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HomeMy WebLinkAbout560 Nutmeg Road - UST - Fire Marshal EcEr M E AUG 16 2012 Tankworks Jordan Perlroth 44 Hitchcock Lane Avon, CT 06001 RE: Removal and Disposal of(1) 2,000 Gallon Gasoline Tank At: 560 Nutmeg Lane, South Windsor, CT To Mr. Perlroth, Thank you for the opportunity to service the removal of the buried Gasoline tank at the above referenced address. The work was performed in accordance with E.P.A. Regulations and N.F.P.A. 30 and 30A Requirements. The soil in the grave showed no signs of contamination and was backfilled. Before backfilling 6 final confirmation soil samples were collected and tested at an independent lab for Method 8260. All soil samples taken were below detectable limits. This letter, along with the attached soil sample results, should be stored safely with all legal documents pertaining to this property. This information, along with your Tankworks invoice and cancelled checks will serve as verification for future reference. Please feel free to call us if you have any further questions. It has been a pleasure working with you. We hope that you are pleased with our services and that you will recommend us to others. Very truly ours, v . Rosemary Viola Ramville Owner CC: Town of South Windsor, Office of the Fire Marshal, : aa a • m ® aa PHOEVY - Wednesday,August 08, 2012 Attn: Mrs. Rose Rainville Tankworks Removal & Replacement, LLC 360 East Center Street Manchester, CT 06040 Project ID: 560 NUTMEG Sample ID#s: BC50477 - BC50481 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory. All soils and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original. If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200. Sincerely yours, Phyllis Shiller Laboratory Director NELAC -#NY11301 NJ Lab Registration#CT-003 CT Lab Registration#PH-0618 NY Lab Registration#11301 MA Lab Registration#MA-CT-007 PA Lab Registration#68-03530 ME Lab Registration #CT-007 RI Lab Registration#63 NH Lab Registration #213693-A,B VT Lab Registration#VT11301 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06040 Telephone(860)645-1102 Fax(860)645-0823 r Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Mrs. Rose Rainville Tankworks Removal & Replacement, LLC August 08, 2012 360 East Center Street Manchester, CT 06040 Sample Information Custody Information Date Time Matrix: SOIL Coilected by: 08/06/12 0:00 Location Code: TANKWKS Received by: LB 08/06/12 12:30 Rush Request: 24 Hour Analyzed by: see"By"below P.O.#: Laboratory Data SDG ID: GBC50477 Phoenix ID: BC50477 Project ID: 560 NUTMEG Client ID: NORTH RU Parameter Result PQL Units Date/Time By Reference Percent Solid 85 % 08/06/12 JL E160.3 Aromatic Volatiles 1,2,3-Trichlorobenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trichlorobenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trimethylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 1,2-Dichlorobenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 1,3,5-Trimethylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 1,3-Dichlorobenzene ND 4.9 ug/Kg 08/06/12 R/J SW802118260 1,4-Dichlorobenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Benzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Chlorobenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Ethylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Isopropylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 m&p-Xylene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Methyl t-butyl ether(MTBE) ND 9.8 ug/Kg 08/06/12 R/J SW8021/8260 Naphthalene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 n-Butylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 n-Propylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 o-Xylene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 p-Isopropyltoluene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 sec-Butylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Styrene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 tert-Butylbenzene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Toluene ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 Total Xylenes ND 4.9 ug/Kg 08/06/12 R/J SW8021/8260 QAIQC Surrogates •1,2-dichlorobenzene-d4 103 % 08106/12 R/J 70-130% •Bromofluorobenzene 82 % 08/06/12 R/J 70-130 Page 1 of 10 Ver 1 Project ID: 560 NUTMEG Phoenix I.D.: BC50477 Client ID: NORTH RL/ Parameter Result PQL Units Date/Time By Reference %Dibromofluoromethane 107 % 08/06/12 R/J 70-130% %Toluene-d8 97 % 08/06/12 R/J 70-130% RUPQL=Reporting/Pratical Quantitation Level ND=Not Detected BRL=Below Reporting Level Comments: All soils and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If there are any questions regarding this data,please call Phoenix Client Services at extension 200. This report must not be reproduced except in full as defined by the attached chain of custody. Phyllis hiller,Laboratory Director August 08,2012 Reviewed and Released by:Johanna Harrington,Project Manager Page 2 of 10 Ver 1 PHOEVY t' Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Mrs. Rose Rainville Tankworks Removal & Replacement, LLC August 08, 2012 360 East Center Street Manchester, CT 06040 Sample Information Custody Information Date Time Matrix: SOIL Collected by: 08/06/12 0:00 Location Code: TANKWKS Received by: LB 08/06/12 12:30 Rush Request: 24 Hour Analyzed by: see"By"below P.O.#: Laboratory Data SDG ID: GBC50477 Phoenix ID: BC50478 Project ID: 560 NUTMEG Client ID: SOUTH RL/ Parameter Result PQL Units Date/Time By Reference Percent Solid 81 % 08/06/12 JL E160.3 Aromatic Volatiles 1,2,3-Trichlorobenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trichlorobenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trimethylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 1,2-Dichlorobenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 1,3,5-Trimethylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 1,3-Dichlorobenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 1,4-Dichlorobenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 Benzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 Chlorobenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 Ethylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 Isopropylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 m&p-Xylene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 Methyl t-butyl ether(MTBE) ND 10 ug/Kg 08/06/12 R/J SW8021/8260 Naphthalene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 n-Butylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 n-Propylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW802118260 o-Xylene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 p-Isopropyltoluene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 sec-Butylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW802118260 Styrene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 tert-Butylbenzene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 Toluene ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 Total Xylenes ND 5.1 ug/Kg 08/06/12 R/J SW8021/8260 QA/QC Surrogates •1,2-dichlorobenzene-d4 100 % 08/06/12 R/J 70-130% •Bromofluorobenzene 88 % 08/06/12 R/J 70-130% Page 3 of 10 Ver 1 Project ID: 560 NUTMEG Phoenix I.D.: BC50478 Client ID: SOUTH RL/ Parameter Result PQL Units Date/Time By Reference •Dibromofluoro methane 106 % 08/06/12 R/J 70-130% •Toluene-d8 97 % 08/06/12 R/J 70-130% RUPQL=Reporting/Pratical Quantitation Level ND=Not Detected BRL=Below Reporting Level Comments: All soils and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If there are any questions regarding this data,please call Phoenix Client Services at extension 200. This report must not be reproduced except in full as defined by the attached chain of custody. Phyllis hiller,Laboratory Director August 08,2012 Reviewed and Released by:Johanna Harrington,Project Manager Page 4 of 10 Ver 1 PHOENIXly Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Mrs. Rose Rainville Tankworks Removal & Replacement, LLC August 08, 2012 360 East Center Street Manchester, CT 06040 Sample Information Custody Information Date Time Matrix: SOIL Collected by: 08/06l12 0:00 Location Code: TANKWKS Received by: LB 08/06/12 12:30 Rush Request: 24 Hour Analyzed by: see"By"below P.O.#: Laboratory Data SDG ID: GBC50477 Phoenix ID: BC50479 Project ID: 560 NUTMEG Client ID: EAST RL! Parameter Result PQL Units Date/Time By Reference Percent Solid 79 % 08/06/12 JL E160.3 Aromatic Volatiles 1,2,3-Trichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trichlorobenzene ND 5.3 ug/Kg 08/06/12 RIJ SW8021/8260 1,2,4-Trimethylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,2-Dichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,3,5-Trimethylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,3-Dichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,4-Dichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Benzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Chlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Ethylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Isopropylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 m&p-Xylene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Methyl t-butyl ether(MTBE) ND 11 ug/Kg 08/06/12 R/J SW8021/8260 Naphthalene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 n-Butylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 n-Propylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 o-Xylene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 p-Isopropyltoluene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 sec-Butylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Styrene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 tert-Butylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW802118260 Toluene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Total Xylenes ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 QA/QC Surrogates % 104 % 08/06/12 R/J 70-130 1,2-dichlorobenzene-d4 %Bromofluorobenzene 80 % 08/06112 R/J 70-130 Page 5 of 10 Ver 1 Project ID: 560 NUTMEG Phoenix I.D.: BC50479 Client ID: EAST RL/ Parameter Result PQL Units Date/Time By Reference %Dibromofluoromethane 105 % 08/06/12 R/J 70-130% %Toluene-d8 97 % 08/06/12 R/J 70-130% RL/PQL=Reporting/Pratical Quantitation Level ND=Not Detected BRL=Below Reporting Level Comments: All soils and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If there are any questions regarding this data,please call Phoenix Client Services at extension 200. This report must not be reproduced except in full as defined by the attached chain of custody. Phyllis hiller,Laboratory Director August 08,2012 Reviewed and Released by:Johanna Harrington,Project Manager Page 6 of 10 Ver 1 j .............. Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Mrs. Rose Rainville Tankworks Removal& Replacement, LLC August 08, 2012 360 East Center Street Manchester, CT 06040 Sample Information Custody Information Date Time Matrix: SOIL Collected by: 08/06/12 0:00 Location Code: TANKWKS Received by: LB 08/06/12 12:30 Rush Request: 24 Hour Analyzed by: see"By"below P.O.#: Laboratory Data SDG ID: GBC50477 Phoenix ID: BC50480 Project ID: 560 NUTMEG Client ID: WEST RL/ Parameter Result PQL Units Date/Time By Reference Percent Solid 90 % 08/06/12 JL E160.3 Aromatic Volatiles 1,2,3-Trichlorobenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trichlorobenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trimethylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 1,2-Dichlorobenzene ND 4.6 ug/Kg 08/06/12 R/J SW802118260 1,3,5-Trimethylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 1,3-Dichlorobenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 1,4-Dichlorobenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Benzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Chlorobenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Ethylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Isopropylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 m&p-Xylene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Methyl t-butyl ether(MTBE) ND 9.2 ug/Kg 08/06/12 R/J SW802118260 Naphthalene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 n-Butylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 n-Propylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 o-Xylene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 p-Isopropyltoluene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 sec-Butylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Styrene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 tert-Butylbenzene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Toluene ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 Total Xylenes ND 4.6 ug/Kg 08/06/12 R/J SW8021/8260 QAIQC Surrogates %1,2-dichlorobenzene-d4 99 % 08/06/12 R/J 70-130% %Bromofluorobenzene 88 % 08/06/12 R/J 70-130% Page 7 of 10 Ver 1 Project ID: 560 NUTMEG Phoenix I.D.: BC50480 Client ID: WEST RL/ Parameter Result PQL Units Date/Time By Reference %Dibromofluoromethane 101 % 08/06/12 R/J 70-130% %Toluene-d8 98 % 08/06/12 R/J 70-130% RL/PQL=Reporting/Pratical Qua ntitation Level ND=Not Detected BRL=Below Reporting Level Comments: All soils and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If there are any questions regarding this data,please call Phoenix Client Services at extension 200. This report must not be reproduced except in full as defined by the attached chain of custody. Phyllis hiller,Laboratory Director August 08,2012 Reviewed and Released by:Johanna Harrington,Project Manager �I Page 8 of 10 Ver 1 T P110EIN Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Mrs. Rose Rainville Tankworks Removal &Replacement, LLC August 08, 2012 360 East Center Street Manchester, CT 06040 Sample Information Custody Information Date Time Matrix: SOIL Collected by: 08/06/12 0:00 Location Code: TANKWKS Received by: LB 08/06/12 12:30 Rush Request: 24 Hour Analyzed by: see"By"below P.O.#: Laboratory Data SDG ID: GBC50477 Phoenix ID: BC50481 Project ID: 560 NUTMEG Client ID: BOTTOM RL/ Parameter Result PQL Units Date/Time By Reference Percent Solid 79 °% 08/06/12 JL E160.3 Aromatic Volatiles 1,2,3-Trichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,2,4-Trimethylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,2-Dichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW802118260 1,3,5-Trimethylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,3-Dichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 1,4-Dichlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Benzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Chlorobenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Ethylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW802118260 Isopropylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 m&p-Xylene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Methyl t-butyl ether(MTBE) ND 11 ug/Kg 08/06/12 R/J SW8021/8260 Naphthalene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 n-Butylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW802118260 n-Propylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 o-Xylene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 p-Isopropyltoluene ND 5.3 ug1Kg 08/06/12 R/J SW8021/8260 sec-Butylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Styrene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 tert-Butylbenzene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Toluene ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 Total Xylenes ND 5.3 ug/Kg 08/06/12 R/J SW8021/8260 QA/QC Surrogates %1,2-dichlorobenzene-d4 102 % OS/06/12 R/J 70-130 %Bromofluorobenzene 85 % 08/06/12 R/J 70-130% Page 9 of 10 Ver 1 PHOEATV Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 QA/QC Report August 08, 2012 QA/QC Data SDG I.D.: GBC50477 LCS LCSD LCS MS MSD MS Rec RPD Parameter Blank % % RPD % % RPD Limits Limits QA/QC Batch 206552,QC Sample No:BC50353(BC50477,BC50478,BC50479,BC50480,BC50481) Volatiles-Soil 1,2,3-Trichlorobenzene ND 111 102 8.5 88 91 3.4 7o-13t1 30 1,2,4-Trichlorobenzene ND 119 106 11.6 92 95 3.2 70-130 30 30105 97 7.9 99 94 5.2 70-130 3 1,2,4-Trimethylbenzene ND 1,2-Dichlorobenzene ND 99 97 2.0 92 94 2.2 70-130 30 1,3,5-Trimethylbenzene ND 105 97 7.9 99 93 6.3 70-130 30 1,3-Dichlorobenzene ND 104 97 7.0 93 93 0.0 70-130 30 1,4-Dichlorobenzene ND 104 97 7.0 93 93 0.0 70-130 30 Benzene ND 95 91 4.3 93 87 6.7 70-130 30 Chlorobenzene ND 97 94 3.1 95 93 2.1 70-130 30 Ethylbenzene ND 101 97 4.0 99 94 5.2 70-130 30 Isopropylbenzene ND 102 93 9.2 101 92 9.3 70-130 30 m&p-Xylene ND 102 96 6.1 101 95 6.1 70-130 30 Methyl t-butyl ether(MTBE) ND 75 94 22.5 71 89 22.5 70-130 30 Naphthalene ND 102 90 12.5 88 85 3.5 70-130 30 n-Butylbenzene ND 112 96 15.4 104 94 10.1 70-130 30 n-Propylbenzene ND 100 92 8.3 102 93 9.2 70-130 30 o-Xylene ND 102 98 4.0 101 97 4.0 70-130 30 p-Isopropyltoluene ND 112 100 11.3 103 95 8.1 70-130 30 sec-Butylbenzene ND 100 91 9.4 103 93 10.2 70-130 30 Styrene ND 103 100 3.0 95 96 1.0 70-130 30 tert-Butylbenzene ND 101 92 9.3 101 93 8.2 70-130 30 Toluene ND 96 93 3.2 94 88 6.6 70-130 30 •1,2-dichlorobenzene-d4 103 99 100 1.0 99 101 2.0 70-130 30 •Bromofluorobenzene 94 93 97 4.2 96 97 1.0 70-130 30 %Dibromofluoromethane 108 100 101 1.0 101 99 2.0 70-130 30 %Toluene-d8 99 99 100 1.0 99 98 1.0 70-130 30 Comment: Additional 8260 criteria:10%of compounds can be outside of acceptance criteria as long as recovery is 40-160%. If there are any questions regarding this data,please call Phoenix Client Services at extension 200. RPD-Relative Percent Difference LCS-Laboratory Control Sample LCSD-Laboratory Control Sample Duplicate MS-Matrix Spike Phylli Shiller, Laboratory Director MS Dup-Matrix Spike Duplicate Augu t 08,2012 NC-No Criteria Intf-Interference Page 1 of 1