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HomeMy WebLinkAboutWell Inspection 143 Oakland Road (3) • r --� Groundwater L%N 1 -916 1% RECEIVED V & Environmental Services, Inc. 425E Hayden Station Road • Windsor,CT 06095 • Tel(860)688-9023 • Fax(860)688-9278 'JUL 102008 July 8,2008 Ms. Melissa Barton 143 Oakland Road South Windsor,CT 06074 Re: Potable Well Sampling Information 143 Oakland Road South Windsor, CT 06074 Dear Ms. Barton, On behalf of ExxonMobil Oil Corporation, Groundwater and Environmental Services (GES), ExxonMobil's consultant, would like to thank you for allowing GES to conduct sampling of your drinking water well on May 23, 2008. The water sample from your well was tested for the presence of a number of volatile organic compounds found in gasoline, including methyl tertiary butyl ether (MTBE). For your information, the tests were conducted utilizing Environmental Protection Agency (EPA) approved methods and a copy of the laboratory report is enclosed. The laboratory results indicate no presence of MTBE or any other compound found in gasoline in your well water. As you know, the tests conducted on your drinking water well are part of an ongoing groundwater investigation being conducted in cooperation with the Connecticut Department of the Environmental Protection (CT DEP). Please note; the sampling frequency of your well, as requested by the CT DEP, is quarterly. Therefore,the next sampling event is scheduled for August 2008. Again,thank you for your patience and cooperation. If you have any questions regarding the test results or the investigation in the area,please feel free to call the toll free ExxonMobil Information Line at 1-877-346-0302 or, if you prefer, we suggest you contact Kevin Neary with the DEP at 860-424-3947 or Robert Deptula, the Environmental Health Officer for the Town of South Windsor, at 860-644-2511 ext. 248. Sinc re y, Sohn D. Mo s -l—dr- Karen L. Harris Project Manager Senior Project Manager Enclosure cc: Kevin Neary-Connecticut Department of the Environmental Protection Robert Deptula-Town of South Windsor C. Fredrick Shaw-Town of South Windsor Jeff Folger-Town of South Windsor Walter Summers-Fire Marshal Town of South Windsor Environmental Solutions and Liability Management e-Ilardeolpy 2.0 .Autorrruted RiTort New England t,.r. �. a r°� ALL IN rfit CrzEMas'rrty 06/16/08 Technical Report for ExxonMobil GESCT:01-QQA 249 Oakland Rd., South Windsor CT PO#4509333735 WBS#08 Accutest Job Number: M73758 Sampling Date: 05/23/08 Report to: Groundwater & Environmental Services JMoss@gesonline.com ATTN: John Moss Total number of pages in report: 2 "O 1N ACCo,,,0 # • . Test results contained within this data package meet the requirements ZIa and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y E �1 $w� NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com 012 1 of 20 12 M73758 ' . �������� r���0 � �� Table ��� ��A���te��ts _"_ Section1: Sample Summary ......,...........,....,^..,,,.....^...,...^^.,,.......,,,.,.,.^...,,,,,,,,,,^,^,,,,^,,^,,,,,,,,^^, 3 N�N� Section2: Cmse Narrative/Conformance Smmommary ....,..,..,.~......~~~.,..~,.~~.~~~.~,,~^.~~....~~. 4 Section3. Sample Results .~~^~'.^~........ ....~~,~,,~~,-~~~~~~^^^,~,,.~,,~,..~,,. .^,,,,~,.~,~,,,~,~~,,,~''^ 5 11. M73758-1: 143/151 OAKI.ANI) ROAD —.--.---------.----------. 6 Section4: Misc. Forms ............................................................................................................ 0 4.1: Chain of Custody ----------------.---'—.--------------. g ---- 4.2: RCP Fnzoz 11 4.3^ 8nn`n�' Chronicle ' . --'r'- �ru:u�n� c -------------------.----------- 12 Section 5` ���/8�� �������� ��� l� t Summaries . - �_ o � ...,.......~~,...,.,~...~..~..~.....,.,..~,,,,,....^, 13 5.8: Method Blank Summary ................................................................................................ 14 5^ , _r-_e�` ]��z��AnJ, Snuoo Summary ................................................................................................... 16 5~3- Duplicate Sluomazy ---------.------.—..---.------.------- 18 5'4z Surrogate Recovery 8nozozmica ----------------------------. 20 all 2 of 20 M73758 Ac cutest Laboratories Sample Summary ExxonMobil GESCT:01-QQA 249 Oakland Rd., South Windsor CT Job No: M73758 Project No: PO#4509333735 WBS#08 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M73758-1 05/23/08 08:45 KGA 05/27/08 DW Drinking Water 143/151 OAKLAND ROAD ® 3 of 20 ®ACCtJ'>msT. ......... ... .. ..... .. M73758 a '• - -, --..._._.._....... SAMPLE DELIVERY GROUP CASE NARRATIVE Client: ExxonMobil Job No M73758 Site: GESCT:01-QQA 249Oakland Rd.,South Windsor CT Report Date 6/14/2008 12:09:58 PM I Sample was collected on 05/23/2008 and were received at Accutest on 05/27/2008properly preserved,at 3.4 Deg.C and intact. These Samples received an Accutest job number of M73758.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method EPA 524.2 REV 4.1 Matrix AQ Batch ID: MSR191 a All method blanks for this batch meet method specific criteria. Sample(s) M73920-1 DUP were used as the QC samples indicated. Blank Spike Recovery(s)for 1,1-Dichloro ethane, 1,1-Dichloropropene,1,2-Dichloroethane, 1,2-Dichloropropane,2,2- Dichloropropane,Benzene,Chloroethane,Chloroform,Chloromethane,cis-1,2-Dichloro ethylene,trans-1,2-Dichloroethylene,trans- 1,3-Dichloropropene are outside control limits. Associated samples are non-detect for this compound. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M73758). Saturday,June 14,2008 Page I of I MEJ 4 of 24 M73758 :.�. . —......, New England - QAOO r., sectimi ...__......._. Sample Results Report of Analysis ® 5 of 2.0 M73758 Accutest Laboratories Report of Analysis Page I oft Client Sample ID: 143/151 OAKLAND ROAD Lab Sample ID: M73758-1 Date Sampled: 05/23/08 Matrix: DW-Drinking Water Date Received: 05/27/08 Method: EPA 524.2 REV 4.1 Percent Solids: n/a Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R5004.1) 1 06/06/08 AA n/a n/a MSR191 Run#2 Purge Volume Run#1 5.0 ml Run#2 VOA List CAS No. Compound Result MCL RL Units Q 71-43-2 Benzene ND 5.0 0.50 ug/1 108-86-1 Bromobenzene ND 0.50 ug/I 74-97-5 Bromochloromethane ND 0.50 ug/I 75-27-4 Bromodichloromethane ND 0.50 ug/1 75-25-2 Bromoform ND 0.50 ug/I 74-83-9 Bromomethane ND 0.50 ug/1 104-51-8 n-Butylbenzene ND 0.50 ug/I 135-98-8 sec-Butylbenzene ND 0.50 ug/I 98-06-6 tert-Butylbenzene ND 0.50 ug/I 108-90-7 Chlorobenzene ND 100 0.50 ug/1 75-00-3 Chloroethane ND 0.50 ug/I 67-66-3 Chloroform ND 0.50 ug/I 74-87-3 Chloromethane ND 0.50 ug/1 95-49-8 o-Chlorotoluene ND 0.50 ug/I 106-43-4 p-Chlorotoluene ND 0.50 . ug/I 56-23-5 Carbon tetrachloride ND 5.0 0.50 ug/1 75-34-3 1,1-Dichloroethane ND 0.50 ug/l 75-35-4 1,1-Dichloroethylene ND 7.0 0.50 ug/1 563-58-6 1,1-Dichloropropene ND 0.50 ug/I 96-12-8 1,2-Dibromo-3-chloropropane ND 0.20 0.50 ug/I 106-93-4 1,2-Dibromoethane ND 0.050 0.50 ug/I 107-06-2 1,2-Dichloroethane ND 5.0 0.50 ug/I 78-87-5 1,2-Dichloropropane ND 5.0 0.50 ug/I 142-28-9 1,3-Dichloropropane ND 0.50 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 ug/I 124-48-1 Dibromochloromethane ND 0.50 ug/I 74-95-3 Dibromomethane ND 0.50 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 ug/1 10061-01-5 cis-1,3-Dichloropropene ND 0.50 ug/I 541-73-1 m-Dichlorobenzene ND 0.50 ug/I 95-50-1 o-Dichlorobenzene ND 600 0.50 ug/I 106-46-7 p-Dichlorobenzene ND 75 0.50 ug/1 ND = Not detected J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 141) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 6 of 20 QACCLffEST M73758 ,.1 1 . -..-.. ., Accutest Laboratories Report of Analysis Page 2 of 2 Client Sample ID: 143/151 OAKLAND ROAD Lab Sample ID: M73758-1 Date Sampled: 05/23/08 Matrix: DW-Drinking Water Date Received: 05/27/08 Method: EPA 524.2 REV 4.1 Percent Solids: n/a Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT VOA List CAS No. Compound Result MCL RL Units Q 156-60-5 trans-1,2-Dichloroethylene ND 100 0.50 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 70 0.50 ug/1 10061-02-6 trans-1,3-Dichloropropene ND 0.50 ug/I 100-41-4 Ethylbenzene ND 700 0.50 ug/1 87-68-3 Hexachlorobutadiene ND 0.50 ug/1 98-82-8 Isopropylbenzene ND 0.50 ug/I 99-87-6 p-Isopropyltoluene ND 0.50 ug/1 75-09-2 Methylene chloride ND 5.0 0.50 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/I 91-20-3 Naphthalene ND 0.50 ug/1 103-65-1 n-Propylbenzene ND 0.50 ug/I 100-42-5 Styrene ND 100 0.50 ug/I 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/1 71-55-6 1,1,1-Trichloroethane ND 200 0.50 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ug/I 79-00-5 1,1,2-Trichloroethane ND 5.0 0.50 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 ug/I 120-82-1 1,2,4-Trichlorobenzene ND 70 0.50 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/1 127-18-4 Tetrachloroethylene ND 5.0 0.50 ug/1 108-88-3 Toluene ND 1000 0.50 ug/1 79-01-6 Trichloroethylene ND 5.0 0.50 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 ug/1 75-01-4 Vinyl chloride ND 2.0 0.50 ug/1 m,p-Xylene ND 0.50 ug/1 95-47-6 o-Xylene ND 0.50 ug/1 1330-20-7 Xylenes (total) ND 10000 0.50 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits 2199-69-1 1,2-Dichlorobenzene-d4 103% 70-130% 460-00-4 4-Bromofluorobenzene 87% 70-130% ND = Not detected J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 141) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® 7 of 20 UACCXJ 7C1EST M73768 New England T' woos .> Section 4 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: Chain of Custody • RCP Form • Sample Tracking Chronicle Ell 8 of 20 QACXNJTEST M73758 :. . C"N OF CUSTODY 495 Tech Center Wes%Bldg.I Madbom,MA 01752 732-329-0200 FAX:732.329-349913480 Aoe—N be A 73 7-94 ill4f4ffilif0lent Reporting Information WAII Facilitv Infomre8on Ana al Infonmtion EXXONMOBIL CORPORATION-Re tonal Lab tory Program Northeast Consultants Company N.— Prgecl Ila— - Groundwater&Environmental Services Inc.-WNE Mobil-S.Windsor#01-OQA Address Slnet 425 B Hayden Station Road 249 Oakland Road City 3W. ZIP City 3.w �► Windsor Conncecticut 06095 South Windsor CT Protect Coltten: E•mall ExxonMobll ConlacL• J. gtsonline Ma Caruso Samplers'e Name ✓ � EmmMebll Correct Phone#(609)586.4071 Phms• Fare L-11.108 Was# 800 220-6119 860 688-9278 01-QOA AFES Pot U-S ACCulest Collaction Preservation �w Sample# ad + a 3 Field ID/Point of Collection Dale Time sam d b Mebix bolses R 1431151 Oakland Road 'j"Z3 A 9. Tumammld Time audnese da -Data D811vemNe Iniom laon "i9i Cpm n /R—ft ®Std.10 WmlM s Days APp..d Sy:t 0a: Commercial W FULL CLP B Day RUSH El Ca—.f.l•e' NYASP Category A Please follow RCP protocol for a GA groundwater classification S Day RUSH NJ Redueed NYASP Coto,,a a Day EMERGENCY NJ WH State Fonns 2 Day EMERGENCY lythar EDD Fonn,t I©^1 Day EMERGENCY Omer C--rcW*A-Results Only Emergency T/A data available VIA Lablink Sample C tOdY mutt be documented below each rims samples than a pose ssion,including courier dolNory. N O� 3. «. r: 4 5 °" y; S vrw r M73758: Chain of Custody 'age f of 2 ® 9 of 20 12ACCUTESTe _._.... M73758 - . • -....—., J* PROJECT COMMUNICATION FORM Client Name: ExxonMobil Protect Name:South Windsor Protect Number:01-QQA Protect Manaser:John Moss Contact Info:(800)220-6119 x3540 FleldManazer: Sample Matria: ❑groundwater or surface water,❑soil,❑sediment,X drinking water,❑air,❑other Constituents of Concern:Please note any known or suspected contaminants in high concentrations or any non-standard analytes not contained in routine target lists(see notes). BTEX Reeulatory Criteria: ❑Residential Direct Exposure Criteria,❑Industrial/Cotnmercial Direct Exposure Criteria, ❑GA Pollutant Mobility Criteria,❑GB Pollutant Mobility Criteria,❑Other: ❑Groundwater Protection Criteria,❑Surface Water Protection Criteria,❑Aquatic Life Criteria(specify applicable criteria below)X Other: EPA MCL's;CTDPH Action Levels Quality Control Requirements:Indicate if your project will have Project specific field quality control samples.Check all that apply.Also spec!if special QAIQC site requirements exist:i.e.,QAPP ❑Matrix Spike,❑Matrix Spike Duplicate,X Trip Blank(s), ❑Other Field QC: ❑Project QAPP(send appropriate section(s)to lab) Report Deliverables Requirements:Indicate any reporting requirements other than routine lab data sheets such as electronicformats: ❑Excel Tables,❑GISKey,❑Envirodata,X GES Format,X RCP,0Other: Expected Sampling Date(s):Indicate expected number ofsampling events or duration J May,August,November Total Number of Samples and Expected Sample Load Per Day:(indicate number of each matrix if applicable) 1 Sample Pick Up: X office(s),❑site(address),[]other Special Instructions: ❑ Report TICS ® t� kv Notes: Ifreauestin¢non-routine compounds that have no regulatory criteria indicate required re�orli� C limit for each compound a Reasonable Confidence Protocol Laboratory Analysis QA/QC Certification Form N Laboratory Name: Accutest New England Client: ExxonMobil Project Location: GESCT:01-QQA 249 Oakland Rd.,South project Number: p0#4509333735 WBS#08 Windsor CT Sampling Date(s): 5/23/2008 Laboratory Sample ID(s): M73758-1 Methods: EPA 524.2 REV 4.1 For each analytical method referenced in this laboratory report package, were all specified QA/QC performance criteria followed,including the requirement to explain any 1 criteria falling outside of acceptable guidelines,as specified in the CTDEP method- Yes No i= specific Reasonable Confidence Protocol documents)? 1A Where all the method specified preservation and holding time requirments met? Yes 2! No I" 1 B VPH and EPH mehods only: Was the VPH or EPH method conducted without Yes E No significant modifications (See section 11.3 of respective methods) NA r 2 Were all samples received by the laboratory in a condition consistent with that described on the associated chain-of-custody document(s)? Yes 171 No 3 Were samples received at an appropriate temperature(<6°C)? Yes 1= No 4 Were all QA/QC performance criteria specified in the CTDEP Reasonable r Confidence Protocol documents achieved? Yes No 5 a)Were reporting limits specified or referenced on the chain-of-custody? Yes No b)Were these reporting limits met? Yes l- No For each analytical method referenced in this laboratory report package, 6 were results reported for all constituents identified in the method-specific Yes t° No analyte lists presented in the Reasonable Confidence Protocol documents? 7 Are project-specific matrix spikes and laboratory duplicates included in this data set? Yes -� No Note: For all questions to which the response was"No"(with the exception of question#7),additional information must be provided in an attached narrative. If the answer to question#1,#1A or#1B is"No",the data package does not meet the requirements for"Reasonable Confidence". I,the undersigned,attest under pains and penalties of perjury that,to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report,such information is accurate and complete. Authorized , Signature: /��_ �/ Position: Lab Director Printed Name: Reza Tend / ` Date: 6/14/2008 Accutest New England 11 of 20 ®ACCNN T ........................................ M73758 Accutest Laboratories Internal Sample Tracking Chronicle W ExxonMobil GESCT:01-QQA 249 Oakland Rd., South Windsor CT Job No: M73758 Project No: PO#4509333735 WBS#08 Sample Number Method Analyzed By Prepped By Test Codes M73758-1 Collected: 23-MAY-08 0845 By''€ KGA Received: 27-MAY-08 By: 143/151 OAKLAND ROAD M73758-1 EPA 524.2 REV 4.1 06-JUN-08 18:46 AA V524STD Page 1 of 1 om ® 12 of 20 ACt".,UTEST. M73758 0.. New England j2AC -- - M a, 0 Section 5 i 'S ALL If3 THt Chem sTAY GC/MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ® 13 of 20 QAC T. M73758 = Method Blank Summary Page 1 of 2 Job Number: M73758 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-MB R5000.1) 1 06/06/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73758-1 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 0.50 ug/1 108-86-1 Bromobenzene ND 0.50 ug/1 74-97-5 Bromochloromethane ND 0.50 ug/I 75-27-4 Bromodichloromethane ND 0.50 ug/1 75-25-2 Bromoform ND 0.50 ug/1 74-83-9 Bromomethane ND 0.50 ug/1 104-51-8 n-Butylbenzene ND 0.50 ug/I 135-98-8 sec-Butylbenzene ND 0.50 ug/1 98-06-6 tert-Butylbenzene ND 0.50 ug/1 108-90-7 Chlorobenzene ND 0.50 ug/I 75-00-3 Chloroethane ND 0.50 ug/1 67-66-3 Chloroform ND 0.50 ug/1 74-87-3 Chloromethane ND 0.50 ug/1 95-49-8 o-Chlorotoluene ND 0.50 ug/I 106-43-4 p-Chlorotoluene ND 0.50 ug/1 56-23-5 Carbon tetrachloride ND 0.50 ug/I 75-34-3 1,1-Dichloroethane ND 0.50 ug/1 75-35-4 1,1-Dichloroethylene ND 0.50 ug/I 563-58-6 1,1-Dichloropropene ND 0.50 ug/1 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 ug/I 107-06-2 1,2-Dichloroethane ND 0.50 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 ug/I 142-28-9 1,3-Dichloropropane ND 0.50 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 ug/1 124-48-1 Dibromochloromethane ND 0.50 ug/1 74-95-3 Dibromomethane ND 0.50 ug/I 75-71-8 Dichlorodifluoromethane ND 0.50 ug/1 10061-01-5 cis-1,3-Dichloropropene ND 0.50 ug/1 541-73-1 m-Dichlorobenzene ND 0.50 ug/1 95-50-1 o-Dichlorobenzene ND 0.50 ug/1 106-46-7 p-Dichlorobenzene ND 0.50 ug/I 156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/I 10061-02-6 trans-1,3-Dichloropropene ND 0.50 ug/1 100-41-4 Ethylbenzene ND 0.50 ug/1 1211 14 of 20 ®ACCUTES'T. _.._........_.-_..___.... M73758 Method Blank Summary Page 2 of Job Number: M73758 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-MB R5000.1) 1 06/06/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73758-1 CAS No. Compound Result RL Units Q 87-68-3 Hexachlorobutadiene ND 0.50 ug/1 98-82-8 Isopropylbenzene ND 0.50 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 ug/I 75-09-2 Methylene chloride ND 0.50 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/1 91-20-3 Naphthalene ND 0.50 ug/I 103-65-1 n-Propylbenzene ND 0.50 ug/1 100-42-5 Styrene . ND 0.50 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/1 71-55-6 1,1,1-Trichloroethane ND 0.50 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ug/1 79-00-5 1,1,2-Trichloroethane ND 0.50 ug/I 87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 ug/I 120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/1 95-63 6 1,2,4-Trimethylbenzene ND 0.50 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/I 127-18-4 Tetrachloroethylene ND 0.50 ug/1 108-88-3 Toluene ND 0.50 ug/I 79-01-6 Trichloroethylene ND 0.50 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 ug/I 75-01-4 Vinyl chloride ND 0.50 ug/I m,p-Xylene ND 0.50 ug/I 95-47-6 o-Xylene ND 0.50 ug/I 1330-20-7 Xylenes (total) ND 0.50 ug/1 CAS No. Surrogate Recoveries Limits 2199-69-1 1,2-Dichlorobenzene-d4 96% 70-130% 460-00-4 4-Bromofluorobenzene 82% 70-130% CAS No. Tentatively Identified Compounds R.T. Est. Cone. Units Q Total TIC, Volatile 0 ug/I 15of20 QACCUTEST M73758 Blank Spike Summary Page 1 of 2 Job Number: M73758 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-BS R4998.1) 1 06/06/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73758-1 Spike BSP BSP CAS No. Compound ug/l ug/1 % Limits 71-43-2 Benzene 5 7.3 146*a 70-130 108-86-1 Bromobenzene 5 4.8 96 70-130 74-97-5 Bromochloromethane 5 5.7 114 70-130 75-27-4 Bromodichloromethane 5 5.8 116 70-130 75-25-2 Bromoform 5 4.3 86 70-130 74-83-9 Bromomethane 5 5.8 116 70-130 104-51-8 n-Butylbenzene 5 5.7 114 70-130 135-98-8 sec-Butylbenzene 5 5.5 110 70-130 98-06-6 tert-Butylbenzene 5 5.4 108 70-130 108-90-7 Chlorobenzene 5 5.6 112 70-130 75-00-3 Chloroethane 5 7.1 142* a 70-130 67-66-3 Chloroform 5 6.8 136* a 70-130 74-87-3 Chloromethane 5 7.4 148* a 70-130 95-49-8 o-Chlorotoluene 5 5.7 114 70-130 106-43-4 p-Chlorotoluene 5 5.7 114 70-130 56-23-5 Carbon tetrachloride 5 5.9 118 70-130 75-34-3 1,1-Dichloroethane 5 7.6 152*a 70-130 75-35-4 1,1-Dichloroethylene 5 6.3 126 70-130 563-58-6 1,1-Dichloropropene 5 6.9 138* a 70-130 96-12-8 1,2-Dibromo-3-chloropropane 5 5.3 106 70-130 106-93-4 1,2-Dibromoethane 5 5.2 104 70-130 107-06-2 1,2-Dichloroethane 5 6.6 132*a 70-130 78-87-5 1,2-Dichloropropane 5 6.9 138* a 70-130 142-28-9 1,3-Dichloropropane 5 6.2 124 70-130 594-20-7 2,2-Dichloropropane 5 7.0 140*a 70-130 124-48-1 Dibromochloromethane 5 5.0 100 70-130 74-95-3 Dibromomethane 5 6.4 128- 70-130 75-71-8 Dichlorodifluoromethane 5 3.5 70 70-130 10061-01-5 cis-1,3-Dichloropropene 5 6.3 126 70-130 541-73-1 m-Dichlorobenzene 5 5.5 110 70-130 95-50-1 o-Dichlorobenzene 5 5.1 102 70-130 106-46-7 p-Dichlorobenzene 5 5.5 110 70-130 156-60-5 trans-1,2-Dichloroethylene 5 7.4 148*a 70-130 156-59-2 cis-1,2-Dichloroethylene 5 6.6 132*a 70-130 10061-02-6 trans-1,3-Dichloropropene 5 6.6 132*a 70-130 100-41-4 Ethylbenzene 5 6.0 120 70-130 IMEJ 16 of 20 ®AC CUTEST. M73758 Blank Spike Summary Page 2 of 2 Job Number: M73758 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-BS R4998.D 1 06/06/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73758-1 Spike BSP BSP CAS No. Compound ug/l ug/1 % Limits 87-68-3 Hexachlorobutadiene 5 4.1 82 70-130 98-82-8 Isopropylbenzene 5 5.6 112 70-130 99-87-6 p-Isopropyltoluene 5 5.0 100 70-130 75-09-2 Methylene chloride 5 6.4 128 70-130 1634-04-4 Methyl Tert Butyl Ether 5 6.1 122 70-130 91-20-3 Naphthalene 5 4.1 82 70-130 103-65-1 n-Propylbenzene 5 5.8 116 70-130 100-42-5 Styrene 5. 5.1 102 70-130 630-20-6 1,1,1,2-Tetrachloroethane 5 5.0 100 70-130 71-55-6 1,1,1-Trichloroethane 5 6.2 124 70-130 79-34-5 1,1,2,2-Tetrachloroethane 5 5.6 112 70-130 79-00-5 1,1,2-Trichloroethane 5 5.3 106 70-130 87-61-6 1,2,3-Trichlorobenzene 5 4.3 86 70-130 96-18-4 1,2,3-Trichloropropane 5 5.1 102 70-130 120-82-1 1,2,4-Trichlorobenzene 5 4.4 88 70-130 95-63-6 1,2,4-Trimethylbenzene 5 5.2 104 70-130 108-67-8 1,3,5-Trimethylbenzene 5 5.5 110 70-130 127-18-4 Tetrachloroethylene 5 5.5 110 70-130 108-88-3 Toluene 5 6.5 130 70-130 79-01-6 Trichloroethylene 5 6.3 126 70-130 75-69-4 Trichlorofluoromethane 5 5.2 104 70-130 75-01-4 Vinyl chloride 5 6.5 130 70-130 m,p-Xylene 10 11.7 117 70-130 95-47-6 o-Xylene 5 5.7 114 70-130 1330-20-7 Xylenes (total) 15 17.4 116 70-130 CAS No. Surrogate Recoveries BSP Limits 2199-69-1 1,2-Dichlorobenzene-d4 80% 70-130% 460-00-4 4-Bromofluorobenzene 96% 70-130% (a) Outside control limits. Associated samples are non-detect for this compound. 17 of 20 ACGt3 TEST. M73758 Duplicate Summary Page 1 of Job Number: M73758 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73920-11)UP R5018.1) 1 06/07/08 AA n/a n/a MSR191 M73920-1 R5017.1) 1 06/07/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73758-1 M73920-1 DUP CAS No. Compound ug/l Q ug/l Q RRD Limits 71-43-2 Benzene ND ND nc 30 108-86-1 Bromobenzene ND ND nc 30 74-97-5 Bromochloromethane ND ND nc 30 75-27-4 Bromodichloromethane ND ND nc 30 75-25-2 Bromoform ND ND nc 30 74-83-9 Bromomethane ND ND nc 30 104-51-8 n-Butylbenzene ND ND nc 30 135-98-8 sec-Butylbenzene ND ND nc 30 98-06-6 tert-Butylbenzene ND ND nc 30 108-90-7 Chlorobenzene ND ND nc 30 75-00-3 Chloroethane ND ND nc 30 67-66-3 Chloroform ND ND nc 30 74-87-3 Chloromethane ND ND nc 30 95-49-8 o-Chlorotoluene ND ND nc 30 106-43-4 p-Chlorotoluene ND ND nc 30 56-23-5 Carbon tetrachloride ND ND nc 30 75-34-3 1,1-Dichloroethane ND ND nc 30 75-35-4 1,1-Dichloroethylene ND ND nc 30 563-58-6 1,1-Dichloropropene ND ND nc 30 96-12-8 1,2-Dibromo-3-chloropropane ND ND nc 30 106-93-4 1,2-Dibromoethane ND ND nc 30 107-06-2 1,2-Dichloroethane ND ND nc . 30 78-87-5 1,2-Dichloropropane ND ND nc 30 142-28-9 1,3-Dichloropropane ND ND nc 30 594-20-7 2,2-Dichloropropane ND ND nc 30 124-48-1 Dibromochloromethane ND ND nc 30 74-95-3 Dibromomethane ND ND nc 30 75-71-8 Dichlorodifluoromethane ND ND nc 30 10061-01-5 cis-1,3-Dichloropropene ND ND nc 30 541-73-1 m-Dichlorobenzene ND ND nc 30 95-50-1 o-Dichlorobenzene ND ND nc 30 106-46-7 p-Dichlorobenzene ND ND nc 30 156-60-5 trans-1,2-Dichloroethylene ND ND nc 30 156-59-2 cis-1,2-Dichloroethylene ND ND nc 30 10061-02-6 trans-1,3-Dichloropropene ND ND nc 30 100-41-4 Ethylbenzene ND ND nc 30 ® 18 of 20 Q ACC1.!"?E ST, M73758 Duplicate Summary Page 2 of 2 Job Number: M73758 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73920-1DUP R5018.1) 1 06/07/08 AA n/a n/a MSR191 M73920-1 R5017.D 1 06/07/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73758-1 M73920-1 DUP CAS No. Compound ug/l Q ug/l Q RPD Limits 87-68-3 Hexachlorobutadiene ND ND nc 30 98-82-8 Isopropylbenzene ND ND nc 30 99-87-6 p-Isopropyltoluene ND ND nc 30 75-09-2 Methylene chloride ND ND nc . 30 1634-04-4 Methyl Tert Butyl Ether ND ND nc 30 91-20-3 Naphthalene ND ND nc 30 103-65-1 n-Propylbenzene ND ND nc 30 100-42-5 Styrene ND ND nc 30 630-20-6 1,1,1,2-Tetrachloroethane ND ND nc 30 71-55-6 1,1,1-Trichloroethane ND ND nc 30 79-34-5 1,1,2,2-Tetrachloroethane ND ND nc 30 79-00-5 1,1,2-Trichloroethane ND ND nc 30 87-61-6 1,2,3-Trichlorobenzene ND ND nc 30 96-18-4 1,2,3-Trichloropropane ND ND nc 30 120-82-1 1,2,4-Trichlorobenzene ND ND nc 30 95-63-6 1,2,4-Trimethylbenzene ND ND nc 30 108-67-8 1,3,5-Trimethylbenzene ND ND nc 30 127-18-4 Tetrachloroethylene 0.56 0.65 15 30 108-88-3 Toluene ND ND nc 30 79-01-6 Trichloroethylene ND ND nc 30 75-69-4 Trichlorofluoromethane ND ND nc 30 75-01-4 Vinyl chloride ND ND nc 30 m,p-Xylene ND ND nc 30 95-47-6 o-Xylene ND ND nc 30 1330-20-7 Xylenes (total) ND ND nc 30 CAS No. Surrogate Recoveries DUP M73920-1 Limits 2199-69-1 1,2-Dichlorobenzene-d4 97% 104% 70-130% 460-00-4 4-Bromofluorobenzene 98% 108% 70-130% ® 19 of 20 0ACX =.ITF"r. _.._........__.._... M73758 -.. Volatile Surrogate Recovery Summary Page I of I Job Number: M73758 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Method: EPA 524.2 REV 4.1 Matrix: AQ Samples and QC shown here apply to the above method cn Lab Lab Sample ID File ID S1 S2 M73758-1 R5004.D 103.0 87.0 M73920-1-DUP R5018.1) 97.0 98.0 MSR191-BS R4998.1) 80.0 96.0 MSR191-MB R5000.1) 96.0 82.0 Surrogate Recovery Compounds Limits Sl = 1,2-Dichlorobenzene-d4 70-130% S2 = 4-Bromofluorobenzene 70-130% ® 20 of 20 rI,ACXAJ....... ....._...._.._.... M7375&