3-Chloropropane CTNY 1,2,4-Trichlorobenzene CTNY Hexachlorobutadiene CTNY Naphthalene CTNY 1,2,3-Trichlorobenzene CT CPA 8270D in Soil Naphthalene CTNY 2-Methyl Naphthalene CTNY Acenaphthylene CTNY Acenaphthene CTNY Fluorene CTNY Phenanthrene CTNY Anthracene CTNY Fluoranthene CTNY Page 21 of 23 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA 8270D in Soil Pyrene CTNY Benzo[a]anthracene CTNY Chrysene CTNY Benzo[b]fluoranthene CTNY Benzo[k]tuoranthene CTNY Benzo[a]pyrene CTNY Indeno[1,2,3-cd]pyrene CTNY Dibenz[a,h]anthracene CTNY Benzo[g,h,i]perylene CTNY Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires CT Connecticut Public Health PH0116 09/30/2016 NY New York Certification(NELAC) 11982 04/01/2016 Page 22 of 23 �III6III�N2III�3NI11�I81N� N ENVIRO ,._.,SHIELD INC N �..._.._ ENVIROSHIELD, INC. PRIORITY LEVEL: 250 MOFFITT STREET P.O. BOX 1296 STRATFORD, CT 06615 CHAIN OF CUSTODY PROJECT NAME: PROJECT LOCATION: TPURCIHIASE ORDER So•a'4" i,. ��A,>vr C,T 7 Io SOURCE CODES:" W=WELL O=OUTFALL WO=WASTE OIL RO=RUN OFF B=BOTTOM SEDIMENT SW=SEWAGE SG=SLUDGE S=SOIL R=RIVER/STREAM LF=LANDFILL W W=WASTE WATER L=LAKE/OCEAN X=OTHER;SPECIFY ITEM SAMPLE SOURCE CONT. CONT. CONT. FONT. ANALYSIS REQUESTED DATE TIME COMMENTS/"RCP"Required'? NO. I.D. CODE NO. TYPE SIZE PRES. RQlp 5 1Ask v j jug•• 3 `" k ���� h r Y -'TPR 9,46 d 7t� NAs e�5 b �oST RCRA irm-4A� 5PLP I _i CONTAINER CODS: P=PLASTIC E=EPA VIAL G GLASS A=AM BER GLASS B=BACTERIA BOTTLE — PRESERVATIVE CODES: I=ICED H=HYDROCHLORIC ACID(HCI) S=SODIUM HYROXIDE(NaOH) Na=SODIUM BISULFATE(NaHSO4) M=METHANOL(MeOH) O=OTHER;SPECIFY SAMPLER'S SIGNATURE AFFILIATION DATE TRNSF ITEM TRANSFERS: NO. NO. RELINQUISHED BY ACCEPTED BY DATE TIME I ADDITIONAL COMMENTS: —� r f Data on server/templates/forms/chain of custody (revised July 2014) 80 Lupes Drive Tel: (203)377-9984 Stratford,CT 06615 (VET Fax:(203)377-9952 e-mail:cetl@cetlabs.com li` RI1T11NVINONhlfNIX TE511NG L Client: Mr. Tim Farrelly Enviroshield,Inc. P.O.Box 1296 Stratford,CT 06615 Analytical Report CET# 6020394 Report Date:February 25,2016 Project: County Distributors, 1510 John Fitch Blvd, PO Number:26477 Connecticut Laboratory Certificate:PH 0116 New York Certification: 11982 Massachusetts laboratory Certificate:M-CT903 r ` Rhode Island Certification: 199 Page 1 of 5 CET#:6020394 SAMPLE SUMMARY The sample(s)were received at 2.9°C. This report contains analytical data associated with following samples only. Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date Fuel Oil Bottom 6020394-01 Soil 2/19/2016 02/22/2016 Analyte: Total Solids[EPA 160.3 modified] Analyst:TWF Matrix: Soil Date/Time Laboratory ID Client Sample ID Result RL Units Dilution Batch Prepared Analyzed Notes 6020394-01 Fuel Oil Bottom 88 1.0 % 1 B6B2306 02/23/2016 02/23/2016 15:33 Client Sample ID Fuel Oil Bottom Lab ID: 6020394-01 Conn.Extractable TPH Analyst:MH Method: CT ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH ND 57 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 10:08 Surrogate:Octacosane 91.1% 50-150 B6B2338 02/23/2016 0212412016 10:08 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•wHtiv.cetlabs.com Page 2 of 7-1 5 CET#:6020394 Questions related to this report should be directed to David Ditta,Timothy Fusco,or Robert Blake at 203-377-9984. Sincerely, r` p ale David Ditta Laboratory Director Report Comments: Sample Result Flags: E-The result is estimated,above the calibration range. H-The surrogate recovery is above the control limits. L-The surrogate recovery is below the control limits. B-The compound was detected in the laboratory blank. P-The Relative Percent Difference(RPD)of dual column analyses exceeds 40%. D-The RPD between the sample and the sample duplicate is high. Sample Homogenity may be a problem. +- The Surrogate was diluted out. *Cl-The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2-The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *FI-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *172-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I-The Analyte exceeds%RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result,or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 3 of 5 CET 4:6020394 CERTIFICATIONS Certified Analyses included in this Report Analyte Cerfifications CT-ETPH in.Sail ETPH CT Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires CT Connecticut Public Health PH0116 09/30/2016 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•wviw.cetlabs.com Page 4 of 5 i _ � � , � IIId0111111111�II��II��iIIldillE --.- _. ENVIRO�� � �� 6020394 L, 0 _ o 0 d LNV IRO SHIELD, INC. PRIORITY LEVEL: 250 MOFFITT STREET --'— P,O, BOX 1296 STRATFORD, CT 0661 a CHAIN OF CUSTODY Y I'ROJ,iF PROJECT LOCATION; PURCFlASE ORDER l�.J:J �, `�_E�_ �1+c 11 V I V `j' '1 -' 1't n cl� 1- �\a C_.: 0 lv '-1 7 7 O l R 1. CODES: W=WELL 0=OUTFALL WO=WASTE OIL —Rd=RUN OFF B=BOTTOM SEDIMENT Sf:`,UA SG=SLUDGE S=SOIL R=RIVER/STREAM LP=LANDFILL W W=WASTE WATER SW=L=SEilGE /�OCEAN _ \=O'r}-}GR;SPECIFY !'1'lni Ml SAMPLE' SOURCE CONT. CONY. CONT, CONT. ANALYSIS REQUESTED _ ?._ I D• -- CODE NO. TYPE SIZE PRES. DATE TIME COMMENTS/"RCP"Required? isst ES c; Gv.. �.2- AiNER CODES: P=PLASTIC PRIi:SI"fRVA'1'IVL'CODIiS: !=1CL'D L'=EPA VIAL G=GLASS A=AMBER GLASS I _ 1 I i=HYDROCHLORIC ACID HCI B=BACTERIA BOTTLE 0=OTHER;SPECIFY ( ) S=SODIUM HYROXIDE(NaOH) Na=SODIUM BISULFATE(NaHSO4 M= METHANOL(1vicOH) I S A i vlI LJ.:R'S SIGNATUR1 — AI=1 1Wf\PION DATE TRNSF . }TEM TRANSFERS NO. NO. RELINQUISHED BY ACCEP 1 TED BY DATE- TIME (�' t.)i! OVAL C ! OMMENTS: L' u V' f / Data on server/temPlates/forms/chain 01'custody (revise(i Ju!y 2014) Clean, Preserve...Protect t�C► Environmental Specialists March 31, 2016 \4r. _flan Gordon County Distributors, Inc. 1510 John Fitch Boulevard South Windsor, Connecticut 06074 Subject: Tank Removals, February 15-19, 2016 Reference: CT-DEEP UST Site ID Number 132-2292 CT-DEEP Spill Number 2016-01251 Location: 1510 John Fitch Boulevard South Windsor, Connecticut Dear Mr. Gordon: During the week of February 15, 2016, En'%>iroshield staff completed the removal of four (4) underground fuel storage tank systems located at the subject property. The groundwater classification for the subject property is GA. The tank systems were identified as follows: Tank A1R1 4,000-gallon cathodically protected steel diesel tank with fiberglass discharge piping. Tank B1R1 1,000-gallon cathodically protected steel gasoline tank with fiberglass suction piping. Tank D1 550-gallon bare steel waste oil tank. Unregistered 550-gallon bare steel #2 heating fuel oil tank. The former location of each tank is shown on a Site Sketch (not to scale) attached in Appendix A of this report. Prior to the removal of the four (4) tanks, all liquid was pumped and disposed of by Envvroshield, Inc., a State of Connecticut licensed waste transporter at Tradebe Treatment and Recycling of Bridgeport LLC, 50 Cross Street, Bridgeport, Connecticut. Copies of the disposal manifests / bills of lading are included in Appendix B of this report. .After the diesel tank system removal, soil samples were selected from the open excavations as follows: Diesel Tank Grave (North, East and West walls and Bottom center) Diesel Dispenser (beneath former dispenser location) Diesel Line (beneath midpoint of former discharge line between tank and dispenser) All of the above-referenced samples were submitted to Complete Environmental Testing (CET). CET is a State of Connecticut certified environmental laboratory located in Stratford, Connecticut. The samples were all analyzed by the Extractable Total Petroleum Hydrocarbons (ETPH), EPA Methods 8270D (Semi-volatile Organics) and 8260C (Volatile Organics). A copy of the CET Analytical Report (CET# 6020396) is included ui Appendix C; all of the samples yielded results below the applicable CT-DEEP criteria. CT Home Improvement Contractor HIC.0582591 — Westchester Home Improvement License WC-27310-1-114 P.O. Box 1296, 250 Moffitt Street, Stratford, CT 06615 (203) 380-5644 (800) 394-2268 FAX (203) 378-8736 www.enviroshield.com UST Removals — 1510 John Fitch Blvd., S. Windsor CT-DEEP UST Site ID 132-2292 CT-DEEP Spill Number 2016-01251 vlarch 31, 2016 Page Two After the gasoline tank system removal, soil samples were selected from the open excavations as follows: Gasoline Tank Grave (South, East and West walls and Bottom center) Gasoline Dispenser (beneath former dispenser location) Gasoline Line (beneath midpoint of former suction line between tank and pump) All of the above-referenced samples were submitted to CET for analysis by EPA Method 8260C (Volatile Organics) and Oxygenates. A copy of the CET Analytical Report (CET# 6020397) is included in Appendix C; all of the samples yielded results below the applicable CT-DEEP criteria with the exception of the dispenser sample that yielded a result of 41 parts per billion (ppb) of Benzene which exceeds the applicable CT-DEEP criteria level of 20 ppb for Benzene. h open excavation as follows: After the waste oil tank removal, soil samples were selected from the P P Waste Oil (North, South, East and West walls and Bottom center) All of the above-referenced samples were submitted to CET for analysis by ETPH. The Bottom sample was additionally analyzed by EPA Methods 6021A-1312 (8 RCRA Metals by SPLP), 8082A (PCBs), 8270D (Semi-volatile Organics) and 8260C (Volatile Organics). A copy of the CET Analytical Report (CET# 6020395) is included in Appendix C; all of the samples yielded results exceeding the applicable CT-DEEP criteria of 500 parts per million (ppm) of ETPH ranging from 1,100 ppm to 5,100 ppm of ETPH. All of the additional analyses for bottom sample yielded results below the laboratory detection limits for the compounds tested. After the fuel oil tank removal, a sample was collected from the bottom of the excavation and was submitted to CET for analysis by ETPH. A copy of the CET Analytical Report (CET# 6020394) is included in Appendix C; the Fuel Oil Bottom sample yielded a result below the laboratory detection limit; no petroleum was detected within the sample. The tanks were transported, cleaned and disposed of in a manner consistent with industry standards and in compliance with all Local, State and Federal Codes and Regulations. The tank graves were backfilled. UST Removals — 1510 John Fitch Blvd., S. Windsor CT-DEEP UST Site ID 132-2292 CT-DEEP Spill Number 2016-01251 March 31, 2016 Page Three As requested, Enviroshield has completed the removal of the tanks; appropriate sampling and laboratory analysis required by the CT-DEEP was completed in the former tank areas. All samples were collected, preserved and transferred using all industry standard and CT-DEEP guidance in accordance with specified EPA analytical methods. A data quality assurance (DQA) and data usability evaluation (DUE) was performed based on the supplied analytical report contained in Appendix C within this report. Based on the quality assurance & quality control (QA/QC) Certification Form and our subsequent review of the data, including but not limited to the analysis requested, number of samples collected and any exceptions listed, the laboratory data does not indicate any problems with the reported findings and it appears to be usable for its intended purpose. Notwithstanding the specific constituents listed as Exceptions(those outside of the QC/QA limits for analysis), none of the listed constituents were compounds of interest or concern. The results of analysis indicated constituents exceeding the established criteria in the former gasoline pump/dispenser area and the waste oil area. The CT-DEEP was notified as required by Law and Spill Number 2016-01251 was assigned. If you have any questions concerning any of this work,please contact me at your earliest convenience at (800) 394-2268. Sincerely, Enviroshield, Inc. 0un Farre General Manager Enclosures cc: South Windsor Fire Marshal cc: paul.clark a,ct.gov cc: deep.ustnov e,ct.gov Appendix A Site Sketch (Not to Scale) SITE SKETCH Job Requested By: Date: Job Site: 15ko Supervisor: Site Phone: Key: Furnace 0 Vent Pipe ............. Concrete Tank with fill pipe 0 Remote or Indirect Fill -------------- Asphalt Potable Well (@ Monitoring Well Fence Wood Deck --Boring Property Line BE Wall (stone) Tree <:g) Shrub (NOT TO SCALE) LSD 4.S1 a 06 C. 7 V/Saw Oft j 7f" WA'5f VIC-A- e, L CTXI--. 315 tj C,A-c tat v P.O. Box 1296, 250 Moffitt St., Stratford, CT 06615 (203) 380-5644 (800) 394-2268 FAX (203) 378-8736 www.enviroshield.com Appendix B Waste Disposal Manifests and Bills of Lading c NOR, Please print or type.(Form designed for use on elite(1 2-pitch)typewriter.) Form Approved.OMB No.2050-0039 UNIFORM HAZARDOUS 1.Generator ID Number 2.Page 1 of 3.Emergency Response Phone 4.Manifest Tracking Number �[ WASTE MANIFEST y tfi t z t : 'z 6.� 360 JJ'K 5.Generator's Name and Mailing Address r Generatorr''s,,Site Address(if different than mailing address)34rf` e f i�f i t�"J r; r if J01 ¢43�1L 7: "dsi vVi ,.�f l iw � g Generator's Phone: " f 9 4 6.Transporter 1`Compan Name _ U.S.EPA ID Number 7.Transporter 2 Company Name U.S.EPA ID Number 8.DesipViMWV jM A ldrr s jf tqjjk 3 t LL U.S.EPA ID Number . CAM%. la` Facility's Phone: ga 9b.U.S.DOT Description(including Proper Shipping Name,Hazard Class,ID Number, 10.Containers 11.Total 12.Unit 13.Waste Codes HM and Packing Group(if any)) No. Type Quantity Wt.Nol. _ 4 W i 3. ( 4. t A; 4 14.Special Handling Instructions and Additional Information ° �' < j } 15. GENERATOR'S/OFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name,and are classified,packaged, marked and labeled/placarded,and are in all respects in proper condition for transport according to applicable international and national governmental regulations.If export shipment and 1 am the Primary Exporter,I certify that the contents of this consignment conform to the terms of the attached EPAAcknowledgment of Consent. I certifylhatlhe waste minimization statement identified in 40 CFR 262.27(a)(if I am a large quantity generator)or(b)(if I am a small quantity generator)is true. Genera tors/Offeror's'PrintediTyp ad Name,' 1 ,Signature Month Day Year f. 0;1 "t 16.Intelnational Shipments rr ❑Import to U.S. ❑Export from U.S. Port of entrylexit: z Transporter signature(for exports only): Date leaving U.S.: W 17.TransporterAcknowledgment of Receipt of Materials Transporter 4'Printedliyped'Name Signature Month Day Year Z Transporter 2 Printed/Typed Name Signature. Month Day Year H 18.Discrepancy 18a.Discrepancy Indication Space ❑ Quantity ❑Type ❑Residue ❑Partial Rejection ❑Full Rejection Manifest Reference Number: 18b.Alternate Facility(or Generator) U.S.EPA ID Number J U 'Facility's Phone: w 18c.Signature of Alternate Facility(or Generator) Month Day Year a z N19.Hazardous Waste Report Management Method Codes(i.e.,codes for hazardous waste treatment,disposal,and recycling systems) LU 1. ➢ 2. 3. T ? 1 20.Designated Facility Owner or Operator:Certification of receipt hazardous materials covered by the manifest except as noted in Item 18a Printedrryped Name Signature Month Day Year' t � EPA Form 8700-22(Rev.3-05) Previous editions are obsolete. TRANSPORTER'S COPY THIS ®�J�A ®� is an acknowledgement that a bill of lading has been issued and is not the Original Bill of Lading,not a copy Shipper's No. T[� M or duplicate,covering the property named herein,and is intended solely for filing or record. Carrier EWRCSHIEM, MC. SCAC Carrier's No. CT PLMM5 RECEIVED,subject to individually determined rates or contracts that have been agreed upon in writing between the carrier and shipper,if appliy&ble,otherwise to the rates,classifications and rules that have been established by the carrier and are available to the shipper,.ot'erequ t anCL4Iapplicaple stab:arld federaltegulahgps ' at date ' r from u , the Piopedy described below,1p a6parent good order,except as noted(contents and condition of contents of packages unknown),marked,consigned,and destined as indicated 1) �¢which said company(the word company being understood throughout this contract as meaning any person or Corpbrau`on in possession orlhe property under the conimct)agrees to carry to delivery at said destination,lf on Us route,or otherwise to deliver to anothe(G°a der on the route to said destination.It is mutually agreed as to each carrier of all or any of said Property over all or any portion of said route to destination and as to each party at any time interested in all or any of said Property that every service to be performed hereunder shall be subject to all the conditions not prohibited by law,Whether printed or written,herein contained,including the conditions on the back hereof,which are hereby agreed to by the shipper and accepted for himself and his assigns. Consigned to TRADESE TR TMEN T& RECYCLING OF IDGEPOIF-IT�C Destination State County Zip Delivery 50 GF1 S SSE'.- BRHDGEEO T° CT Address Route f Delivering EH"SVIROSMIA INC. ehicle Carrier Number t Number of Weight Class subject to section 7 of conditions,if this Description o€Articles shipment is to be delivered to the consignee Packages (sub.to correction) or Rate without recourse on the consignor,the consignor shall sign the following statement: The carrier shall not make delivery of this WASTE— 0 Af{+tIN—RCR A ! IlAZ @ D A€O.& shipment without payment of freight and all other Ftl/1a7 IEV`� iYTvt"Y.f'a Liar€ €Lf' tT.. lawful charges. �» (Signature of Consignor) l FREIGHT CHARGES: Prepaid ❑ Collect ❑ COD AMT: TOTAL CHARGES: Collect On Delivery and remit to COD FEE: Prepaid ❑ $ $ Collect ❑ NOTE: Where the rate is dependent on value, shippers are required to state specifically in writing the agreed or declared value of the property. The agreed of- declared value of the property is hereby specifically stated by the shipper to be not exceeding$ per NOTE:Liability Limitation for loss or damage in this shipment may be applicable.See 49 U.S.C.14706(c)(1)(A)and n (B). Shipper: J'` '' i- _�`` `j Carrier: `� f Per: Date.___ er: 1 Date. F 1 BLS 10(Rev. 1/07) sr Ti�ll� SHIPPING ORDER mustbel legibly filled in,in Ink,in Indelible Pencil,or in es y shipper's No. Carbon,and retained by the Agent. Carrier ENVIROSHIELD, INC. SCAC Carrier's No. CT RECEIVED,subject to individually determined rates or contracts that have been agreed upon in writing between the carrier and shipper,if applicable,otherwise to the rates,classifications and rules that have been established by the carrier and are available to the shipper,on request;and al.ep icable sta�.�ililand fe ml regulations; _ at y e t l r} c / date `T 1 from Ab ,k r ,-)c the Property described below,in apparent good order,except as noted(contents and condition of contents of packages un own), rked,consigned,and destined as indicated below which said company(the word company being understood throughout this contract as meaning any person or corporation in possession of the property under the contract)agrees to carry to delivery at said destination,if on its route,or otherwise to deliver to another carrier on the route to said destination.It is mutually agreed as to each carrier of all or any of said Property over all or any portion of said route to destination and as to each party at any time interested in all or any of said Property that every service to be performed hereunder shall be subject to all the conditions not prohibited by law,whether printed or written,herein contained,including the conditions on the back hereof,which are hereby agreed to by the shipper and accepted for himself and his assigns. Consigned to TRADEBE TREATMENT& RECYCLING OF aruDGEPORT LL. Destination State County Zip Delivery 50 CROSS ST.-BRICCEPORT CT Address Route ' A1 Delivering , INC. Vehicle f Carrier ENVIROSHIELD INC Number Number of Subject to Section 7 of conditions,if this Packages Description of Articles Weight Class shipment is to be delivered to the consignee 9 (sub.to correction) or Rate without recourse on the consignor,the consignor shall sign the following statement: !(� The carrier shall not make deliveryof this WASTE, NON-RCr i LIWD, N.Q S shipment without payment of freight an all other g lawful charges. {gQ�i1UWA�T-�EAR�rt�IX) p�/y�I r i iiJr\l^rillStii;'ZiJOUS, NONE (Signature of Consignor) 1 FREIGHT CHARGES: Prepaid ❑ Collect ❑ CO® AMT: TOTAL CHARGES: Collect On Delivery and remit to COD FEE: Prepaid ❑ $ $ Collect ❑ NOTE: Where the rate is dependent on value, shippers are required to state specifically in writing the agreed or declared value of the property. The agreed or declared value of the property is hereby specifically stated by the shipper to be not exceeding$ per NOTE:Liability Limitation for-loss or damage in this shipment may be applicable.See 49 U.S.C.14706(c)(1)(A)and(B). Shipper: ,;CI^ i1 ~;- �?` ► ; ' pp ` Carrier: Per: -1'f Date: Date: Per: 'r C_.__ 1 BLS 10(Rev. 1/07) Agent must detach and retain this Shipping Order and must sign the Original Bill of Lading. Appendix C CET Analytical Reports 80 Lupes Drive Tel:(203)377-9984 Stratford,CT 06615 Fax:(203)377-9952 [VE e-mail:cetl@cetlabs.com MA HE INV11RO 1ENTAl TESTING,!NG. Client: Mr.Tim Farrelly Enviroshield,Inc. P.O.Box 1296 Stratford,CT 06615 Analytical Report CET# 6020396 Report Date:February 26,2016 Project: County Distributors, 1510 John Fitch Blvd, PO Number:26651 Connecticut Laboratory Certificate:PH 0116 New York Certification: 11982 Massachusetts laboratory Certificate:M-CT903 e,. Rhode Island Certification: 199 Page 1 of 37 CET#:6020396 SAMPLE SUMMARY The sample(s)were received at 2.9°C. This report contains analytical data associated with following samples only. Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date Diesel North 6020396-01 Soil 2/17/2016 13:30 02/22/2016 Diesel East 6020396-02 Soil 2/17/2016 13:30 02/22/2016 Diesel West 6020396-03 Soil 2/17/2016 13:30 02/22/2016 Diesel Bottom 6020396-04 Soil 2/17/2016 13:30 02/22/2016 Diesel Dispenser 6020396-05 Soil 2/17/2016 13:30 02/22/2016 Diesel Lines 6020396-06 Soil 2/17/2016 13:30 02/22/2016 Analyte:Total Solids [EPA 160.3 modified] Analyst:JM Matrix: Soil Date/Time Laboratory ID Client Sample ID Result RL Units Dilution Batch Prepared Analyzed Notes 6020396-01 Diesel North 87 1.0 % 1 136132331 02/23/2016 02/24/2016 00:00 6020396-02 Diesel East 87 1.0 % 1 B6B2331 02/23/2016 02/24/2016 00:00 6020396-03 Diesel West 89 1.0 % 1 B6B2331 02/23/2016 02/24/2016 00:00 6020396-04 Diesel Bottom 86 1.0 % I B6B2331 02/23/2016 02/24/2016 00:00 6020396-05 Diesel Dispenser 94 1.0 % 1 B6B2331 02/23/2016 02/24/2016 00:00 6020396-06 Diesel Lines 93 1.0 % 1 136132331 02/23/2016 02/24/2016 00:00 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•WiArw.cetlabs.com Page 2 of 37 CET#:6020396 Client Sample ID Diesel North Lab ID: 6020396-01 Conn.Extractable TPH Analyst: MH Method: CT ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH ND 58 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 12:30 Surrogate:Octacosane 102% 50-150 136132338 02/23/2016 021241201612:30 Semivolatile Organics Analyst:ALB Method: EPA 8270D Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Naphthalene ND 350 1 EPA 3545A 136132506 02/25/2016 02/25/2016 16:41 2-Methyl Naphthalene ND 350 1 EPA 3545A 136B2506 02/25/2016 02/25/2016 16:41 Acenaphthylene ND 350 1 EPA 3545A B6132506 02/25/2016 02/25/2016 16:41 Acenaphthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 16:41 Fluorene ND 350 1 EPA 3545A B6132506 02/25/2016 02/25/2016 16:41 Phenanthrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 16:41 Anthracene ND 350 I EPA 3545A B6132506 02/25/2016 02/25/2016 16:41 Fluoranthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 16:41 Pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 16:41 Benzo[a]anthracene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 16:41 Chrysene ND 350 1 EPA 3545A 136132506 02/25/2016 02/25/2016 16:41 Benzo[b]fluoranthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 16:41 Benzo[k]fluoranthene ND 350 1 EPA 3545A 136B2506 02/25/2016 02/25/2016 16:41 Benzo[a]pyrene ND 350 1 EPA 3545A 136132506 02/25/2016 02/25/2016 16:41 Indeno[1,2,3-cd]pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 16:41 Dibenz[a,h]anthracene ND 350 1 EPA 3545A 136132506 02/25/2016 02/25/2016 16:41 Benzo[g,h,i]perylene ND 350 1 EPA 3545A 136132506 02/25/2016 02/25/2016 16:41 Surrogate:Nitrobenzene-d5 31.3% 30-130 136132506 02/25/2016 021251201616.41 Surrogate:2-Fluorobiphenyl 37.2% 30-130 136B2506 02/25/2016 021251201616.41 Surrogate:Teiphenyl-d14 39.3% 30-130 136B2506 02/25/2016 021251201616:41 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 3 0f 37 CET#:6020396 Client Sample ID Diesel North Lab ID: 6020396-01 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 17 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 *F2 Chloromethane ND 11 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *F2*C2 Vinyl Chloride ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *F2*C2 Bromomethane ND 11 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *F2*C2 Chloroethane ND 11 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 Trichlorofluoromethane ND 45 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:04 Acetone ND 170 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Acrylonitrile ND 9.0 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Trichlorotrifluoroethane ND 45 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 1,1-Dichloroethene ND 5.6 1.96 EPA5035A-L 136B2514 02/25/2016 02/25/2016 15:04 Methylene Chloride ND 56 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Carbon Disulfide ND 11 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Methyl-t-Butyl Ether(MTBE) ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 trans-1,2-Dichloroethene ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 ],I-Dichloroethane ND 5.6 1.96 EPA5035A-L 136132514 02/25/2016 02/25/2016 15:04 2-Butanone(MEK) ND 28 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 2,2-Dichloropropane ND 5.6 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 cis-1,2-Dichloroethene ND 5.6 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 Chloroform ND 5.6 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 Tetrahydrofuran ND 28 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 1,1,1-Trichloroethane ND 5.6 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Carbon Tetrachloride ND 5.6 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 1,1-Dichloropropene ND 5.6 1.96 EPA5035A-L B6132514 02/25/2016 02/25/2016 15:04 Benzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,2-Dichloroethane ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Trichloroethene ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 1,2-Dichloropropane ND 5.6 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:04 Dibromomethane ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 Bromodichloromethane ND 5.6 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 Methyl Isobutyl Ketone ND 28 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 cis-1,3-Dichloropropene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Toluene ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 trans-1,3-Dichloropropene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 2-Hexanone ND 28 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,1,2-Trichloroethane ND 5.6 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Teti achloroethene ND 5.6 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,3-Dichloropropane ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Complete Environmental Testing,Inc. 7-1 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•w"ryv.cetlabs.com Page 4 of 37 CET#:6020396 Client Sample ID Diesel North Lab ID: 6020396-01 Volatile Organics Analyst: TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dibromochloromethane ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,2-Dibromoethane ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 trans-1,4-Dichloro-2-Butene ND 28 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Chlorobenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,1,1,2-Tetrachloroethane ND 5.6 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Ethylbenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 m+p Xylenes ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 o-Xylene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Styrene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *C2 Bromofonn ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Isopropylbenzene ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 1,1,2,2-Tetrachloroethane ND 5.6 1.96 EPA5035A-L B6132514 02/25/2016 02/25/2016 15:04 Bromobenzene ND 5.6 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:04 1,2,3-Trichloropropane ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 n-Propylbenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 2-Chlorotoluene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *C2 4-Chlorotoluene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *C2 1,3,5-Trimethylbenzene ND 5.6 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *C2 tert-Butylbenzene ND 5.6 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:04 1,2,4-Trimethylbenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 sec-Butylbenzene ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 1,3-Dichlorobenzene ND 5.6 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:04 *C2 4-Isopropyltoluene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,4-Dichlorobenzene ND 5.6 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,2-Dichlorobenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *F2*C2 n-Butylbenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 *C2 1,2-Dibromo-3-Chloropropane ND 5.6 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:04 1,2,4-Trichlorobenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Hexachlorobutadiene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Naphthalene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 1,2,3-Tiichlorobenzene ND 5.6 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:04 Surrogate:1,2-Dichloroethane-d4 104% 70-130 B6B2514 02/25/2016 021251201615:04 Surrogate:Tohrene-d8 89.5% 70-130 B6B2514 02/25/2016 0212512016 15:04 Surrogate:4-Bromofluoroberzene 85.5% 70-130 B6B2514 02/25/2016 0212512016 15:04 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615*Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com. Page 5 of 37 CET#:6020396 Client Sample ID Diesel East Lab ID: 6020396-02 Conn.Extractable TPH Analyst: MH Method: CT ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH ND 58 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 12:54 Surrogate:Octacosane 97.3% 50-150 B6B2338 02/23/2016 0212412016 12:54 Semivolatile Organics Analyst:ALB Method: EPA 8270D Matrix: Soil Result RL Datefrime Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Naphthalene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 2-Methyl Naphthalene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Acenaphthylene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Acenaphthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Fluorene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Phenanthrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Anthracene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Fluoranthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Benzo[a]anthracene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Chrysene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Benzo[b]fluoranthene ND 350 1 EPA 3545A 136B2506 02/25/2016 02/25/2016 17:16 Benzo[k]fluoranthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 1716 Benzo[a]pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:16 Indeno[1,2,3-cd]pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/251201617:16 Dibenz[a,h]anthracene ND 350 1 EPA3545A B6132506 02/25/2016 02/25/201617.16 Benzo[g,h,i]perylene ND 350 1 EPA 3545A B6132506 02/25/2016 02/25/2016 17:16 Surrogate:Nitrobenzene-d5 43.6% 30-130 B6B2506 02/25/2016 021251201617:16 Surrogate:2-Fluorobiphenyl 50.5% 30-130 B6B2506 02/25/2016 021251201617:16 Surrogate:Teiphenyl-d]4 55.3% 30-130 B6B2506 02/25/2016 021251201617:16 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•vmrw.cetlabs.com Page 6 of 37 CET#t:6020396 Client Sample ID Diesel East Lab ID: 6020396-02 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 18 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 *F2 Chloromethane ND 12 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 *F2*C2 Vinyl Chloride ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 *F2*C2 Bromomethane ND 12 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 *F2*C2 Chloroethane ND 12 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Trichlorofluoromethane ND 49 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Acetone ND 180 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Acrylonitrile ND 9.8 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Trichlorotrifluoroethane ND 49 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,1-Dichloroethene ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Methylene Chloride ND 61 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Carbon Disulfide ND 12 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Methyl-t-Butyl Ether(MTBE) ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 trans-1,2-Dichloroethene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 ],I-Dichloroethane ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 2-Butanone(MEK) ND 31 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 2,2-Dichloropropane ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 cis-1,2-Dichloroethene ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Chloroform ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Tetrahydrofuran ND 31 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,1,1-Trichloroethane ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Carbon Tetrachloride ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 ],I-Dichloropropene ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Benzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,2-Dichloroethane ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Trichloroethene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,2-Dichloropropane ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15.28 Dibromomethane ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Bromodichloromethane ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Methyl Isobutyl Ketone ND 31 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 1528 cis-1,3-Dichloropropene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Toluene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 trans-1,3-Dichloropropene ND &1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 2-Hexanone ND 31 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,1,2-Trichloroethane ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Teh-achloroethene ND 6.1 2.13 EPA 5035A-L B61325I4 02/25/2016 02/25/2016 15.28 13-Dichloropropane ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetiabs.com Page 7 of 37 CET#:6020396 Client Sample ID Diesel East Lab ID: 6020396-02 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dibromochloromethane ND 6.1 2.13 EPA5035A-L B6132514 02/25/2016 02/25/2016 15:28 1,2-Dibromoethane ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 trans-1,4-Dichloro-2-Butene ND 31 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Chlorobenzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,1,1,2-Tetrachloroethane ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Ethylbenzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 m+p Xylenes ND 6.1 2.13 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:28 o-Xylene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Styrene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 *C2 Bromoform ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Isopropylbenzene ND 6.1 2.13 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:28 1,1,2,2-Tetrachloroethane ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Bromobenzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,2,3-Trichloropropane ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 n-Propylbenzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 2-Chlorotoluene ND 6.1 2.13 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:28 *C2 4-Chlorotoluene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 *C2 1,3,5-Trimethylbenzene ND 6.1 2.13 EPA5035A-L B6132514 02/25/2016 02/25/2016 15:28 *C2 tert-Butylbenzene ND 6.1 2.13 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:28 1,2,4-Trimethylbenzene ND 6.1 2.13 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:28 sec-Butyl benzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,3-Dichlorobenzene ND 6.1 2.13 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:28 *C2 4-Isopropyholuene ND 6.1 2.13 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:28 1,4-Dichlorobenzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,2-Dichlorobenzene ND 6.1 2.13 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:28 *F2*C2 n-Butylbenzene ND 6.1 2.13 EPA5035A-L B6132514 02/25/2016 02/25/2016 15:28 *C2 1,2-Dibromo-3-Chloropropane ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,2,4-Trichlorobenzene ND 6.1 2.13 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:28 Hexachlorobutadiene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Naphthalene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 1,2,3-Trichlorobenzene ND 6.1 2.13 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:28 Surrogate:1,2-Dichloroethane-d4 109% 70-130 B6132514 02/25/2016 021251201615:28 Surrogate:Toluene-d8 93.8% 70-130 B6B2514 02/25/2016 021251201615:28 Surrogate:4-Bron2o luoroben:ene 84.3% 70-130 B6B2514 02/25/2016 021251201615:28 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984*Fax:203-377-9952•www.cetlabs.com Page 8 of 37 CET 4:6020396 Client Sample ID Diesel West Lab ID: 6020396-03 Conn.Extractable TPH Analyst: MH Method: CT ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH ND 56 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 13:18 Surrogate:Octacosane 97.8% 50-150 B6B2338 02/23/2016 021241201613:18 Semivolatile Organics Analyst:ALB Method: EPA 8270D Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Naphthalene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 2-Methyl Naphthalene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Acenaphthylene ND 340 1 EPA3545A B6B2506 02/25/2016 02/25/2016 17:51 Acenaphthene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Fluorene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Phenanthrene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Anthracene ND 340 1 EPA 3545A 136B2506 02/25/2016 02/25/2016 17:51 Fluoranthene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Pyrene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Benzo[a]anthracene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Chrysene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Benzo[b]fluoranthene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Benzo[b]fluoranthene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Benzo[a]pyrene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Indeno[l,2,3-cd]pyrene ND 340 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 17:51 Dibenz[a,h]anthracene ND 340 1 EPA 3545A 136B2506 02/25/2016 02/25/2016 17:51 Benzo[g,h,i]perylene ND 340 1 EPA 3545A 136B2506 02/25/2016 02/25/2016 17:51 Surrogate:Nitroben_ene-d5 51.2% 30-130 B6B2506 02/25/2016 0212512016 17:51 Surrogate:2-Fluorobiphenyl 64.0% 30-130 B6B2506 02/25/2016 021251201617:51 Surrogate:Teiphenyl-d14 84.7% 30-130 B6B2506 02/25/2016 021251201617:51 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 9 of 37 CET#:6020396 Client Sample ID Diesel West Lab ID: 6020396-03 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes _] Dichlorodifluoromethane ND 16 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *F2 Chloromethane ND 11 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *F2*C2 Vinyl Chloride ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *F2*C2 Bromomethane ND 11 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *F2*C2 Chloroethane ND 11 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Trichlorofluoromethane ND 43 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Acetone ND 160 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Acrylonitrile ND 8.7 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Trichlorotrifluoroethane ND 43 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,1-Dichloroethene ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Methylene Chloride ND 54 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Carbon Disulfide ND 11 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Methyl-t-Butyl Ether(MTBE) ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 trans-1,2-Dichloroethene ND 5.4 193 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 ],I-Dichloroethane ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/201615:51 2-Butanone(MEK) ND 27 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:51 2,2-Dichloropropane ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 cis-1,2-Dichloroethene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Chloroform ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Tetrahydrofuran ND 27 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,l,l-Trichloroethane ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Carbon Tetrachloride ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,1-Dichloropropene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Benzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2-Dichloroethane ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Trichloroethene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2-Dichloropropane ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Dibromomethane ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Bromodichloromethane ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Methyl Isobutyl Ketone ND 27 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 cis-1,3-Dichloropropene ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Toluene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 trans-1,3-Dichloropropene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15.51 2-Hexanone ND 27 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,1,2-Trichloroethane ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Teirachloroethene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,3-Dichloropropane ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•wwwxetlabs.coin Page 13 of 37 CET 4: 6020396 Client Sample ID Diesel West Lab ID: 6020396-03 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dibromochloromethane ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2-Dibromoethane ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 trans-1,4-Dichloro-2-Butene ND 27 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 15:51 Chlorobenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,1,1,2-Tetrachloroethane ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Ethylbenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 m+p Xylenes ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 o-Xylene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Styrene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *C2 Bromofonn ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Isopropyl benzene ND 5A 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,1,2,2-Tetrachloroethane ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Bromobenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2,3-Trichloropropane ND 5.4 1.93 EPA5035A-L B6132514 02/25/2016 02/25/2016 15:51 n-Propylbenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 2-Chlorotoluene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *C2 4-Chlorotoluene ND 5.4 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 15:51 *C2 1,3,5-Trimethylbenzene ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *C2 tert-Butylbenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2,4-Trimethylbenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 sec-Butyl benzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,3-Dichlorobenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *C2 4-Isopropyltoluene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,4-Dichlorobenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2-Dichlorobenzene ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *F2*C2 n-Buylbenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 *C2 1,2-Dibromo-3-Chloropropane ND 5.4 1.93 EPA5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2,4-Trichlorobenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Hexachlorobutadiene ND 5.4 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 15:51 Naphthalene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 1,2,3-Tiichlorobenzene ND 5.4 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 15:51 Surrogate:1,2-Dichloroethane-d4 109% 70-130 B6B2514 02/25/2016 021251201615:51 Surrogate:Toluene-& 110% 70-130 B6B2514 02/25/2016 021251201615:51 Surrogate:4-BrontoJluoroben ene 85.8% 70-130 B6B2514 02/25/2016 021251201615:51 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 11 of 37 CET 4:6020396 Client Sample ID Diesel Bottom Lab ID: 6020396-04 Conn.Extractable TPH Analyst: MH Method: CT ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH ND 58 1 EPA 3550C B6B2338 02/23/2016 02/24/2016 13:41 Surrogate:Octacosane 101% 50-150 B6B2338 02/23/2016 0212412016 13:41 Semivolatile Organics Analyst:ALB Method: EPA 8270D Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Naphthalene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 2-Methyl Naphthalene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Acenaphthylene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Acenaphthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Fluorene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Phenanthrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Anthracene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Fluoranthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Benzo[a]anthracene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Chrysene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Benzo[k]fluoranthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Benzo[k]fluoranthene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Benzo[a]pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Indeno[1,2,3-cd]pyrene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Dibenz[a,h]anthracene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Benzo[g,h,i]perylene ND 350 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 18:26 Surrogate:Nitrobenzene-d5 53.6% 30-130 B6B2506 02/25/2016 021251201618:26 Surrogate:2-Fluorobiphenyl 63.2% 30-130 B6B2506 02/25/2016 021251201618:26 Surrogate:Teiphenyl-d14 72.5% 30-130 B6B2506 02/25/2016 021251201618:26 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 12 of 37 CET#:6020396 Client Sample ID Diesel Bottom Lab ID: 6020396-04 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix:Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 17 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 *F2 Chloromethane ND 12 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 *F2*C2 Vinyl Chloride ND 5.8 2 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 16:14 *F2*C2 Bromomethane ND 12 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 *F2*C2 Chloroethane ND 12 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Trichlorofluoromethane ND 46 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Acetone ND 170 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16.14 Acrylonitrile ND 9.3 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Trichlorotrifluoroethane ND 46 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 l,l-Dichloroethene ND 5.8 2 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Methylene Chloride ND 58 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Carbon Disulfide ND 12 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Methyl-t-Butyl Ether(MTBE) ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 trans-1,2-Dichloroethene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,1-Dichloroethane ND 5.8 2 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:14 2-Butanone(MEK) ND 29 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 2,2-Dichloropropane ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 cis-1,2-Dichloroethene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Chloroform ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Tetrahydrofuran ND 29 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,1,1-Trichloroethane ND 5.8 2 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Carbon Tetrachloride ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,1-Dichloropropene ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 Benzene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,2-Dichloroethane ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Trichloroethene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,2-Dichloropropane ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Dibromomethane ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Bromodichloromethane ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Methyl Isobutyl Ketone ND 29 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 cis-1,3-Dichloropropene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Toluene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 trans-1,3-Dichloropropene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 2-Hexanone ND 29 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,1,2-Trichloroethane ND 5.8 2 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Tetrachloroethene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,3-Dichloropropane ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 13 of 37 CET#:6020396 Client Sample ID Diesel Bottom Lab ID: 6020396-04 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dibromochloromethane ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 1,2-Dibromoethane ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 trans-1,4-Dichloro-2-Butene ND 29 2 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 16:14 Chlorobenzene ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 1,1,1,2-Tetrachloroethane ND 5.8 2 EPA5035A-L 136B2514 02/25/2016 02/25/2016 16:14 Ethylbenzene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 m+p Xylenes ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 o-Xylene ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 Styrene ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 *C2 Bromoform ND 5.8 2 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 16:14 Isopropyl benzene ND 5.8 2 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 16:14 1,1,2,2-Tetrachloroethane ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Bromobenzene ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 1,2,3-Trichloropropane ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 n-Propylbenzene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 2-Chlorotoluene ND 5.8 2 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 16:14 *C2 4-Chlorotoluene ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 *C2 1,3,5-Trimethylbenzene ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 *C2 tert-Butylbenzene ND 5.8 2 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 16:14 1,2,4-Trimethylbenzene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 sec-Butylbenzene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 1,3-Dichlorobenzene ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 *C2 4-Isopropyltoluene ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 1,4-Dichlorobenzene ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 1,2-Dichlorobenzene ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 *F2*C2 n-Butylbenzene ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 *C2 1,2-Dibromo-3-Chloropropane ND 5.8 2 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:14 1,2,4-Trichlorobenzene ND 5.8 2 EPA5035A-L 136B2514 02/25/2016 02/25/2016 16:14 Hexachlorobutadiene ND 5.8 2 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:14 Naphthalene ND 5.8 2 EPA 5035A-L 136132514 02/25/2016 02/25/2016 16:14 1,2,3-Trichlorobenzene ND 5.8 2 EPA5035A-L 136132514 02/25/2016 02/25/201616.14 Surrogate:1,2-Dichloroethane-d4 116% 70-130 B6132514 02/25/2016 021251201616:14 Surrogate:Tohuene-d8 101% 70-130 136132514 02/25/2016 0212512016 16:14 Surrogate:4-Bromofluoroben_ene 88.4% 70-130 B6B2514 02/25/2016 021251201616:14 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•wwtiv.cetlabs.com Page 14 of 37 CET#:6020396 Client Sample ID Diesel Dispenser Lab ID: 6020396-05 Conn.Extractable TPH Analyst: MH Method: CT ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH 8o 53 1 EPA 3550C B6B2339 02/23/2016 02/24/2016 07:51 2 Surrogate:Octacosane 62.2% 50-150 B6B2339 02/23/2016 0212412016 07.51 2 C9-C28 Fuel Oil Range Semivolatile Organics Analyst:ALB Method: EPA 8270D Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Naphthalene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 2-Methyl Naphthalene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Acenaphthylene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Acenaphthene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Fluorene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Phenanthrene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Anthracene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Fluoranthene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Pyrene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Benzo[a]anthracene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Chrysene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Benzo[b]fluoranthene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Benzo[k]fluoranthene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Benzo[a]pyrene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Indeno[1,2,3-cd]pyrene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Dibenz[a,h]anthracene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Benzo[g,h,i]perylene ND 320 1 EPA 3545A B6B2506 02/25/2016 02/25/2016 23:16 Surrogate:Nitroben_ene-d5 58.3% 30-130 B6B2506 02/25/2016 0212512016 23:16 Surrogate:2-Fluorobiphenyl 85.6% 30-130 B6B2506 02/25/2016 0212512016 23:16 Surrogate:Terpheuyl-dM 74.4% 30-130 B6B2506 02/25/2016 0212512016 23:16 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 15 of 37 CET#:6020396 Client Sample ID Diesel Dispenser Lab ID: 6020396-05 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 16 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *F2 Chloromethane ND 10 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *F2*C2 Vinyl Chloride ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *F2*C2 Bromomethane ND 10 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *F2*C2 Chloroethane ND 10 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Trichlorofluoromethane ND 41 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Acetone ND 160 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Acrylonitrile ND 8.3 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Trichlorotrifluoroethane ND 41 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 I,1-Dichloroethene ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Methylene Chloride ND 52 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Carbon Disulfide ND 10 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Methyl-t-Butyl Ether(MTBE) ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 trans-1,2-Dichloroethene ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,1-Dichloroethane ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 2-Butanone(MEK) ND 26 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 2,2-Dichloropropane ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 cis-1,2-Dichloroethene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Chloroform ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Tetrahydrofuran ND 26 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,1,1-Trichloroethane ND 5.2 1.95 EPA5035A-L 136B2514 02/25/2016 02/25/2016 16:38 Carbon Tetrachloride ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,1-Dichloropropene ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/201616.38 Benzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2-Dichloroethane ND 5.2 1.95 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 1638 Trichloroethene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2-Dichloropropane ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Dibromomethane ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Bromodichloromethane ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Methyl Isobutyl Ketone ND 26 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 cis-1,3-Dichloropropene ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Toluene ND 5.2 1.95 EPA 5035A-L B6132514 02/25/2016 02/25/2016 16:38 trans-l,3-Dichloropropene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 2-Hexanone ND 26 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,1,2-Trichloroethane ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Tetrachloroethenc ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,3-Dichloropropane ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 16 of 37 CET#:6020396 Client Sample ID Diesel Dispenser Lab ID: 6020396-05 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL DatePfime Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dibromochloromethane ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2-Dibromoethane ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 trans-1,4-Dichloro-2-Butene ND 26 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Chlorobenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,1,1,2-Tetrachloroethane ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/201616.38 Etylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 m+p Xylenes ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 o-Xylene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Styrene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *C2 Bromoform ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Isopropylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,1,2,2-Tetrachloroethane ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Bromobenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2,3-Trichloropropane ND 5.2 1.95 EPA5035A-L B6B2514 02/25/2016 02/25/2016 16:38 n-Propylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 2-Chlorotoluene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *C2 4-Chlorotoluene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *C2 1,3,5-Trimethylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *C2 tert-Butylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2,4-Trimethylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 sec-Butylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,3-Dichlorobenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *C2 4-Isopropyltoluene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,4-Dichlorobenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2-Dichlorobenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *F2*C2 n-Butylbenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 *C2 1,2-Dibromo-3-Chloropropane ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2,4-Trichlorobenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Hexachlorobutadiene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Naphthalene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 1,2,3-Trichlorobenzene ND 5.2 1.95 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 16:38 Surrogate:1,2-Dichloroethane-d4 107% 70-130 B6B2514 02/25/2016 021251201616:38 Surrogate:Tohrene-d8 101% 70-130 B6B2514 02/25/2016 021251201616:38 Surrogate:4-Bromofluoroben ene 88.3% 70-130 B6B2514 02/25/2016 021251201616:38 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 17 of 37 CET#:6020396 Client Sample ID Diesel Lines Lab ID: 6020396-06 Conn.Extractable TPH Analyst: MH Method: CT ETPH Matrix: Soil Result RL Date/Time Analyte (mg/kg dry) (mg/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes ETPH 54 54 1 EPA 3550C B6B2339 02/23/2016 02/24/2016 08:14 2 Surrogate:Octacosane 68.9% 50-150 B6B2339 02/23/2016 0212412016 08:14 2 C9-C28 Fuel Oil Range Semivolatile Organics Analyst:ALB Method: EPA 8270D Matrix:Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Naphthalene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 2-Methyl Naphthalene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Acenaphthylene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Acenaphthene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Fluorene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Phenanthrene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Anthracene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Fluoranthene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Pyrene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Benzo[a]anthracene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Chrysene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Benzo[blfluoranthene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Benzo[k]fluoranthene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Benzo[a]pyrene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Indeno[1,2,3-cd]pyrene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Dibenz[a,h]anthracene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Benzo[g,h,i]perylene ND 320 1 EPA 3545A B6B2308 02/23/2016 02/25/2016 19:01 Surrogate:Nitroben_ene-d5 65.9% 30-130 B6B2308 02/23/2016 0212512016 19:01 Surrogate:2-Fluorobiphenyl 80.0% 30-130 B6B2308 02/23/2016 021251201619:01 Surrogate:Terphenyl-dM 89.3% 30-130 B6B2308 02/23/2016 021251201619:01 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•wmwcetlabs.corn Page 18 of 37 CET#:6020396 Client Sample ID Diesel Lines Lab ID: 6020396-06 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 16 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *F2 Chloromethane ND 11 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *F2*C2 Vinyl Chloride ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *F2*C2 Bromomethane ND 11 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *F2*C2 Chloroethane ND 11 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:01 Trichlorofluoromethane ND 42 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:01 Acetone ND 160 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Acrylonitrile ND 8A 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Trichlorotrifluoroethane ND 42 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 l,l-Dichloroethene ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Methylene Chloride ND 53 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Carbon Disulfide ND 11 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Methyl-t-Butyl Ether(MTBE) ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 trans-l,2-Dichloroethene ND 5.3 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:01 1,1-Dichloroethane ND 5.3 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:01 2-Butanone(MEK) ND 26 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:01 2,2-Dichloropropane ND 5.3 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:01 cis-1,2-Dichloroethene ND 5.3 1.97 EPA5035A-L B6132514 02/25/2016 02/25/2016 17:01 Chloroform ND 5.3 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:01 Tetrahydrofuran ND 26 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:01 1,1,1-Trichloroethane ND 5.3 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:01 Carbon Tetrachloride ND 5.3 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:01 1,1-Dichloropropene ND 5.3 1.97 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:01 Benzene ND 5.3 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:01 1,2-Dichloroethane ND 5.3 1.97 EPA5035A-L 136132514 02/25/2016 02/25/201617.01 Trichloroethene ND 5.3 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:01 1,2-Dichloropropane ND 5.3 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:01 Dibromomethane ND 5.3 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:01 Bromodichloromethane ND 5.3 1.97 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:01 Methyl Isobutyl Ketone ND 26 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:01 cis-1,3-Dichloropropene ND 5.3 1.97 EPA5035A-L 136132514 02/25/2016 02/25/201617.01 Toluene ND 5.3 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:01 trans-1,3-Dichloropropene ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 2-Hexanone ND 26 1.97 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:01 1,1,2-Trichloroethane ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Tetrachloroethene ND 5.3 1.97 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:01 1,3-Dichloropropane ND 53 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 19 of 37 CET#:6020396 Client Sample ID Diesel Lines Lab ID: 6020396-06 Volatile Organics Analyst: TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dibromochloromethane ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,2-Dibromoethane ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 trans-1,4-Dichloro-2-Butene ND 26 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Chlorobenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,1,1,2-Tetrachloroethane ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Ethylbenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 m+p Xylenes ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 o-Xylene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Styrene ND 53 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *C2 Bromofonn ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Isopropylbenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,1,2,2-Tetrachloroethane ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Bromobenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,2,3-Trichloropropane ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 n-Propylbenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 2-Chlorotoluene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *C2 4-Chlorotoluene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *C2 1,3,5-Trimethylbenzene ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *C2 tert-Butyl benzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,2,4-Trimethylbenzene ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 sec-Butylbenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,3-Dichlorobenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *C2 4-Isopropyltoluene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,4-Dichlorobenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,2-Dichlorobenzene ND 53 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *F2*C2 n-Butylbenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 *C2 1,2-Dibromo-3-Chloropropane ND 5.3 1.97 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,2,4-Trichlorobenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Hexachlorobutadiene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Naphthalene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 1,2,3-Trichlorobenzene ND 5.3 1.97 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:01 Surrogate:1,2-Dichloroethane-d4 111% 70-130 B6B2514 02/25/2016 0212512016 17:01 Surrogate:Toluene-d8 98.8% 70-130 B6B2514 02/25/2016 0212512016 17:01 Surrogate:4-Bronuofluoroheuz:ene 86.0% 70-130 B6B2514 02/25/2016 021251201617:01 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•WIAW.cetlabs.com Page 20 0737 CET#:6020396 QUALITY CONTROL SECTION Batch B6B2308-EPA 8270D Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2308-BLK1) Prepared:2/23/2016 Analyzed:2/24/2016 Naphthalene ND 300 2-Methyl Naphthalene ND 300 Acenaphthylene ND 300 Acenaphthene ND 300 Fluorene ND 300 Phenanthrene ND 300 Anthracene ND 300 Fluoranthene ND 300 Pyrene ND 300 Benzo[a]anthracene ND 300 Chrysene ND 300 Benzo[b]fluoranthene ND 300 Benzo[k]fluoranthene ND 300 Benzo[a]pyrene ND 300 Indeno[1,2,3-cd]pyrene ND 300 Dibenz[a,h]anthracene ND 300 Benzo[g,h,i]perylene ND 300 Surrogate:Nitrobenzene-d5 53.4 30-130 Surrogate:2-Fluorobiphetyl 53.7 30-130 Surrogate:Terphenyl-d]4 55.3 30-130 LCS(B6B2308-BSI) Prepared:2/23/2016 Analyzed:2/24/2016 Naphthalene 2030 300 4,000.000 50.6 40-140 2-Methyl Naphthalene 2080 300 4,000.000 52.0 40-140 Acenaphthylene 2100 300 4,000.000 52.5 40-140 Acenaphthene 2150 300 4,000.000 53.8 40-140 Fluorene 2250 300 4,000.000 56.3 40-140 Phenanthrene 2300 300 4,000.000 57.4 40-140 Anthracene 2350 300 4,000.000 58.7 40-140 Fluoranthene 2360 300 4,000.000 58.9 40-140 Pyrene 2370 300 4,000.000 59.2 40-140 Benzo[a]anthracene 2410 300 4,000.000 60.2 40-140 Chrysene 2420 300 4,000.000 60.5 40-140 Benzo[b]fluoranthene 3210 300 4,000.000 80.2 40-140 Benzo[k]fluoranthene 3510 300 4,000.000 87.8 40-140 Benzo[a]pyrene 3550 300 4,000.000 88.7 40-140 Indeno[1,2,3-cd]pyrene 3680 300 4,000.000 92.0 40-140 Dibenz[a,h]anthracene 3610 300 4,000.000 90.3 40-140 Benzo[g,h,i]perylene 3680 300 4,000.000 92.1 40-140 Surrogate:Nitrobenzene-d5 51.4 30-130 Surrogate:2-Fluorobiphenyl 52.9 30-130 Surrogate:Terphenyl-d14 52.6 30-130 Complete Environmental Testing,Inc. p g. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•WWW.cetlabs.com Page 21 o 337 CET#:6020396 Batch B6B2338-CT-ETPH Result RL Spike Source %Rec RPD Analyte (mg/kg) (mg/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2338-BLK1) Prepared:2/23/2016 Analyzed:2/24/2016 ETPH ND 50 Surrogate:Oclacosane 106 50-150 LCS(B6B2338-BSI) Prepared:2/23/2016Analyzed:2/24/2016 ETPH 1270 50 1,500.000 84.6 60-120 Surrogale:Oclacosane 94.6 50-150 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•"wv.cetlabs.coin Page 22 of 37 CET#:6020396 Batch B6B2339-CT-ETPH Result RL Spike Source %Rec RPD Analyte (mg/kg) (mg/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2339-BLKI) Prepared:2/23/2016 Analyzed:2/24/2016 ETPH ND 50 Surrogate:Octacosane 839 50-150 LCS(B6B2339-BS1) Prepared:2/23/2016 Analyzed:2/24/2016 ETPH 1390 50 1,500.000 92.8 60-120 Surrogate:Oelacosane 88.8 50-I50 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 23 of 37 CET#:6020396 Batch B6B2506-EPA 8270D Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2506-BLKI) Prepared:2/25/2016 Analyzed:2/25/2016 Naphthalene ND 300 2-Methyl Naphthalene ND 300 Acenaphthylene ND 300 Acenaphthene ND 300 Fluorene ND 300 Phenanthrene ND 300 Anthracene ND 300 Fluoranthene ND 300 Pyrene ND 300 Benzo[a]anthracene ND 300 Chrysene ND 300 Benzo[b]fluoranthene ND 300 Benzo[k]fluoranthene ND 300 Benzo[a]pyrene ND 300 Indeno[1,2,3-cd]pyrene ND 300 Dibenz[a,h]anthracene ND 300 Benzo[g,h,i]perylene ND 300 Surrogate:Nitrobenzene-d5 70.9 30-130 Surrogate:2-Fluorobiphenyl 93.2 30-130 Surrogate:Terphenyl-d14 84.9 30-130 LCS(B6B2506-BSI) Prepared:2/25/2016 Analyzed:2/25/2016 Naphthalene 3190 300 4,000.000 79.8 40-140 2-Methyl Naphthalene 3150 300 4,000.000 78.7 40-140 Acenaphthylene 3160 300 4,000.000 79.1 40-140 Acenaphthene 3550 300 4,000.000 88.6 40-140 Fluorene 3580 300 4,000.000 89.4 40-140 Phenanthrene 3590 300 4,000.000 89.6 40-140 Anthracene 3380 300 4,000.000 84.4 40-140 Fluoranthene 3640 300 4,000.000 91.1 40-140 Pyrene 3280 300 4,000.000 81.9 40-140 Benzo[a]anthracene 3600 300 4,000.000 89.9 40-140 Chrysene 3480 300 4,000.000 87.1 40-140 Benzo[b]fluoranthene 3260 300 4,000.000 81.5 40-140 Benzo[k]fluoranthene 4350 300 4,000.000 109 40-140 Benzo[a]pyrene 3860 300 4,000.000 96.4 40-140 Indeno[1,2,3-cd]pyrene 3600 300 4,000.000 90.0 40-140 Dibenz[a,h]anthracene 4080 300 4,000.000 102 40-140 Benzo[g,h,i]perylene 3240 300 4,000.000 81.0 40-140 Surrogate:Nitrobenzene-d5 78.4 30-130 Surrogate:2-Fluorohiphenyl 85.2 30-130 Surrogate:Terphenyl-d14 79.3 30-130 Duplicate(B6B2506-DUPI) Source:6020396-05 Prepared:2/25/2016 Analyzed:2/26/2016 Naphthalene ND 320 ND 30 2-Methyl Naphthalene ND 320 ND 30 Acenaphthylene ND 320 ND 30 Acenaphthene ND 320 ND 30 Fluorene ND 320 ND 30 Phenanthrene ND 320 ND 30 Anthracene ND 320 ND 30 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 24 of 37 CET 4:6020396 Result RL Spike Source %Rec RPD Analyte (ug/kg dry) (ug/kg dry) Level Result %Rec Limits RPD Limit Notes Duplicate(B6132506-DUP1)-Continued Source:6020396-05 Prepared:2/25/2016 Analyzed:2/26/2016 Fluoranthene ND 320 ND 30 Pyrene ND 320 ND 30 Benzo[a]anthracene ND 320 ND 30 Chrysene ND 320 ND 30 Benzo[b]fluoranthene ND 320 ND 30 Benzo[b]fluoranthene ND 320 ND 30 Benzo[a]pyrene ND 320 ND 30 Indeno[1,2,3-ed]pyrene ND 320 ND 30 Dibenz[a,h]anthracene ND 320 ND 30 Benzo[g,h,i]perylene ND 320 ND 30 Surrogate:Nitrobenzene-d5 55.7 30-130 Surrogate:2-Fluorobiphenyl 74.8 30-130 Surrogate:7erphenyl-d]4 65.2 30-130 Matrix Spike(136B2506-MS1) Source:6020396-05 Prepared:2/25/2016 Analyzed:2/26/2016 Naphthalene 2880 320 4,248.562 ND 67.8 40-140 2-Methyl Naphthalene 3130 320 4,248.562 ND 73.8 40-140 Acenaphthylene 3010 320 4,248.562 ND 70.9 40-140 Acenaphthene 3120 320 4,248.562 ND 73.5 40-140 Fluorene 3160 320 4,248.562 ND 74.4 40-140 Phenanthrene 3110 320 4,248.562 ND 73.2 40-140 Anthracene 3250 320 4,248.562 ND 76.5 40-140 Fluoranthene 2820 320 4,248.562 ND 66.4 40-140 Pyrene 2870 320 4,248.562 ND 67.6 40-140 Benzo[a]anthracene 3110 320 4,248.562 ND 73.3 40-140 Chrysene 3060 320 4,248.562 ND 72.0 40-140 Benzo[b]fluoranthene 2870 320 4,248.562 ND 67.5 40-140 Benzo[k]fluoranthene 3700 320 4,248.562 ND 87.1 40-140 Benzo[a]pyrene 3360 320 4,248.562 ND 79.1 40-140 Indeno[1,2,3-cd]pyrene 3930 320 4,248.562 ND 92.4 40-140 Dibenz[a,h]anthracene 4320 320 4,248.562 ND 102 40-140 Benzo[g,h,i]perylene 3770 320 4,248.562 ND 88.8 40-140 Surrogate:Nitrobenzene-d5 63.1 30-130 Surrogate:2-Fluorobiphenyl 75.1 30-130 Surrogate:Terphenyl-d14 59.8 30-130 Matrix Spike Dup(B6B2506-MSD1) Source:6020396-05 Prepared:2/25/2016 Analyzed:2/26/2016 Naphthalene 2650 320 4,248.562 ND 62.5 40-140 8.18 30 2-Methyl Naphthalene 2870 320 4,248.562 ND 67.6 40-140 8.70 30 Acenaphthylene 2890 320 4,248.562 ND 68.0 40-140 4.10 30 Acenaphthene 2870 320 4,248.562 ND 67.5 40-140 8.62 30 Fluorene 2950 320 4,248.562 ND 69.6 40-140 6.74 30 Phenanthrene 3030 320 4,248.562 ND 71.2 40-140 2.73 30 Anthracene 3050 320 4,248.562 ND 71.7 40-140 6.54 30 Fluoranthene 2600 320 4,248.562 ND 61.2 40-140 8.07 30 Pyrene 2620 320 4,248.562 ND 61.6 40-140 9.25 30 Benzo[a]anthracene 2810 320 4,248.562 ND 66.1 40-140 10.2 30 Chrysene 2900 320 4,248.562 ND 68.4 40-140 5.24 30 Benzo[b]fluoranthene 2740 320 4,248.562 ND 64.5 40-140 4.51 30 Benzo[k]fluoranthene 3260 320 4,248.562 ND 76.8 40-140 12.5 30 Benzo[a)pyrene 3110 320 4,248.562 ND 73.2 40-140 7.75 30 Indeno[1,2,3-cd]pyrene 3550 320 4,248.562 ND 83.5 40-140 10.1 30 Dibenz[a,h]anthracene 4020 320 4,248.562 ND 94.6 40-140 7.28 30 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•wwryv.cetlabs.com Page 25 of 37 CET 4:6020396 Result RL Spike Source %Rec RPD Analyte (ug/kg dry) (ug/kg dry) Level Result %Rec Limits RPD Limit Notes Matrix Spike Dup(B6B2506-MSDI)-Continued Source:6020396-05 Prepared:2/25/2016 Analyzed:2/26/2016 Benzo[g,h,i]perylene 3450 320 4,248.562 ND 81.2 40-140 9.03 30 Surrogate:Nitrobenzene-d5 59.9 30-130 Surrogate:2-Fluorobiphenyl 71.3 30-130 Surrogate:Terpheny1414 54.0 30-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetiabs.com Page 26 of 37 CET 4:6020396 Batch B6B2514-EPA 8260C Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6132514-BLKI) Prepared:2/25/2016 Analyzed:2/25/2016 Dichlorodifluoromethane ND 7.5 Chloromethane ND 5.0 Vinyl Chloride ND 2.5 Bromomethane ND 5.0 Chloroethane ND 5.0 Trichlorofluoromethane ND 20 Acetone ND 75 Acrylonitrile ND 4.0 Trichlorotrifluoroethane ND 20 1,1-Dichloroethene ND 2.5 Methylene Chloride ND 25 Carbon Disulfide ND 5.0 Methyl-t-Butyl Ether(MTBE) ND 2.5 trans-1,2-Dichloroethene ND 2.5 I,1-Dichloroethane ND 2.5 2-Butanone(MEK) ND 13 2,2-Dichloropropane ND 2.5 cis-1,2-Dichloroethene ND 2.5 Chloroform ND 2.5 Tetrahydrofuran ND 13 1,1,1-Trichloroethane ND 2.5 Carbon Tetrachloride ND 2.5 1,1-Dichloropropene ND 2.5 Benzene ND 2.5 1,2-Dichloroethane ND 2.5 Trichloroethene ND 2.5 1,2-Dichloropropane ND 2.5 Dibromomethane ND 2.5 Bromodichloromethane ND 2.5 Methyl Isobutyl Ketone ND 13 cis-1,3-Dichloropropene ND 2.5 Toluene ND 2.5 trans-1,3-Dichloropropene ND 2.5 2-Hexanone ND 13 1,1,2-Trichloroethane ND 2.5 Tetrachloroethene ND 2.5 1,3-Dichloropropane ND 2.5 Dibromochloromethane ND 2.5 1,2-Dibromoethane ND 2.5 trans-l,4-Dichloro-2-Butene ND 13 Chlorobenzene ND 2.5 1,1,1,2-Tetrachloroethane ND 2.5 Ethylbenzene ND 2.5 m+p Xylenes ND 2.5 o-Xylene ND 2.5 Styrene ND 2.5 Bromoform ND 2.5 Isopropylbenzene ND 2.5 1,1,2,2-Tetrachloroethane ND 2.5 Bromobenzene ND 2.5 1,2,3-Trichloropropane ND 2.5 n-Propylbenzene ND 2.5 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 27 of 37 CET#:6020396 Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2514-BLK1)-Continued Prepared:2/25/2016 Analyzed:2/25/2016 2-Chlorotoluene ND 2.5 4-Chlorotoluene ND 2.5 1,3,5-Trimethylbenzene ND 2.5 tert-Butylbenzene ND 2.5 1,2,4-Trimethylbenzene ND 2.5 sec-B utyl benzene ND 2.5 1,3-Dichlorobenzene ND 2.5 4-Isopropyltoluene ND 2.5 1,4-Dichlorobenzene ND 2.5 1,2-Dichlorobenzene ND 2.5 n-Butylbenzene ND 2.5 1,2-Dibromo-3-Chloropropane ND 2.5 1,2,4-Trichlorobenzene ND 2.5 Hexachlorobutadiene ND 2.5 Naphthalene ND 2.5 1,2,3-Trichlorobenzene ND 2.5 Surrogate:1,2-Dichloroethane-d4 96.3 70-130 Surrogate:Toluene-& 91.1 70-130 Surrogate:4-Biomojluorohenaene 84.3 70-130 LCS(B6B2514-BSl) Prepared:2/25/2016 Analyzed:2/25/2016 Dichlorodifluoromethane 70.0 7.5 50.000 140 70-130 H Chloromethane 85.3 5.0 50.000 171 70-130 H Vinyl Chloride 85.8 2.5 50.000 172 70-130 H Bromomethane 91.9 5.0 50.000 184 70-130 H Chloroethane 60.0 5.0 50.000 120 70-130 Trichlorofluoromethane 54.8 20 50.000 110 70-130 Acetone 97.4 75 100.000 97.4 70-130 Acrylonitrile 49.0 4.0 50.000 98.0 70-130 Trichlorotrifluoroethane 41.0 20 50.000 81.9 70-130 1,1-Dichloroethene 37.2 2.5 50.000 74.3 70-130 Methylene Chloride 42.3 25 50.000 84.6 70-130 Carbon Disulfide 37.6 5.0 50.000 75.2 70-130 Methyl-t-Butyl Ether(MTBE) 44.0 2.5 50.000 88.1 70-130 trans-l,2-Dichloroethene 42.5 2.5 50.000 84.9 70-130 1,1-Dichloroethane 51.7 2.5 50.000 103 70-130 2-Butanone(MEK) 102 13 100.000 102 70-130 2,2-Dichloropropane 54.4 2.5 50.000 109 70-130 cis-1,2-Dichloroethene 55.2 2.5 50.000 110 70-130 Chloroform 50.4 2.5 50.000 101 70-130 Tetrahydrofuran 47.6 13 50.000 95.2 70-130 1,1,1-Trichloroethane 53.9 2.5 50.000 108 70-130 Carbon Tetrachloride 47.0 2.5 50.000 93.9 70-130 1,1-Dichloropropene 48.1 2.5 50.000 96.2 70-130 Benzene 51.3 2.5 50.000 103 70-130 1,2-Dichloroethane 53.5 2.5 50.000 107 70-130 Trichloroethene 46.1 2.5 50.000 92.2 70-130 1,2-Dichloropropane 52.9 2.5 50.000 106 70-130 Dibromomethane 50.3 2.5 50.000 101 70-130 Bromodichloromethane 52.5 2.5 50.000 105 70-130 Methyl Isobutyl Ketone 111 13 100.000 111 70-130 cis-1,3-Dichloropropene 51.3 2.5 50.000 103 70-130 Toluene 48.1 2.5 50.000 96.2 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•wHtiv.cetlabs.com Page 28 of 37 CET#:6020396 Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes LCS(B6B2514-BSI)-Continued Prepared:2/25/2016 Analyzed:2/25/2016 trans-1,3-Dichloropropene 55.4 2.5 50.000 111 70-130 2-Hexanone 120 13 100.000 120 70-130 1,1,2-Trichloroethane 53.0 2.5 50.000 106 70-130 Tetrachloroethene 48.1 2.5 50.000 96.2 70-130 1,3-Dichloropropane 52.1 2.5 50.000 104 70-130 Dibromochloromethane 56.9 2.5 50,000 114 70-130 1,2-Dibromoethane 57.3 2.5 50.000 115 70-130 trans-1,4-Dichloro-2-Butene 57.1 13 50A00 114 70-130 Chlorobenzene 56.6 2.5 50.000 113 70-130 1,1,1,2-Tetrachloroethane 56.9 2.5 50.000 114 70-130 Ethylbenzene 55.0 2.5 50.000 110 70-130 m+p Xylenes 118 2.5 100.000 118 70-130 o-Xylene 53.0 2.5 50.000 106 70-130 Styrene 57.0 2.5 50.000 114 70-130 Bromoform 51.9 2.5 50.000 104 70-130 Isopropylbenzene 56.7 2.5 50.000 113 70-130 1,1,2,2-Tetrachloroethane 57.8 2.5 50.000 116 70-130 Bromobenzene 62.0 2.5 50.000 124 70-130 1,2,3-Trichloropropane 59.0 2.5 50.000 118 70-130 n-Propylbenzene 63.0 2.5 50.000 126 70-130 2-Chlorotoluene 54.3 2.5 50.000 109 70-130 4-Chlorotoluene 56.0 2.5 50.000 112 70-130 1,3,5-Trimethylbenzene 54.5 2.5 50.000 109 70-130 ten-Butyl benzene 50.9 2.5 50.000 102 70-130 1,2,4-Trimethylbenzene 55.9 2.5 50.000 112 70-130 sec-Butylbenzene 56.2 2.5 50.000 112 70-130 1,3-Dichlorobenzene 59.8 2.5 50.000 120 70-130 4-Isopropyltoluene 58.6 2.5 50.000 117 70-130 1,4-Dichlorobenzene 60.6 2.5 50.000 121 70-130 1,2-Dichlorobenzene 66.3 2.5 50.000 133 70-130 H n-Butylbenzene 63.7 2.5 50.000 127 70-130 1,2-Dibromo-3-Chloropropane 54.4 2.5 50.000 109 70-130 1,2,4-Trichlorobenzene 60.4 2.5 50.000 121 70-130 Hexachlorobutadiene 49.8 2.5 50.000 99.6 70-130 Naphthalene 55.6 2.5 50.000 111 70-130 1,2,3-Trichlorobenzene 60.8 2.5 50.000 122 70-130 Surrogate:1.2-Dichloroethane-d 1 102 70-130 Surrogate:Toluene-& 97.8 70-130 Surrogate:4-Bromo luorobenzene 102 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Pax:203-377-9952•wHtiv.cetlabs.com Page 29 of 37 CET 4:6020396 Questions related to this report should be directed to David Ditta,Timothy Fusco,or Robert Blake at 203-377-9984. Sincerely, t David Ditta Laboratory Director Report Comments: Sample Result Flags: E-The result is estimated,above the calibration range. H-The surrogate recovery is above the control limits. L-The surrogate recovery is below the control limits. B-The compound was detected in the laboratory blank. P-The Relative Percent Difference(RPD)of dual column analyses exceeds 40%. D-The RPD between the sample and the sample duplicate is high. Sample Homogenity may be a problem. +- The Surrogate was diluted out. *Cl-The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2-The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F 1-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I-The Analyte exceeds%RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result,or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 30 of 37 CET#:6020396 80 Lupes Drive Tel:(203)377-9984 Stratford,CT 06615 CI PIIII INVIRJNMINIAt 1'MING,IKI Fax:(203)377-9952 email:cetl@cetlabs.com Quality Control Definitions and Abbreviations Internal Standard(IS) An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time,calculate relative response,and quantify analytes of interest. Surrogate Recovery The%recovery for non-tarer organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method,sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels(MDL)and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte foun in duplicate spikes including amount that was spike. Matrix Spike%Recovery %Recovery of spiked amount in sample. Matrix Spike Dup%Recovery %Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS%Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H- Recovery is above the control limits L- Recovery is below the control limits B- Compound detected in the Blank P- RPD of dual column results exceeds 40% #- Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 31 of 37 _ REASONABLE CONFIDENCE PROTOCOL ` - LABORATORY ANALYSIS QA/QC CERTIFICATION FORM Laboratory Name: Complete Environmental Testing,Inc. Client: Enviroshield,Inc. Project Location: Tank Pull Project Number: Laboratory Sample ID(s): Sample Date(s): 6020396-01thru 6020396-06 02/17/2016 List RCP Methods Used: CET#: 6020396 CT-E7PH,EPA 8260C,EPA 8270D 1 For each analytical method referenced in this laboratory report package,were all specified QA/QC ❑✓Yes ❑ No performance criteria followed,including the requirement to explain any criteria falling outside of acceptable guidelines,as specified in the CTDEP method-specific Reasonable Confidence Protocol documents? 1A Were the method specified preservation and holding time requirements met? Yes ❑ No 1 B VPH and EPH Methods only: Was the VPH and EPH method conducted without significant ❑Yes ❑ No modifications(see Section 11.3 of respective RCP methods)? ❑✓ N/A 2 Were all samples received by the laboratory in a condition consistent with that described on the 0 Yes ❑ No associated chain-of-custody document(s)? 3 Were samples received at an appropriate temperature(<G degrees C.)? ❑✓Yes ❑ No ❑ N/A 4 Were all QA/QC performance criteria specified in the CT DEP Reasonable Confidence Protocol ❑Yes ❑✓ No documents achieved? 5a a)Were reporting limits specified or referenced on the chain-of-custody? ❑Yes ❑✓ No 5b b)Were these reporting limits met? ❑Yes ❑ No 6 For each analytical method referenced in this laboratory report package,were results reported for ❑Yes ❑✓ No all consituents identified in the method-specific analyte lists presented in the Reasonable Confidence Protocol documents? 7 Are project specific matrix spikes and laboratory duplicates included with this data set? 0 Yes ❑ No Notes:For all questions to which the response was"No"(with the exception of question 47),additional information must be provided in an attached narrative.If the answer to question 41,#1 A,or#I B is"No",the data package does not meet the requirements for'Reasonable Confidence." This form may not be altered and all questions must be answered. 1,the undersigned,attest under the pains and penalties of perjury that,to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report,such information is accurate and complete. Authorized Signature: Position:Laboratory Director Printed Name:David Ditta Date: 02/26/2016 Name of Laboratory:Complete Environmental Testing,Inc. This certification form is to be used for RCP methods only. CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 32 of 37 RCP Case Narrative 4-See Exceptions Report Below 6-The client requested a subset of the CT8270 List. 4-Exceptions Report Recovery Batch/Sequence Analyte QC Type Exception Result RPD (%) Sample ID 1,2-Dichlorobenzene LCS High 133 B6B2514 Bromomethane LCS High 184 B6132514 Chloromethane LCS High 171 B6132514 Dichlorodifluoromethane LCS High 140 B6B2514 Vinyl Chloride LCS High 172 B6B2514 1,2-Dichlorobenzene CC High 72.7 145 S6B2602 1,3,5-Trimethylbenzene CC High 68.0 136 S6B2602 1,3-Dichlorobenzene CC High 68.6 137 S6B2602 2-Chlorotoluene CC High 69.3 139 S6B2602 4-Chlorotoluene CC High 70.0 140 S6132602 Bromomethane CC High 71.5 143 S6B2602 Chloromethane CC High 68.1 136 S6B2602 n-Butylbenzene CC High 67.1 134 S6B2602 Styrene CC High 66.3 133 S6B2602 Vinyl Chloride CC High 65.0 130 S6B2602 CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 33 of 37 QC Batch/Sequence Report Batch Sequence CET ID Sample ID Specific Method Matrix Collection Date B6B2338 6020396-01 Diesel North CT-ETPH Soil 02/17/2016 B6B2338 6020396-02 Diesel East CT-ETPH Soil 02/17/2016 B6B2338 6020396-03 Diesel West CT-ETPH Soil 02/17/2016 B6B2338 6020396-04 Diesel Bottom CT-ETPH Soil 02/17/2016 B6B2339 6020396-05 Diesel Dispenser CT-ETPH Soil 02/17/2016 B6B2339 6020396-06 Diesel Lines CT-ETPH Soil 02/17/2016 B6B2514 S6B2602 6020396-01 Diesel North EPA 8260C Soil 02/17/2016 B6B2514 S6B2602 6020396-02 Diesel East EPA 8260C Soil 02/17/2016 B6B2514 S6B2602 6020396-03 Diesel West EPA 8260C Soil 02/17/2016 B6B2514 S6B2602 6020396-04 Diesel Bottom EPA 8260C Soil 02/17/2016 B6B2514 S6B2602 6020396-05 Diesel Dispenser EPA 8260C Soil 02/17/2016 B6B2514 S6B2602 6020396-06 Diesel Lines EPA 8260C Soil 02/17/2016 B6B2308 S6B2604 6020396-06 Diesel Lines EPA 8270D Soil 02/17/2016 B6B2506 S6B2604 6020396-01 Diesel North EPA 8270D Soil 02/17/2016 B6B2506 S6B2604 6020396-02 Diesel East EPA 8270D Soil 02/17/2016 B6B2506 S6B2604 6020396-03 Diesel West EPA 8270D Soil 02/17/2016 B6B2506 S6B2604 6020396-04 Diesel Bottom EPA 8270D Soil 02/17/2016 B6B2506 S6B2605 6020396-05 Diesel Dispenser EPA 8270D Soil 02/17/2016 CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 34 of 37 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications CT-ETPAin Soil ETPH CT EPA 8260C in Sail Dichlorodifluoromethane CTNY Chloromethane CTNY Vinyl Chloride CTNY Bromonrethane CTNY Chloroethane CTNY Trichlorofluoromethane CTNY Acetone CTNY Acrylonitrile CTNY Trichlorottifluoroethaue CTNY I,1-Dichloroethene CTNY Methylene Chloride CTNY Carbon Disulfide CTNY Methyl-t-Butyl Ether(MTBE) CTNY trans-1,2-Dichloroethene CTNY I,I-Dichloroethene CTNY 2-Butanone(MEK) CTNY 2,2-Dichloropropene CTNY cis-1,2-Dichloroethene CTNY Chloroform CTNY Tetrahydrofuran CT 1,1,1-Trichloroethane CTNY Carbon Tetrachloride CTNY l,1-Dichloropropene CTNY Benzene CTNY 1,2-Dichloroethane CTNY Trichloroethene CTNY 1,2-Dichloropropane CTNY Dibromomethane CTNY Bromodichloromethane CTNY Methyl Isobutyl Ketone CTNY cis-1,3-Dichloropropene CTNY Toluene CTNY trans-1,3-Dichloropropene CTNY 2-Heaanoue CTNY 1,1,2-Trichloroetlrane CTNY Tetrachloroethene CTNY 1,3-Dichloropropane CTNY Dibromochloromethane CTNY 1,2-Dibrontoethane CTNY trans-1,4-Dichloro-2-Bmtene CTNY Chlorobenzene CTNY 1,1,1,2-Tetrachloroethane CTNY Ethylbenzene CTNY m+p Xylenes CTNY o-Xylene CTNY Styrene CT,NY Bromofonu CTNY Page 35 of 37 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA 8260C in Soil Isopropylbenzene CTNY 1,1,2,2-Tetrachloroethane CTNY Bromobenzene CTNY 1,2,3-Trichloropropane CTNY n-Propylbenzene CTNY 2-Chlorotoluene CTNY 4-Chlorotoluene CTNY 1,3,5-Trimethylbenzene CTNY tert-Butylbenzene CTNY 1,2,4-Trimethylbenzene CTNY sec-Butylbenzene CTNY 1,3-Dichlorobenzene CTNY 4-Isopropyltoluene CTNY 1,4-Dichlorobenzene CTNY 1,2-Dichlorobenzene CTNY n-Butylbenzene CTNY 1,2-Dibromo-3-Chloropropane CTNY 1,2,4-Trichlorobenzeue CTNY Hexachlorobutadiene CTNY Naphthalene CTNY 1,2,3-Trichlorobenzene CT EPA 8270D in Soi! Naphthalene CTNY 2-Methyl Naphthalene CTNY Acenaphthylene CTNY Acenaphthene CTNY Fluorene CTNY Phenanthrene CTNY Anthracene CTNY Fluoranthene CTNY Pyrene CTNY Benzo[a]anthracene CTNY Chrysene CTNY Benzo[61fluoranthene CTNY Benzo[k]fluorandiene CTNY Benzo[a]pyrene CTNY indeno[1,2,3-cd]pyrene CTNY Dibenz[a,hjanthracene CTNY Benzo[g,h,i]perylene CTNY Complete Environmental Testing operates under die following certifications and accreditations: Code Description Number Expires CT Connecticut Public Health PHO116 09/30/2016 NY New York Certification(NELAC) 11982 04/01/2016 Page 36 of 37 M EN ,IROO!t�SHIEL 6020396 0 HVC. M N cu NVIROSHIELD, INC. PRIORITY LEVEL: (.} MOFFITT STREET .0. BOX 1296 -11-RATFORD, CT 06615 CHAIN OF CUSTODY „OJECT NAME:`� t t C PROJECTT LOCATION: i �^ 1 PURC/H/ASE[ORDER COO CAA S , �,j A 0� S 1 L Y J�l� �tJ Y1 1� T c�� � � l V�� 4 J� LJ 1 n S C: �✓! � tr7 ICJ J )URCE CODES: W=WELL, O=OUTFALL WO=WASTE OIL RO=RUN OFF B=BOTTOM SEDIMENT SW=SEWAGE SG=SLUDGE S=SOIL R=RIVER/STREAM LF=LANDFILL W W=WASTE WATER L=LAKE/OCEAN _ _ X=OTHER;SPECIFY .1 I SAMPLE SOURCE CONT, CONT. CONT. CONT. ANALYSIS REQUESTED 1 DATE TIME COMMENTS/"RCP"Required? `_-__ l.D• CODE NO. TYPE SIZE PRES. I 1 3 �!i btu`.` �N(v � P� $�'"70 �cZ�+C-7 2���/1� ; �3 _ -e 5-2 atk �,j,,• / �,r+ r, « �• ," -e_sci I "1'\11vF?P.CODES: P=PLASTIC L-'-'=EPA VIAL G=GLASS A=AMBER GLASS B=BACTERIA BOTTLE [iSLiI:VA'1'IVE CODES: I=ICED I1=HYDROCHLORIC ACID(HCI) S=SODIUM HYROXIDE(NaOH) Na=SODIUM BISULFATE(NaHSO4) M=METHANOL(NkH) O=OTHER;SPECIFY ��91 i,.ER'S S1GNr\T L AFFILIATION DATE. TRNSF ITEM TRANSFERS �!(p NO. NO. RELINQUISHED BY ACCEPTED BY DATE TIME \i)1:>I'I'10NAl..COMMI:NTS: �. ILI Data on server/templates/forms/chain of custody (revised July 2014) 80 Lupes Drive Tel:(203)377-9984 Stratford,CT 06615 Fax:(203)377-9952 (VET e-mail:cetl@cetlabs.com GGIVIRUf fNVIRON1 t I.If STING,INII Client: Mr.Tim Farrelly Enviroshield,Inc. P.O.Box 1296 Stratford,CT 06615 Analytical Report CET# 6020397 Report Date:February 29,2016 Project: County Distributors, 1510 John Fitch Blvd, PO Number: 26648 Connecticut Laboratory Certificate:PH 0116 New York Certification: 11982 Massachusetts laboratory Certificate:M-CT903 Rhode Island Certification: 199 Page 1 of 37 CET#:6020397 SAMPLE SUMMARY The sample(s)were received at 2.9°C. This report contains analytical data associated with following samples only. Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date Gas South 6020397-01 Soil 2/18/2016 13:00 02/22/2016 Gas East 6020397-02 Soil 2/18/2016 13:00 02/22/2016 Gas West 6020397-03 Soil 2/18/2016 13:00 02/22/2016 Gas Bottom 6020397-04 Soil 2/18/2016 13:00 02/22/2016 Gas Dispenser 6020397-05 Soil 2/18/2016 13:00 02/22/2016 Gas Lines 6020397-06 Soil 2/18/2016 13:00 02/22/2016 Analyte:Total Solids [EPA 160.3 modified] Analyst:JM Matrix: Soil Date/Time Laboratory ID Client Sample ID Result RL Units Dilution Batch Prepared Analyzed Notes 6020397-01 Gas South 80 1.0 % 1 B6B2331 02/23/2016 02/24/2016 00:00 6020397-02 Gas East 86 1.0 % 1 136132331 02/23/2016 02/24/2016 00:00 6020397-03 Gas West 86 1.0 % I B6132331 02/23/2016 02/24/2016 00:00 6020397-04 Gas Bottom 87 1.0 % 1 B6B2331 02/23/2016 02/24/2016 00:00 6020397-05 Gas Dispenser 96 1.0 % 1 136132331 02/23/2016 02/24/2016 00:00 6020397-06 Gas Lines 94 1.0 % 1 B6B2331 02/23/2016 02/24/2016 00:00 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetiabs.com Page 2 of 37 CET#:6020397 Client Sample ID Gas South Lab ID: 6020397-01 Volatile Organics Analyst:TWF Method:EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Di-isopropyl ether ND 13 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 t-Butanol ND 53 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 t-Butyl ethyl ether ND 13 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 tert-Amyl methyl ether(TAME) ND 13 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Surrogate:1,2-Dichloroethane-d4 107% 70-130 B6132514 02/25/2016 021251201617:24 Surrogate:Toluene-d8 94.8% 70-130 136B2514 02/25/2016 021251201617:24 Surrogate:4-BromoJluorobenzene 84.1% 70-130 B6B2514 02/25/2016 021251201617:24 Volatile Organics Analyst:TWF Method:EPA 8260C Matrix:Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 20 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 *F2 Chloromethane ND 13 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 *F2*C2 Vinyl Chloride ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 *F2*C2 Bromomethane ND 13 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 *F2*C2 Chloroethane ND 13 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Trichlorofluoromethane ND 53 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Acetone ND 200 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 Acrylonitrile ND 11 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 Trichlorotrifluoroethane ND 53 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 ],I-Dichloroethene ND 6.6 2.11 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:24 Methylene Chloride ND 66 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 Carbon Disulfide ND 13 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 Methyl-t-Butyl Ether(MTBE) ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 trans-1,2-Dichloroethene ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 I,I-Dichloroethane ND 6.6 2.11 EPA5035A-L 136B2514 02/25/2016 02/25/2016 17:24 2-Butanone(MEK) ND 33 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 2,2-Dichloropropane ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 cis-1,2-Dichloroethene ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 Chloroform ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Tctrahydrofuran ND 33 2.11 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:24 1,1,1-Trichloroethanc ND 6.6 2.11 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 3 of 37 CET#:6020397 Client Sample ID Gas South Lab ID: 6020397-01 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix:Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Carbon Tetrachloride ND 6.6 2.11 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:24 1,1-Dichloropropene ND 6.6 2.11 EPA5035A-L B6132514 02/25/2016 02/25/2016 17:24 Benzene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 1,2-Dichloroethane ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 Trichloroethene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 1,2-Dichloropropane ND 6.6 2.11 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:24 Dibromomethane ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Bromodichloromethane ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 Methyl Isobutyl Ketone ND 33 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 cis-1,3-Dichloropropene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 Toluene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 trans-1,3-Dichloropropene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 2-Hexanone ND 33 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 1,1,2-Trichloroethane ND 6.6 2.11 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:24 Tetrachloroethene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 1,3-Dichloropropane ND 6.6 2.11 EPA5035A-L 136B2514 02/25/2016 02/25/2016 17:24 Dibromochloromethane ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 1,2-Dibromoethane ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 trans-1,4-Dichloro-2-Butene ND 33 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 Chlorobenzene ND 6.6 2.11 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:24 1,1,1,2-Tetrachloroethane ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Ethylbenzene ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 m+p Xylenes ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 o-Xylene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 Styrene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 *C2 Bromoform ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Isopropylbenzene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 1,1,2,2-Tetrachloroethane ND 6.6 2.11 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:24 Bromobenzene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 1,2,3-Trichloropropane ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 n-Propylbenzene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 2-Chlorotoluene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 *C2 4-Chlorotoluene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 *C2 1,3,5-Trimethylbenzene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 *C2 tert-Butylbenzene ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 1,2,4-Trimethylbenzene ND 6.6 2.11 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:24 sec-Butylbenzene ND 6.6 2.11 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:24 1,3-Dichorobenzene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 *C2 4-Isopropyltoluene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 1,4-Dichlorobenzene ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 1,2-Dichlorobenzene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 I7:24 *F2*C2 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 4 0f 37 CET#:6020397 Client Sample ID Gas South Lab ID: 6020397-01 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes n-Butylbenzene ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 *C2 1,2-Dibromo-3-Chloropropane ND 6.6 2.11 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:24 1,2,4-Trichlorobenzene ND 6.6 2.11 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:24 Hexachlorobutadiene ND 6.6 2.11 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:24 Naphthalene ND 6.6 2.11 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:24 1,2,3-Trichlorobenzene ND 6.6 2.11 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:24 Surrogate:1,2-Dichloroethane-d4 107% 70-130 136132514 02/25/2016 021251201617:24 Surrogate:Toluene-d8 94.8% 70-130 B6B2514 02/25/2016 021251201617:24 Surrogate:4-Bromofluorohenzene 84.1% 70-130 B6B2514 02/25/2016 021251201617:24 Complete Environmental Testing,Inc. 80 Lupcs Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectiabs.com Page 5 of 37 CET#:6020397 Client Sample ID Gas East Lab ID:6020397-02 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Di-isopropyl ether ND 12 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 t-Butanol ND 48 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 t-Butyl ethyl ether ND 12 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 tert-Amy]methyl ether(TAME) ND 12 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 Surrogate:1,2-Dichloroethane-d4 115% 70-130 136132514 02/25/2016 021251201617:47 Surrogate:Toluene-d8 98.1% 70-130 136132514 02/25/2016 021251201617:47 Surrogate:4-Bromofluorobenzene 96.2% 70-130 B6B2514 02/25/2016 021251201617:47 Volatile Organics Analyst:TWF Method:EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 18 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 *F2 Chloromethane ND 12 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 *F2*C2 Vinyl Chloride ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 *F2*C2 Bromomethane ND 12 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 *F2*C2 Chloroethane ND 12 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 Trichlorofluoromethane ND 48 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 Acetone ND 180 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 Acrylonitrile ND 9.5 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 Trichlorotrifluoroethane ND 48 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 1,1-Dichloroethene ND 5.9 2.04 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:47 Methylene Chloride ND 59 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 Carbon Disulfide ND 12 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 Methyl-t-Butyl Ether(MTBE) ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 trans-1,2-Dichloroethene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 1,1-Dichloroethane ND 5.9 2.04 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:47 2-Butanonc(MEK) ND 30 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 2,2-Dichloropropane ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 cis-1,2-Dichloroethene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 Chloroform ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 Tetrahydrofuran ND 30 2.04 EPA 5035A-L 136132514 . 02/25/2016 02/25/2016 17:47 1,1,1-Trichloroethane ND 5.9 2.04 EPA5035A-L 136B2514 02/25/2016 02/25/2016 17:47 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 6 of 37 CET#:6020397 Client Sample ID Gas East Lab ID: 6020397-02 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Carbon Tetrachloride ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 I,1-Dichloropropene ND 5.9 2.04 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:47 Benzene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 1,2-Dichloroethane ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 Trichloroethene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 1,2-Dichloropropane ND 5.9 2.04 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:47 Dibromomethane ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 Bromodichloromethane ND 5.9 2.04 EPA 5035A-L 136112514 02/25/2016 02/25/2016 17:47 Methyl Isobutyl Ketone ND 30 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 cis-1,3-Dichloropropene ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 Toluene ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 trans-1,3-Dichloropropene ND 5.9 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 2-Hexanone ND 30 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 1,1,2-Trichloroethane ND 5.9 2.04 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:47 Tetrachloroethene ND 5.9 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 1,3-Dichloropropane ND 5.9 2.04 EPA5035A-L B6132514 02/25/2016 02/25/2016 17:47 Dibromochloromethane ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 1,2-Dibromoethane ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 trans-1,4-Dichloro-2-Butene ND 30 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 Chlorobenzene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 1,1,1,2-Tetrachloroethane ND 5.9 2.04 EPA5035A-L 136132514 02/25/2016 02/25/2016 17:47 Etylbenzene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 m+p Xylenes ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 o-Xylene ND 5.9 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 Styrene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 *C2 Bromoform ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 Isopropylbenzene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 1,1,2,2-Tetrachloroethane ND 5.9 2.04 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:47 Bromobenzene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 1,2,3-Trichloropropane ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 n-Propylbenzene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 2-Chlorotoluene ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 *C2 4-Chlorotoluene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 *C2 1,3,5-Trimethylbenzene ND 5.9 2.04 EPA5035A-L B6B2514 02/25/2016 02/25/2016 17:47 *C2 tert-Butylbenzene ND 5.9 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 1,2,4-Trimcthylbenzene ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 sec-Butylbenzene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 1,3-Dichlorobenzene ND 5.9 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 *C2 4-Isopropyltoluene ND 5.9 2.04 EPA 5035A-L B6132514 02/25/2016 02/25/2016 17:47 1,4-Dichlorobenzene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 1,2-Dichlorobenzene ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 *F2*C2 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 7 of 37 CET#:6020397 Client Sample ID Gas East Lab ID: 6020397-02 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes n-Butylbenzene ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 *C2 1,2-Dibromo-3-Chloropropane ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 1,2,4-Trichlorobenzene ND 5.9 2.04 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 17:47 Hexachlorobutadiene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 Naphthalene ND 5.9 2.04 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 17:47 1,2,3-Trichlorobenzene ND 5.9 2.04 EPA 5035A-L 136132514 02/25/2016 02/25/2016 17:47 Surrogate:1,2-Dichloroethane-d4 115% 70-130 136132514 02/25/2016 021251201617:47 Surrogate:Toluene-d8 98.1% 70-130 B6B2514 02/25/2016 021251201617:47 Surrogate:4-Bromofluorohenzene 96.2% 70-130 B6132514 02/25/2016 021251201617:47 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 8 of 37 CET#:6020397 Client Sample ID Gas West Lab ID: 6020397-03 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Di-isopropyl ether ND 12 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 t-Butanol ND 47 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 t-Butyl ethyl ether ND 12 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 tert-Amyl methyl ether(TAME) ND 12 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 Surrogate:I,2-Dichloroethane-d4 119% 70-130 136B2514 02/25/2016 021251201618:11 Surrogate:Toluene-d8 93.8% 70-130 B6B2514 02/25/2016 021251201618:11 Surrogate:4-Bromofluorobenzene 94.0% 70-130 136B2514 02/25/2016 021251201618:11 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 18 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 *F2 Chloromethane ND 12 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 *F2*C2 Vinyl Chloride ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 *F2*C2 Bromomethane ND 12 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 *F2*C2 Chloroethane ND 12 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 Trichlorofluoromethane ND 47 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 Acetone ND 180 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 Acrylonitrile ND 9.4 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 Trichlorotrifluoroethane ND 47 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 1,1-Dichlorocthenc ND 5.9 2.02 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:11 Methylene Chloride ND 59 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 Carbon Disulfide ND 12 2.02 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:11 Methyl-t-Butyl Ether(MTBE) ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 trans-1,2-Dichlorocthenc ND 5.9 2.02 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:11 ],I-Dichloroethane ND 5.9 2.02 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:11 2-Butanonc(MEK) ND 29 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 2,2-Dichloropropane ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 cis-1,2-Dichloroethene ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 Chloroform ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 Tetrahydrofuran ND 29 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 1,1,1-Trichloroethane ND 5.9 2.02 EPA5035A-L B6132514 02/25/2016 02/25/2016 18:11 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 9 of 37 CET#:6020397 Client Sample ID Gas West Lab ID:6020397-03 Volatile Organics Analyst:TWF Method:EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Carbon Tetrachloride ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 1,1-Dichloropropene ND 5.9 2.02 EPA5035A-L 136B2514 02/25/2016 02/25/2016 18:11 Benzene ND 5.9 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 1,2-Dichloroethane ND 5.9 2.02 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:11 Trichloroethene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 1,2-Dichloropropane ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 Dibromomethane ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 Bromodichloromethane ND 5.9 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 Methyl Isobutyl Ketone ND 29 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 cis-1,3-Dichloropropene ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 Toluene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 trans-1,3-Dichloropropene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 2-Hexanone ND 29 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 1,1,2-Trichloroethane ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 Tetrachloroethene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 1,3-Dichloropropane ND 5.9 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 Dibromochloromethane ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 1,2-Dibromoethane ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 trans-1,4-Dichloro-2-Butene ND 29 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 Chlorobenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 11111,2-Tetrachloroethane ND 5.9 2.02 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:11 Ethylbenzene ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 m+p Xylenes ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 o-Xylene ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 Styrene ND 5.9 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 *C2 Bromoform ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 Isopropylbenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 1,1,2,2-Tetrachloroethane ND 5.9 2.02 EPA5035A-L 136B2514 02/25/2016 02/25/2016 18:11 Bromobenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 1,2,3-Trichloropropane ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 n-Propylbenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 2-Chlorotoluenc ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 *C2 4-Chlorotoluene ND 5.9 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 *C2 1,3,5-Trimethylbenzene ND 5.9 2.02 EPA 5035A-L B6112514 02/25/2016 02/25/2016 18:11 *C2 tert-Butylbenzene ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 1,2,4-Trimethylbenzene ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 sec-Butylbenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 1,3-Dichlorobenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 *C2 4-Isopropyltoluene ND 5.9 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 1,4-Dichlorobenzene ND 5.9 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:11 1,2-Dichlorobenzene ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 *F2*C2 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 15 of 37 CET#:6020397 Client Sample ID Gas West Lab ID: 6020397-03 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes n-Butylbenzene ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 *C2 1,2-Dibromo-3-Chloropropane ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 1,2,4-Trichlorobenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 Hexachlorobutadiene ND 5.9 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:11 Naphthalene ND 5.9 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:11 1,2,3-Trichlorobenzene ND 5.9 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:11 Surrogate:1,2-Dichloroethane-d4 119% 70-130 B6132514 02/25/2016 021251201618:11 Surrogate:Toluene-d8 93.8% 70-130 B6B2514 02/25/2016 021251201618:11 Surrogate:4-BromoJluorobenzene 94.0% 70-130 B6B2514 02/25/2016 021251201618:11 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectiabs.com page 1177371 CET#:6020397 Client Sample ID Gas Bottom Lab ID:6020397-04 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Di-isopropyl ether ND 12 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 t-Butanol ND 47 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 t-Butyl ethyl ether ND 12 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 tert-Amyl methyl ether(TAME) ND 12 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 Surrogate:1,2-Dichloroethane-d4 108% 70-130 136B2514 02/25/2016 021251201618:34 Surrogate:Toluene-d8 93.7% 70-130 B6B2514 02/25/2016 021251201618:34 Surrogate:4-Bromofluorobenzene 93.7% 70-130 B6B2514 02/25/2016 021251201618:34 Volatile Organics Analyst:TWIT Method:EPA 8260C Matrix: Soil Result RL Date/Time Analyt: (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 17 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 *F2 Chloromethanc ND 12 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 *F2*C2 Vinyl Chloride ND 5.8 2.02 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:34 *F2*C2 Bromomethane ND 12 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 *F2*C2 Chloroethane ND 12 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 Trichlorofluoromethane ND 47 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 Acetone ND 170 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Acrylonitrile ND 9.3 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Trichlorotrifluoroethane ND 47 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 1,1-Dichloroethcne ND 5.8 2.02 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:34 Methylene Chloride ND 58 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 Carbon Disulfide ND 12 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 Methyl-t-Butyl Ether(MTBE) ND 5.8 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 trans-1,2-Dichloroethcne ND 5.8 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 1,1-Dichlorocthane ND 5.8 2.02 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:34 2-Butanone(MEK) ND 29 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 2,2-Dichloropropane ND 5.8 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 cis-1,2-Dichloroethcne ND 5.8 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 Chloroform ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Tetrahydrofuran ND 29 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 l,t,l-Trichlorocthanc ND 5.8 2.02 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetiabs.com Page 12 of 37 CET#:6020397 Client Sample ID Gas Bottom Lab ID: 6020397-04 Volatile Organics Analyst: TWF Method:EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Carbon Tetrachloride ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 1,1-Dichloropropene ND 5.8 2.02 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Benzene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 1,2-Dichloroethane ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 Trichloroethene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 1,2-Dichloropropane ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 Dibromomethane ND 5.8 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 Bromodichloromethane ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Methyl Isobutyl Ketone ND 29 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 cis-1,3-Dichloropropene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 Toluene ND 5.8 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 trans-1,3-Dichloropropene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 2-Hexanone ND 29 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 1,1,2-Trichloroethane ND 5.8 2.02 EPA5035A-L B6132514 02/25/2016 02/25/2016 18:34 Tetrachloroethene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 1,3-Dichloropropane ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Dibromochloromethane ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 1,2-Dibromoethane ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 trans-1,4-Dichloro-2-Butene ND 29 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Chlorobenzene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 1,1,1,2-Tetrachloroethane ND 5.8 2.02 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Ethylbenzene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 m+p Xylenes ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 o-Xylene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Styrene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 *C2 Bromoform ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 Isopropylbenzene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 1,1,2,2-Tetrachloroethane ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Bromobenzene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 1,2,3-Trichloropropane ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 n-Propylbenzene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 2-Chlorotoluene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 *C2 4-Chlorotoluene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 *C2 1,3,5-Trimethylbenzene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 *C2 tert-Butylbenzene ND 5.8 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 1,2,4-Trimethylbenzene ND 5.8 2.02 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:34 sec-Butylbenzene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 1,3-Dichlorobenzcne ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 *C2 4-Isopropyholuene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 1,4-Dichlorobenzcne ND 5.8 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 1,2-Dichiorobcnzene ND 5.8 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 *F2*C2 Complete Environmental Testing,Inc. 80 Lupcs Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetiabs.com Page 13 of 37 CET##:6020397 Client Sample ID Gas Bottom Lab ID: 6020397-04 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes n-Butylbenzene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 *C2 1,2-Dibromo-3-Chloropropane ND 5.8 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 1,2,4-Trichlorobenzene ND 5.8 2.02 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:34 Hexachlorobutadiene ND 5.8 2.02 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:34 Naphthalene ND 5.8 2.02 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:34 1,2,3-Trichlorobenzene ND 5.8 2.02 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:34 Surrogate:1,2-Dichloroethane-d4 108% 70-130 136B2514 02/25/2016 021251201618:34 Surrogate:Toluene-d8 93.7% 70-130 B6B2514 02/25/2016 021251201618:34 Surrogate:4-Bromofluorobenzene 93.7% 70-130 B6B2514 02/25/2016 021251201618:34 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 14 of 37 CET#:6020397 Client Sample ID Gas Dispenser Lab ID: 6020397-05 Volatile Organics Analyst: TWF Method: EPA 8260C Matrix: Soil Result RL Datc/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Di-isopropyl ether ND 10 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 t-Butanol ND 41 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 t-Butyl ethyl ether ND 10 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 tert-Amyl methyl ether(TAME) ND 10 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Surrogate:1,2-Dichloroethane-d4 112% 70-130 136112514 02/25/2016 021251201618:58 Surrogate:Toluene-d8 92.1% 70-130 B6B2514 02/25/2016 021251201618:58 Surrogate:4-BromoJluorobenzene 92.9% 70-130 B6B2514 02/25/2016 021251201618:58 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 15 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 *F2 Chloromethane ND 10 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 *F2*C2 Vinyl Chloride ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 *F2*C2 Bromomethane ND 10 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 *F2*C2 Chloroethane ND 10 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Trichlorofluoromethane ND 41 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 Acetone ND 150 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Acrylonitrile ND 8.2 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:58 Trichlorotrifluorocthane ND 41 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 ],I-Dichloroethene ND 5.1 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Methylene Chloride ND 51 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Carbon Disulfide ND 10 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Methyl-t-Butyl Ether(MTBE) ND 5.1 1.96 EPA 5035AL B6B2514 02/25/2016 02/25/2016 18:58 mans-1,2-Dichloroethene ND 5.1 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:58 l,1-Dichloroethane ND 5.1 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:58 2-Butanone(MEK) ND 26 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 2,2-Dichloropropane ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 cis-1,2-Dichloroethene ND 5.1 1.96 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 18:58 Chloroform ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Tetahydrofuran ND 26 1.96 EPA5035A-L B6132514 02/25/2016 02/25/2016 18:58 1,1,1-Trichlorocthanc ND 5.1 1.96 EPA5035A-L B6132514 02/25/2016 02/25/2016 18:58 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 15 of 37 CET#:6020397 Client Sample ID Gas Dispenser Lab ID: 6020397-05 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Carbon Tetrachloride ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 ],I-Dichloropropene ND 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 Benzene 41 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 1,2-Dichloroethane ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Trichloroethene ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 1,2-Dichloropropane ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Dibromomethanc ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Bromodichloromethane ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Mcthyl Isobutyl Ketone ND 26 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 cis-1,3-Dichloropropene ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Toluene 360 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 E trans-1,3-Dichloropropene ND 5.1 1.96 EPA 5035A-L 136112514 02/25/2016 02/25/2016 18:58 2-Hexanonc ND 26 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 1,1,2-Trichloroethane ND 5.1 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Tetrachloroethcne ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 1,3-Dichloropropane ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Dibromochloromethane ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 1,2-Dibromoetliane ND 5.1 1.96 EPA5035A-L B6B2514 02/25/2016 02/25/2016 18:58 trans-1,4-Dichloro-2-Butene ND 26 1.96 EPA5035A-L 136B2514 02/25/2016 02/25/2016 18:58 Chlorobenzene ND 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 1,1,1,2-Tetrachloroethane ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Ethylbenzene 15 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 m+p Xylenes 35 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 o-Xylene 9.0 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 Styrene ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 *C2 Bromoform ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Isopropylbenzcne ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 1,1,2,2-Tetrachloroctliane ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Bromobenzene ND 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 1,2,3-Trichloropropane ND 5.1 1.96 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:58 n-Propylbenzenc ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 2-Chlorotoluenc ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 *C2 4-Chlorotoluenc ND 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 *C2 1,3,5-Trimethylbenzene ND 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 *C2 tert-Butylbenzene ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 1,2,4-Trimethylbenzene ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 sec-Butylbcnzene ND 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 1,3-Dichlorobenzenc ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 *C2 4-Isopropyltoluene ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 1,4-Dichlorobenzenc ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 1,2-Dichlorobenzenc ND 5.1 1.96 EPA 5035A-L 136132514 02/25/2016 02/25/2016 18:58 *1;2*C2 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 16 of 37 CET#:6020397 Client Sample ID Gas Dispenser Lab ID: 6020397-05 Volatile Organics Analyst:TWIT Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes n-Butylbenzene ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 *C2 1,2-Dibromo-3-Chloropropane ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 1,2,4-Trichlorobenzene ND 5.1 1.96 EPA 5035A-L B6132514 02/25/2016 02/25/2016 18:58 Hexachlorobutadiene ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 Naphthalene ND 5.1 1.96 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 18:58 1,2,3-Trichlorobenzene ND 5.1 1.96 EPA5035A-L 136132514 02/25/2016 02/25/2016 18:58 Surrogate:1,2-Dichloroethane-d4 112% 70-130 136B2514 02/25/2016 021251201618:58 Surrogate:Toluene-& 92.1% 70-130 136132514 02/25/2016 021251201618:58 Surrogate:4-BromoJluorobenzene 92.9% 70-130 B6B2514 02/25/2016 021251201618:58 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 17 of 37 CET#:6020397 Client Sample ID Gas Dispenser Lab ID: 6020397-05RE1 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix:Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 390 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 Chloromethane ND 260 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 Vinyl Chloride ND 130 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 Bromomethane ND 260 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 *C2 Chloroethane ND 260 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 Trichlorofluoromethane ND 1000 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 Acetone ND 3900 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 Acrylonitrile ND 210 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 Trichlorotrifluoroethane ND 1000 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 1,1-Dichloroethene ND 130 50.15 EPA5035A-H 136132905 02/26/2016 02/26/2016 14:13 *FI*CI Methylene Chloride ND 1300 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Carbon Disulfide ND 260 50.15 EPA5035A-H 136B2905 02/26/2016 02/26/2016 14:13 *FI*Cl Methyl-t-Butyl Ether(MTBE) ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 trans-1,2-Dichloroethene ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 1,1-Dichloroethane ND 130 50.15 EPA5035A-H 136B2905 02/26/2016 02/26/2016 14:13 2-Butanone(MEK) ND 660 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 2,2-Dichloropropane ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 cis-1,2-Dichloroethene ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 Chloroform ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Tctrahydrofuran ND 660 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 1,1,1-Trichloroethanc ND 130 50.15 EPA5035A-H 136132905 02/26/2016 02/26/2016 14:13 Carbon Tetrachloride ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 *Fl 1,1-Dichloropropenc ND 130 50.15 EPA5035A-H 136132905 02/26/2016 02/26/2016 14:13 *Fl Benzene ND 130 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 1,2-Dichloroethane ND 130 50.15 EPA5035A-H B6132905 02/26/2016 02/26/2016 14:13 Trichloroethene ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 1,2-Dichloropropane ND 130 50.15 EPA5035A-H 136B2905 02/26/2016 02/26/2016 14:13 Dibromomethane ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 Bromodichloromethane ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 Methyl Isobutyl Ketone ND 660 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 cis-1,3-Dichloropropenc ND 130 50.15 EPA5035A-H 136B2905 02/26/2016 02/26/2016 14:13 Toluene 570 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 trans-1,3-Dichloropropenc ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 2-Hexanone ND 660 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 1,1,2-Trichloroethanc ND 130 50.15 EPA5035A-H 136132905 02/26/2016 02/26/2016 14:13 Tctrachloroethene ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 1,3-Dichloropropane ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Dibromochloromethanc ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 *C2 1,2-Dibromoethane ND 130 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 trans-1,4-Dichloro-2-Butcnc ND 660 50.15 EPA5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Complete Environmental Testing,Inc. 80 Lupcs Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cettabs.com Page 18 of 37 CET#:6020397 Client Sample ID Gas Dispenser Lab ID: 6020397-05RE1 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Chlorobenzene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 1,1,1,2-Tetrachloroethane ND 130 50.15 EPA5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Ethylbenzene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 m+p Xylenes ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 o-Xylene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Styrene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Bromoform ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Isopropylbenzene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 1,1,2,2-Tetrachloroethane ND 130 50.15 EPA5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Bromobenzene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 1,2,3-Trichloropropane ND 130 50.15 EPA5035A-H 136B2905 02/26/2016 02/26/2016 14:13 n-Propylbenzene ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 2-Chlorotoluene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 4-Chlorotoluene ND 130 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 1,3,5-Trimcthylbenzene ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 tert-Butylbenzene ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 1,2,4-Trimethylbcnzene ND 130 50.15 EPA5035A-H 136B2905 02/26/2016 02/26/2016 14:13 sec-Butylbenzene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 1,3-Dichlorobenzene ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 *C2 4-Isopropyholuene ND 130 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 *C2 1,4-Dichlorobenzene ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 1,2-Dichlorobenzene ND 130 50.15 EPA5035A-H B6B2905 02/26/2016 02/26/2016 14:13 *C2 n-Butylbenzene ND 130 50.15 EPA 5035A-H B6B2905 02/26/2016 02/26/2016 14:13 *C2 1,2-Dibromo-3-Chloropropane ND 130 50.15 EPA 5035A-H 136B2905 02/26/2016 02/26/2016 14:13 1,2,4-Trichlorobenzene ND 130 50.15 EPA5035A-H B6B2905 02/26/2016 02/26/2016 14:13 Hexachlorobutadicne ND 130 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 Naphthalene ND 130 50.15 EPA 5035A-H 136132905 02/26/2016 02/26/2016 14:13 1,2,3-Trichlorobenzenc ND 130 50.15 EPA 5035A-H B6132905 02/26/2016 02/26/2016 14:13 Surrogate:1,2-Dichloroethane-d4 93.2% 70-130 B6132905 02/26/2016 021261201614:13 Surrogate:Toluene-d8 95.9% 70-130 136132905 02/26/2016 021261201614:13 Surrogate:4-Bromofluorobenzene 90.0% 70-130 136132905 02/26/2016 021261201614:13 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 19 of 37 CET#:6020397 Client Sample ID Gas Lines Lab ID: 6020397-06 Volatile Organics Analyst: TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Di-isopropyl ether ND 10 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 t-Butanol ND 41 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 t-Butyl ethyl ether ND 10 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 tort-Amyl methyl ether(TAME) ND 10 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Surrogate:1,2-Dichloroethane-d4 116% 70-130 136132514 02/25/2016 021251201619:22 Surrogate:Toluene-d8 98.6% 70-130 136B2514 02/25/2016 021251201619:22 Surrogate:4-Bromofluorohenzene 82.5% 70-130 B6132514 02/25/2016 021251201619:22 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix:Soil Result RL Datc/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Dichlorodifluoromethane ND 15 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 *F2 Chloromethane ND 10 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 *F2*C2 Vinyl Chloride ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 *F2*C2 Bromomethane ND 10 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 *F2*C2 Chloroethane ND 10 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Trichlorofluoromethanc ND 41 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Acetone ND 150 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 Acrylonitrile ND 8.3 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 Trichlorotrifluoroethane ND 41 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 1,1-Dichlorocthene ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Methylene Chloride ND 52 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Carbon Disulfide ND 10 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Methyl-t-Butyl Ether(MTBE) ND 5.2 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 trans-1,2-Dicliloroethene ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 ],I-Dichloroethane ND 5.2 1.93 EPA5035A-L B6132514 02/25/2016 02/25/2016 19:22 2-Butanone(MEK) ND 26 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 2,2-Dichloropropane ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 cis-1,2-Dichlorocthene ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 Chloroform ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 Tetrahydrofuran ND 26 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 1,1,1-Tiichloroethane ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 20 of 37 CET#:6020397 Client Sample ID Gas Lines Lab ID: 6020397-06 Volatile Organics Analyst:TWF Method:EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes Carbon Tetrachloride ND 5.2 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 1,1-Dichloropropene ND 5.2 1.93 EPA5035A-L B6132514 02/25/2016 02/25/2016 19:22 Benzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,2-Dichloroethane ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Trichloroethene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,2-Dichloropropane ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 Dibromomethane ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 Bromodichloromethane ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 Methyl Isobutyl Ketone ND 26 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 cis-1,3-Dichloropropene ND 5.2 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 Toluene 10 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 trans-1,3-Dichloropropene ND 5.2 1.93 EPA5035A-L 136B2514 02/25/2016 02/25/2016 19:22 2-Hexanone ND 26 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 1,1,2-Trichloroethane ND 5.2 1.93 EPA5035A-L B6132514 02/25/2016 02/25/2016 19:22 Tetrachloroethene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,3-Dichloropropane ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 Dibromochloromcthane ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,2-Dibromoethane ND 5.2 1.93 EPA5035A-L 136132514 02/25/2016 02/25/2016 19:22 trans-1,4-Dichloro-2-Butene ND 26 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 Chlorobenzenc ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,1,1,2-Tetrachloroethane ND 52 1.93 EPA5035A-L 136B2514 02/25/2016 02/25/2016 19:22 Ethylbenzene ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 m+p Xylenes ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 o-Xylenc ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 Styrene ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 *C2 Bromoform ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 Isopropylbenzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,1,2,2-Tetrachloroethane ND 5.2 1.93 EPA5035A-L 136132514 02/25/2016 02125/201619:22 Bromobenzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,2,3-Trichloropropane ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 n-Propylbenzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 2-Chlorotoluene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 *C2 4-Chlorotoluene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 *C2 1,3,5-Trimethylbenzene ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 *C2 tert-Butylbenzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,2,4-Trimethylbenzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 sec-Butylbenzene ND 5.2 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 1,3-Dichlorobenzene ND 5.2 1.93 EPA 5035A-L 136B2514 02/25/2016 02/25/2016 19:22 *C2 4-Isopropyltoluene ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 1,4-Dichlorobenzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 1,2-Dichlorobenzene ND 5.2 1.93 EPA 5035A-L 136132514 02/25/2016 02/25/2016 19:22 *F2*C2 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetiabs.com Page 21 of 37 CET#:6020397 Client Sample ID Gas Lines Lab ID:6020397-06 Volatile Organics Analyst:TWF Method: EPA 8260C Matrix: Soil Result RL Date/Time Analyte (ug/kg dry) (ug/kg dry) Dilution Prep Method Batch Prepared Analyzed Notes n-Butylbenzene ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 *C2 1,2-Dibromo-3-Chloropropane ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 1,2,4-Trichlorobenzene ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 Hexachlorobutadicne ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 Naphthalene ND 5.2 1.93 EPA 5035A-L B6B2514 02/25/2016 02/25/2016 19:22 1,2,3-Trichlorobenzene ND 5.2 1.93 EPA 5035A-L B6132514 02/25/2016 02/25/2016 19:22 Surrogate:1,2-Dichloroethane-d4 116% 70-130 B6132514 02/25/2016 021251201619:22 Surrogate:Toluene-d8 98.6% 70-130 B6B2514 02/25/2016 021251201619:22 Surrogate:4-BromoJluorobenzene 82.5% 70-130 B6B2514 02/25/2016 021251201619:22 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 22 0737 CET#:6020397 QUALITY CONTROL SECTION Batch B6B2514-EPA 8260C Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2514-BLK1) Prepared:2/25/2016 Analyzed:2/25/2016 Dichlorodifluoromethane ND 7.5 Chloromethane ND 5.0 Vinyl Chloride ND 2.5 Bromomethane ND 5.0 Chloroethane ND 5.0 Trichlorofluoromethane ND 20 Acetone ND 75 Acrylonitrile ND 4.0 Di-isopropyl ether ND 5.0 t-Butanol ND 20 Trichlorotrifluoroethane ND 20 I,1-Dichloroethene ND 2.5 t-Butyl ethyl ether ND 5.0 tert-Amyl methyl ether(TAME) ND 5.0 Methylene Chloride ND 25 Carbon Disulfide ND 5.0 Methyl-t-Butyl Ether(MTBE) ND 2.5 trans-1,2-Dichloroethene ND 2.5 I,1-Dichloroethane ND 2.5 2-Butanone(MEK) ND 13 2,2-Dichloropropane ND 2.5 cis-1,2-Dichloroethene ND 2.5 Chloroform ND 2.5 Tetrahydrofuran ND 13 1,1,1-Trichloroethane ND 2.5 Carbon Tetrachloride ND 2.5 I,1-Dichloropropene ND 2.5 Benzene ND 2.5 1,2-Dichloroethane ND 2.5 Trichloroetliene ND 2.5 1,2-Dichloropropane ND 2.5 Dibromomethane ND 2.5 Bromodichloromethane ND 2.5 Methyl Isobutyl Ketone ND 13 cis-1,3-Dichloropropene ND 2.5 Toluene ND 2.5 trans-1,3-Dichloropropene ND 2.5 2-Hexanone ND 13 1,1,2-Trichloroethane ND 2.5 Tetrachloroethene ND 2.5 1,3-Dichoropropane ND 2.5 Dibromochloromethane ND 2.5 1,2-Dibromoethane ND 2.5 trans-1,4-Dichloro-2-Butene ND 13 Chlorobenzene ND 2.5 1,1,1,2-Tetrachloroethane ND 2.5 Ethylbenzene ND 2.5 m+p Xylenes ND 2.5 o-Xylene ND 2.5 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetiabs.com Page 23 of 37 CET#:6020397 Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rcc Limits RPD Limit Notes Blank(B6B2514-BLKI)-Continued Prepared:2/25/2016 Analyzed:2/25/2016 Styrene ND 2.5 Bromoform ND 2.5 Isopropylbenzene ND 2.5 1,1,2,2-Tetrachloroethane ND 2.5 Bromobenzene ND 2.5 1,2,3-Trichloropropane ND 2.5 n-Propylbenzene ND 2.5 2-Chlorotoluene ND 2.5 4-Chlorotoluene ND 2.5 1,3,5-Trimethylbenzenc ND 2.5 tort-Butylbenzene ND 2.5 1,2,4-Trimethylbenzenc ND 2.5 sec-Butylbenzene ND 2.5 1,3-Dichlorobenzene ND 2.5 4-Isopropyltoluene ND 2.5 1,4-Dichlorobenzene ND 2.5 1,2-Dichlorobenzene ND 2.5 n-Butylbenzene ND 2.5 1,2-Dibromo-3-Chloropropane ND 2.5 1,2,4-Trichlorobenzene ND 2.5 Hexachlorobutadiene ND 2.5 Naphthalene ND 2.5 1,2,3-Trichlorobenzene ND 2.5 Surrogate:l,2-Dichloroethane-d4 96.3 70-130 Surrogate:l,2-Dichloroethane-d4 96.3 70-130 Surrogate:Toluene-d8 91.1 70-130 Surrogate:Toluene-d8 91.1 70-130 Surrogate:4-Bromq luorobenzene 84.3 70-130 Surrogate:4-BromoJluorobenzene 84.3 70-130 LCS(B6B2514-BSI) Prepared:2/25/2016 Analyzed:2/25/2016 Dichlorodifluoromethane 70.0 7.5 50.000 140 70-130 H Chloromcthanc 85.3 5.0 50.000 171 70-130 H Vinyl Chloride 85.8 2.5 50.000 172 70-130 H Bromomcthane 91.9 5.0 50.000 184 70-130 H Chloroethane 60.0 5.0 50.000 120 70-130 Trichlorofluoromethane 54.8 20 50.000 110 70-130 Acetone 97.4 75 100.000 97.4 70-130 Acrylonitrilc 49.0 4.0 50.000 98.0 70-130 Di-isopropyl ether 51.6 5.0 50.000 103 70-130 t-Butanol 450 20 500.000 90.1 70-130 Trichlorotrifluoroethane 41.0 20 50.000 81.9 70-130 1,1-Dichloroethenc 37.2 2.5 50.000 74.3 70-130 t-Butyl ethyl ether 44.6 5.0 50.000 89.1 70-130 tert-Amyl methyl ether(TAME) 41.4 5.0 50.000 82.7 70-130 Methylene Chloride 42.3 25 50.000 84.6 70-130 Carbon Disulfide 37.6 5.0 50.000 75.2 70-130 Methyl-t-Butyl Ether(MTBE) 44.0 2.5 50.000 88.1 70-130 mans-1,2-Dichloroethenc 42.5 2.5 50.000 84.9 70-130 I,l-Dichloroethane 51.7 2.5 50.000 103 70-130 2-Butanone(MEK) 102 13 100.000 102 70-130 2,2-Dichloropropanc 54.4 2.5 50.000 109 70-130 cis-1,2-Dichloroethhene 55.2 2.5 50.000 110 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 24 of 37 CET#:6020397 Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes LCS(B6132514-13SI)-Continued Prepared:2/25/2016 Analyzed:2/25/2016 Chloroform 50.4 2.5 50.000 101 70-130 Tetrahydrofuran 47.6 13 50.000 95.2 70-130 1,1,1-Trichloroethane 53.9 2.5 50.000 108 70-130 Carbon Tetrachloride 47.0 2.5 50.000 93.9 70-130 1,1-Dichloropropene 48.1 2.5 50.000 96.2 70-130 Benzene 51.3 2.5 50.000 103 70-130 1,2-Dichloroethane 53.5 2.5 50.000 107 70-130 Trichloroethene 46.1 2.5 50.000 92.2 70-130 1,2-Dichloropropane 52.9 2.5 50.000 106 70-130 Dibromomethane 50.3 2.5 50.000 101 70-130 Bromodichloromethane 52.5 2.5 50.000 105 70-130 Methyl isobutyl Ketone 111 13 100.000 111 70-130 cis-1,3-Dichloropropene 51.3 2.5 50.000 103 70-130 Toluene 48.1 2.5 50.000 96.2 70-130 trans-1,3-Dichloropropene 55.4 2.5 50.000 ill 70-130 2-Hexanone 120 13 100.000 120 70-130 1,1,2-Trichloroethane 53.0 2.5 50.000 106 70-130 Tetrachloroethene 48.1 2.5 50.000 96.2 70-130 1,3-Dichloropropane 52.1 2.5 50.000 104 70-130 Dibromochloromethane 56.9 2.5 50.000 114 70-130 1,2-Dibromoethane 57.3 2.5 50.000 115 70-130 trans-1,4-Dichloro-2-Butene 57.1 13 50.000 114 70-130 Chlorobenzene 56.6 2.5 50.000 113 70-130 1,1,1,2-Tetrachloroethane 56.9 2.5 50.000 114 70-130 Ethylbenzene 55.0 2.5 50.000 110 70-130 m+p Xylenes 118 2.5 100.000 118 70-130 o-Xylene 53.0 2.5 50.000 106 70-130 Styrene 57.0 2.5 50.000 114 70-130 Bromoform 51.9 2.5 50.000 104 70-130 Isopropylbenzene 56.7 2.5 50.000 113 70-130 1,1,2,2-Tetrachlorocthane 57.8 2.5 50.000 116 70-130 Bromobenzene 62.0 2.5 50.000 124 70-130 1,2,3-Trichloropropane 59.0 2.5 50.000 118 70-130 n-Propylbenzene 63.0 2.5 50.000 126 70-130 2-Chlorotolucnc 54.3 2.5 50.000 109 70-130 4-Chlorotolucnc 56.0 2.5 50.000 112 70-130 1,3,5-Trimethylbenzene 54.5 2.5 50.000 109 70-130 tert-Butylbenzene 50.9 2.5 50.000 102 70-130 1,2,4-Trimethylbenzene 55.9 2.5 50.000 112 70-130 sec-Butylbenzene 56.2 2.5 50.000 112 70-130 1,3-Dichlorobenzene 59.8 2.5 50.000 120 70-130 4-Isopropyltoluene 58.6 2.5 50.000 117 70-130 1,4-Dichlorobenzenc 60.6 2.5 50.000 121 70-130 1,2-Dichlorobenzene 66.3 2.5 50.000 133 70-130 H n-Butylbenzene 63.7 2.5 50.000 127 70-130 1,2-Dibromo-3-Chloropropane 54.4 2.5 50.000 109 70-130 1,2,4-Trichlorobenzene 60.4 2.5 50.000 121 70-130 Hexachlorobutadiene 49.8 2.5 50.000 99.6 70-130 Naphthalene 55.6 2.5 50.000 ill 70-130 1,2,3-Trichlorobenzene 60.8 2.5 50.000 122 70-130 Surrogate:1,2-Dichloroethane-d4 102 70-130 .Surrogate:1,2-Dichloroethane-d4 102 70-130 Szoragate:Tohiene-d8 97.8 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 25 of 37 CET#:6020397 Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes LCS(MMS14-BSI)-Continued Prepared:2/25/2016 Analyzed:2/25/2016 Surrogate:Toluene-418 97.8 70-130 Surrogate:4-Bromofbrorobenzene 102 70-130 Surrogate:4-Bronigluorobenzene 102 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 26 of 7771 CET#:6020397 Batch B6B2905-EPA 8260C Result RL Spike Source %Rec RPD Analytc (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes Blank(B6B2905-BLK1) Prepared:2/26/2016 Analyzed:2/26/2016 Diehlorodifluoromethane ND 7.5 Chloromethane ND 5.0 Vinyl Chloride ND 2.5 Bromomethane ND 5.0 Chloroethane ND 5.0 Trichlorofluoromethane ND 20 Acetone ND 75 Acrylonitrile ND 4.0 Trichlorotrifluoroethane ND 20 I,1-Dichloroethene ND 2.5 Methylene Chloride ND 25 Carbon Disulfide ND 5.0 Methyl-t-Butyl Ether(MTBE) ND 2.5 trans-1,2-Dichloroethene ND 2.5 ],I-Dichloroethane ND 2.5 2-Butanone(MEK) ND 13 2,2-Dichloropropane ND 2.5 cis-1,2-Dichloroethene ND 2.5 Chloroform ND 2.5 Tetrahydrofuran ND 13 1,1,1-Trichloroethane ND 2.5 Carbon Tetrachloride ND 2.5 I,I-Dichloropropene ND 2.5 Benzene ND 2.5 1,2-Dichloroethane ND 2.5 Trichloroethane ND 2.5 1,2-Dichloropropane ND 2.5 Dibromomethane ND 2.5 Bromodichloromethane ND 2.5 Methyl Isobutyl Ketone ND 13 cis-1,3-Dichloropropene ND 2.5 Toluene ND 2.5 trans-1,3-Dichloropropene ND 2.5 2-Hexanone ND 13 1,1,2-Trichloroethane ND 2.5 Tetrachloroethcne ND 2.5 1,3-Dichloropropane ND 2.5 Dibromochloromcthane ND 2.5 1,2-Dibromoethane ND 2.5 trans-1,4-Dichloro-2-Butene ND 13 Chlorobenzene ND 2.5 1,1,1,2-Tetrachloroethane ND 2.5 Ethylbenzene ND 2.5 m+p Xylenes ND 2.5 o-Xylene ND 2.5 Styrene ND 2.5 Bromofonn ND 2.5 Isopropylbcnzene ND 2.5 1,1,2,2-Tetrachloroethane ND 2.5 Bromobenzene ND 2.5 1,2,3-Trichloropropanc ND 2.5 n-Propylbenzene ND 2.5 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.ectlabs.com Page 27 of 37 CET#:6020397 Result RL Spike Source %Roe RPD Analyte (ug/kg) (ug/kg) Level Result %Roe Limits RPD Limit Notes Blank(B6B2905-BLKI)-Continued Prepared:2/26/2016 Analyzed:2/26/2016 2-Chlorotoluene ND 2.5 4-Chlorotoluene ND 2.5 1,3,5-Trimcthylbenzene ND 2.5 tcrt-Butylbenzene ND 2.5 1,2,4-Trimethylbenzcnc ND 2.5 sec-Butylbenzene ND 2.5 1,3-Dichlorobenzene ND 2.5 4-Isopropyltoluene ND 2.5 1,4-Dichlorobenzene ND 2.5 1,2-Dichlorobenzene ND 2.5 n-Butylbenzcne ND 2.5 1,2-Dibromo-3-Chloropropane ND 2.5 1,2,4-Trichlorobenzene ND 2.5 Hexachlorobutadiene ND 2.5 Naphthalene ND 2.5 1,2,3-Trichlorobenzene ND 2.5 Surrogate:l,2-Dichloroethane-d4 95.6 70-130 Surrogate:Toluene-d8 99.9 70-130 Surrogate:4-Bromgfluorobenzene 89.7 70-130 LCS(B6B2905-BSI) Prepared:2/26/2016 Analyzed:2/26/2016 Dichlorodifluoromethane 52.5 7.5 50.000 105 70-130 Chloromethane 43.4 5.0 50.000 86.8 70-130 Vinyl Chloride 39.0 2.5 50.000 77.9 70-130 Bromomethane 59.8 5.0 50.000 120 70-130 Chloroethanc 36.2 5.0 50.000 72.3 70-130 Trichlorofluoromethane 37.8 20 50.000 75.7 70-130 Acetone 91.9 75 100.000 91.9 70-130 Acrylonitrile 39.9 4.0 50.000 79.7 70-130 Trichlorotrifluoroethanc 35.9 20 50.000 71.7 70-130 1,1-Dichloroethene 26.5 2.5 50.000 53.1 70-130 L Methylene Chloride 40.0 25 50.000 79.9 70-130 Carbon Disulfide 27.2 5.0 50.000 54.3 70-130 L Methyl-t-Butyl Ether(MTBE) 41.3 2.5 50.000 82.6 70-130 trans-l,2-Dichloroethenc 38.2 2.5 50.000 76.4 70-130 1,1-Dichloroethane 40.9 2.5 50.000 81.8 70-130 2-Butanone(MEK) 75.8 13 100.000 75.8 70-130 2,2-Dichloropropanc 36.1 2.5 50.000 72.2 70-130 cis-1,2-Dichloroethenc 42.6 2.5 50.000 85.2 70-130 Chlorofonn 39.7 2.5 50.000 79.3 70-130 Tetrahydrofuran 39.5 13 50.000 78.9 70-130 1,1,1-Trichlorocthanc 37.6 2.5 50.000 75.1 70-130 Carbon Tetrachloride 32.4 2.5 50.000 64.9 70-130 L ],I-Dichloropropene 33.2 2.5 50.000 66.5 70-130 L Benzene 41.7 2.5 50.000 83.3 70-130 1,2-Dichloroethane 45.9 2.5 50.000 91.8 70-130 Trichlorocthene 38.9 2.5 50.000 77.7 70-130 1,2-Dichloropropane 49.5 2.5 50.000 99.0 70-130 Dibromomcthane 47.3 2.5 50.000 94.5 70-130 Bromodichloromethane 50.1 2.5 50.000 100 70-130 Methyl Isobutyl Ketone 98.0 13 100.000 98.0 70-130 cis-1,3-Dichloropropene 49.4 2.5 50.000 98.8 70-130 Toluene 40.1 2.5 50.000 80.2 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com rPage 28 0737 CET#:6020397 Result RL Spike Source %Rec RPD Analyte (ug/kg) (ug/kg) Level Result %Rec Limits RPD Limit Notes LCS(B6B2905-BS1)-Continued Prepared:2/26/2016 Analyzed:2/26/2016 trans-1,3-Dichloropropene 49.1 2.5 50.000 98.2 70-130 2-Hexanone 93.4 13 100.000 93.4 70-130 1,1,2-Trichloroethane 46.1 2.5 50.000 92.1 70-130 Tetrachloroethene 35.2 2.5 50.000 70.3 70-130 1,3-Dichloropropane 45.9 2.5 50.000 91.9 70-130 Dibromochloromethane 62.2 2.5 50.000 124 70-130 1,2-Dibromoethane 58.1 2.5 50.000 116 70-130 trans-1,4-Dichloro-2-Butene 52.1 13 50.000 104 70-130 Chlorobenzene 53.4 2.5 50.000 107 70-130 1,1,1,2-Tetrachlorocthane 55.7 2.5 50.000 111 70-130 Ethylbenzene 47.4 2.5 50.000 94.7 70-130 m+p Xylenes 101 2.5 100.000 101 70-130 o-Xylene 50.3 2.5 50.000 101 70-130 Styrene 56.9 2.5 50.000 114 70-130 Bromoform 51.9 2.5 50.000 104 70-130 Isopropylbenzene 48.2 2.5 50.000 96.4 70-130 1,1,2,2-Tetrachloroethane 54.6 2.5 50.000 109 70-130 Bromobenzene 58.4 2.5 50.000 117 70-130 1,2,3-Trichloropropane 59.7 2.5 50.000 119 70-130 n-Propylbenzene 56.0 2.5 50.000 112 70-130 2-Chlorotolucnc 56.9 2.5 50.000 114 70-130 4-Chlorotoluene 57.0 2.5 50.000 114 70-130 1,3,5-Trimethylbenzene 54.3 2.5 50.000 109 70-130 tert-Butylbenzene 49.9 2.5 50.000 99.7 70-130 1,2,4-Trimethylbenzene 55.6 2.5 50.000 111 70-130 sec-Butylbenzene 51.4 2.5 50.000 103 70-130 1,3-Dichlorobenzene 57.0 2.5 50.000 114 70-130 4-Isopropyltoluene 51.1 2.5 50.000 102 70-130 1,4-Dichlorobenzene 57.8 2.5 50.000 116 70-130 1,2-Dichlorobenzene 59.4 2.5 50.000 119 70-130 n-Butylbcnzenc 54.0 2.5 50.000 108 70-130 1,2-Dibromo-3-Chloropropane 54.3 2.5 50.000 109 70-130 1,2,4-Trichlorobenzene 55.9 2.5 50.000 112 70-130 Hexachlorobutadiene 47.8 2.5 50.000 95.6 70-130 Naphthalene 52.9 2.5 50.000 106 70-130 1,2,3-Trichlorobenzene 56.9 2.5 50.000 114 70-130 Surrogate:1,2-Dichloroethane-d4 104 70-130 Surrogate:Toluene-dS 95.2 70-130 Surrogate:4-Bromofluorobenzene 101 70-130 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 29 of 37 CET ff:6020397 Questions related to this report should be directed to David Ditta,Timothy Fusco,or Robert Blake at 203-377-9984. Sincerely, J'c David Ditta Laboratory Director Report Comments: Sample Result Flags: E-The result is estimated,above the calibration range. H-The surrogate recovery is above the control limits. L-The surrogate recovery is below the control limits. B-The compound was detected in the laboratory blank. P-The Relative Percent Difference(RPD)of dual column analyses exceeds 40%. D-The RPD between the sample and the sample duplicate is high. Sample Homogenity may be a problem. +- The Surrogate was diluted out. *Cl-The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2-The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *Fl-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2-The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I-The Analyte exceeds%RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result,or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 30 of 37 CET#:6020397 (203 80 Lupes Drive Tel: )377-9984 Stratford,CT 06615 COMPUT1 INVIRIlNMINTAI 11511NG.ING. Fax:(203)377-9952 email:cctl@cetlabs.com Quality Control Definitions and Abbreviations Internal Standard(IS) An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time,calculate relative response,and quantify analytes of interest. Surrogate Recovery The%recovery for non-tarer organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method,sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels(MDL)and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analytc added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte foun in duplicate spikes including amount that was spike. Matrix Spike%Recovery %Recovery of spiked amount in sample. Matrix Spike Dup%Recovery %Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS%Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H- Recovery is above the control limits L- Recovery is below the control limits B- Compound detected in the Blank P- RPD of dual column results exceeds 40% #- Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 _ j New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Complete Environmental Testing,Inc. 80 Lupes Drive,Stratford,CT 06615•Tel:203-377-9984•Fax:203-377-9952•www.cetlabs.com Page 31 of 37 REASONABLE CONFIDENCE PROTOCOL ` LABORATORY ANALYSIS QA/QC CERTIFICATION FORM Laboratory Name: Complete Environmental Testing,Inc. Client. Enviroshield,Inc. Project Location: Tank Pull Project Number: Laboratory Sample 11)(s): Sample Date(s): 6020397-01thtu 6020397-06 02/18/2016 List RCP Methods Used: CET#: 6020397 EPA 8260C 1 For each analytical method referenced in this laboratory report package,were all specified QA/QC ❑✓Yes ❑ No performance criteria followed,including the requirement to explain any criteria falling outside of acceptable guidelines,as specified in the CTDEP method-specific Reasonable Confidence Protocol documents? IA Were the method specified preservation and holding time requirements met? ❑✓Yes ❑ No 113 VPH and EPH Methods only: Was the VPH and EPH method conducted without significant ❑Yes ❑ No modifications(see Section 11.3 of respective RCP methods)? ❑✓ N/A 2 Were all samples received by the laboratory in a condition consistent with that described on the [Dye, ❑ No associated chain-of-custody document(s)? ❑ 3 Were samples received at an appropriate temperature(<6 degrees C.)? ❑✓Yes No ❑ N/A 4 Were all QA/QC performance criteria specified in the CT DEP Reasonable Confidence Protocol ❑Yes ❑✓ No documents achieved? 5a a)Were reporting limits specified or referenced on the chain-of-custody? ❑Yes ❑✓ No 5b b)Were these reporting limits met? ❑yes ❑ No 6 For each analytical method referenced in this laboratory report package,were results reported for ❑Yes ❑ No all consituents identified in the method-specific analyte lists presented in the Reasonable Confidence Protocol documents? 7 Are project specific matrix spikes and laboratory duplicates included with this data set? ❑Yes ❑✓ No Notes:For all questions to which the response was"No"(with the exception of question#7),additional information must be provided in an attached narrative.If the answer to question#1,#I A,or#I B is"No",the data package does not meet the requirements for"Reasonable Confidence." This form may not be altered and all questions must be answered. I,the undersigned,attest under the pains and penalties of perjury that,to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report,such information is accurate and complete. Authorized Signature: Position:Laboratory Director Printed Name:David Ditta Date: 02/29/2016 Name of Laboratory:Complete Environmental Testine,Inc. This certification form is to be used for RCP methods only. CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 32 of 37 RCP Case Narrative 4-See Exceptions Report Below 7-Project specific QC was not requested by the client. 4-Exceptions Report Recovery Batch/Sequence Analyte QC Type Exception Result RPD (%) Sample ID 1,2-Dichlorobenzene LCS High 133 B6B2514 Bromomcthanc LCS High 184 B6B2514 Chloromethane LCS High 171 B6B2514 Dichlorodifluoromethane LCS High 140 B6B2514 Vinyl Chloride LCS High 172 B6B2514 ],I-Dichloroethene LCS Low 53.1 B6B2905 1,1-Dichloropropene LCS Low 66.5 B6B2905 Carbon Disulfide LCS Low 54.3 B6B2905 Carbon Tetrachloride LCS Low 64.9 B6B2905 1,2-Dichlorobenzene CC High 72.7 145 S6B2602 1,3,5-Trimethylbenzene CC High 68.0 136 S6B2602 1,3-Dichlorobenzene CC High 68.6 137 S6B2602 2-Chlorotoluene CC High 69.3 139 S6B2602 4-Chlorotoluene CC High 70.0 140 S6B2602 Bromomethane CC High 71.5 143 S6B2602 Chloromethane CC High 68.1 136 S6B2602 n-Butylbenzene CC High 67.1 134 S6B2602 Styrene CC High 66.3 133 S6B2602 Vinyl Chloride CC High 65.0 130 S6B2602 1,1-Dichloroethene CC Low 35.3 70.6 S6B2902 1,2-Dichlorobenzene CC High 64.2 128 S6B2902 1,3-Dichlorobenzene CC High 62.8 126 S6B2902 4-Isopropyltoluene CC High 63.3 127 S6B2902 Bromomethane CC High 72.7 145 S6B2902 Carbon Disulfide CC Low 30.4 60.7 S6B2902 Dibromochloromethane CC High 63.2 126 S6B2902 n-Butylbenzene CC High 63.0 126 S6B2902 CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 33 of 37 QC Batch/Sequence Report Batch Sequence CET ID Sample ID Specific Method Matrix Collection Date B6B2514 S6B2602 6020397-01 Gas South EPA 8260C Soil 02/18/2016 B6B2514 S6B2602 6020397-02 Gas East EPA 8260C Soil 02/18/2016 B6B2514 S6B2602 6020397-03 Gas West EPA 8260C Soil 02/18/2016 B6B2514 S6B2602 6020397-04 Gas Bottom EPA 8260C Soil 02/18/2016 B6B2514 S6B2602 602039.7-05 Gas Dispenser EPA 8260C Soil 02/18/2016 B6B2514 S6B2602 6020397-06 Gas Lines EPA 8260C Soil 02/18/2016 B6B2905 S6B2902 6020397-05RE1 Gas Dispenser EPA 8260C Soil 02/18/2016 CTDEP RCP Laboratory Analysis QA/QC Certification Form-November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 34 of 37