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HomeMy WebLinkAboutWell Inspection 291 Oakland Road IN Groundwater J & Environmental Services, Inc. 425B Hayden Station Road • Windsor, CT 06095 • Tel(860)688-9023 • Fax(860)688-9278 July 8, 2008 Mr. Richard Burrill Wapping Shopping Center,LLC 52 Tallwood Drive South Windsor, CT 06074 Re: Potable Well Sampling Information 291C and 291D Oakland Road(also known as 287C and 297DC, respectively) South Windsor, CT 06074 Dear Mr. Burrill, On behalf of ExxonMobil Oil Corporation; Groundwater and Environmental Services (GES), ExxonMobil's consultant, would like to thank you for allowing GES to conduct sampling of your drinking water wells on May 23, 2008. The water samples from your wells were tested for the presence of a number of volatile organic compounds found in gasoline, including methyl tertiary butyl ether (MTBE). For your information, the tests were conducted utilizing Environmental Protection Agency (EPA) approved methods and a copy of the laboratory report is enclosed. The laboratory results indicate no presence of MTBE or any other compound found in gasoline in your well water. As you know, the tests conducted on your drinking water well are part of an ongoing groundwater investigation being conducted under the direction of the Connecticut Department of the Environmental Protection (CT DEP). Please note; the sampling frequency of your well, as requested by the CT DEP, is quarterly. Therefore,the next sampling event is scheduled for August 2008. Again, thank you for your patience and cooperation. If you have any questions regarding the test results or the investigation in the area or if you notice changes in the taste, smell or appearance of your water, please feel free to call the toll free ExxonMobil Information Line at 1-877-346-0302 or, if you prefer, we suggest you contact Kevin Neary with the DEP at 860-424-3947 or Robert Deptula, the Environmental Health Officer for the Town of South Windsor, at 860-644-2511 ext. 248. Sin erely, John D.Moss ar—Karen L. Harris Project Manager Senior Project Manager Enclosure cc: Kevin Neary- Connecticut Department of the Environmental Protection Robert Deptula-Town of South Windsor C. Fredrick Shaw-Town of South Windsor Jeff Folger-Town of South Windsor Walter Summers-Fire Marshal Town of South Windsor Environmental Solutions and Liability Management e- lardcopy Z 0 Automated.Repos t New England uAcCUTIF-a-r. 40 0 .. s�•t ALL IN rKe Ctt�MaSTAY 06/16/08 Technical Report for ExxonMobil GESCT:01-QQA 249 Oakland Rd., South Windsor CT y PO#4509333735 WBS#08 Accutest Job Number: M73763 Sampling Date: 05/23/08 Report to: Groundwater & Environmental Services JMoss@gesonline.com ATTN: John Moss Total number of pages in report: 22 1N ACCpR4gyC� • + ti • Test results contained within this data package meet the requirements /ea and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) WYE R NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE a� Vr9 This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. ti::oi� Test results relate only to samples analyzed. New England • 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com ® 1 of 22 ®xl►►CCUTES-. M73763 . . Sections: ��=�Q � �� Table of 4- Section1: Sample Summary ..................,..............~~..,.........,.,.....~.........,,............................. 3 Section2: Case Na Summary .............................................................. 4 Section 3: Sample Results ~~~. _~~~~~,,,^~~~.~~~~,..... 5 3.1: M73763-1: 29lCOAKl.AN0D ROAD .......................................................................... 6 3'2: M73763-2: 2glDOAKLANDROAD ------------------------. 8 Section4: Misc. Forms ............................................................................................................ 10 4~k: Chain of —.—'------------'-------------------.. ll 0�&� _-__-' 4.2: RCP F000 .----------.----------------------------- 13 4,3: Sample Tracking Chrouinle -----.—.--.---------'----------- 14 Section 5; GCJMSV0latiles - QCData Sum0maries ..,. ...... ...... ........................................... 15 5.1: Method Blank Summary -----------.------.----------.---.. 16 5.2: Blank Spike Summary --------------------------------- 18 5^3: Duplicate Summary -----------------------------.--.--.. 20 5.4: Surrogate Recovery @ooumaries -------.--------------------- 22 Mnro Accutest Laboratories Sample Summary ExxonMobil Job No: M73763 GESCT:01-QQA 249 Oakland Rd., South Windsor CT Project No: PO#4509333735 WBS#08 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M73763-1 05/23/08 09:55 KGA 05/27/08 DW Drinking Water 291C OAKLAND ROAD. M73763-2 05/23/08 10:55 KGA 05/27/08 DW Drinking Water 291D OAKLAND ROAD ® 3 of 22 UAC CLiTEST' M73763 Lat> v " trter- cs SAMPLE DELIVERY GROUP CASE NARRATIVE Client: ExxonMobil Job No M73763 Site: GESCT:01-QQA 249Oakland Rd.,South Windsor CT Report Date 6/14/2008 12:02:54 PM 2 Sample(s)were collected on 05/23/2008 and were received at Accutest on 05/27/2008 properly preserved,at 3.4 Deg.C and intact. These Samples received an Accutestjob number of M73763.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method EPA 524.2 REV 4.1 Matrix AQ Batch ID: MSR191 U All method blanks for this batch meet method specific criteria. Sample(s) M73920-1DUP were used as the QC samples indicated. Blank Spike Recovery(s)for 1,1-Dichlo ro ethane, 1,1-Dichloropropene,1,2-Dichloroethane, 1,2-Dichloropropane,2,2- Dichloropropane,Benzene,Chloroethane,Chloroform,Chloromethane,cis-1,2-Dichloro ethylene,trans-1,2-Dichloroethylene,trans- 1,3-Dichloropropene are outside control limits. Associated samples are non-detect for this compound. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M73763} Saturday,June 14,2008 Page 1 of 1 ® 4of22 MA .UTESr __............_..__........ ._ M73763 -.... ., ® New England e Sample Results Report of Analysis 5 of 22 A� a"T; M73763 :. . Accutest Laboratories Report of Analysis Page 1 of 2 Client Sample ID: 291C OAKLAND ROAD Lab Sample ID: M73763-1 Date Sampled: 05/23/08 Matrix: DW- Drinking Water Date Received: 05/27/08 Method: EPA 524.2 REV 4.1 Percent Solids: n/a Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R5008.1) 1 06/06/08 AA n/a n/a MSR191 Run#2 Purge Volume Run#1 5.O ml Run#2 VOA List CAS No. Compound Result MCL RL Units Q 71-43-2 Benzene ND 5.0 0.50 ug/I 108-86-1 Bromobenzene ND 0.50 ug/I 74-97-5 Bromochloromethane ND 0.50 ug/I 75-27-4 Bromodichloromethane ND 0.50 ug/1 75-25-2 Bromoform ND 0.50 ug/1 74-83-9 Bromomethane ND 0.50 ug/I 104-51-8 n-Butylbenzene ND 0.50 ug/1 135-98-8 sec-Butylbenzene ND 0.50 ug/I 98-06-6 tert-Butylbenzene ND 0.50 ug/I 108-90-7 Chlorobenzene ND 100 0.50 ug/1 75-00-3 Chloroethane ND 0.50 ug/1 .67-66-3 Chloroform ND 0.50 ug/1 74-87-3 Chloromethane ND 0.50 ug/1 95-49-8 o-Chlorotoluene ND 0.50 ug/I 106-43-4 p-Chlorotoluene ND 0.50 ug/I 56-23-5 Carbon tetrachloride ND 5.0 0.50 ug/I 75-34-3 1,1-Dichloroethane ND 0.50 ug/i 75-35-4 1,1-Dichloroethylene ND 7.0 0.50 ug/1 563-58-6 1,1-Dichloropropene ND 0.50 ug/1 96-12-8 1,2-Dibromo-3-chloropropane ND 0.20 0.50 ug/1 106-93-4 1,2-Dibromoethane ND 0.050 0.50 ug/1 107-06-2 1,2-Dichloroethane ND 5.0 0.50 ug/1 78-87-5 1,2-Dichloropropane ND 5.0 0.50 ug/I 142-28-9 1,3-Dichloropropane ND 0.50 ug/I 594-20-7 2,2-Dichloropropane ND 0.50 ug/l 124-48-1 Dibromochloromethane ND 0.50 ug/1 74-95-3 Dibromomethane ND 0.50 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 ug/1 10061-01-5 cis-1,3-Dichloropropene ND 0.50 ug/1 541-73-1 m-Dichlorobenzene ND 0.50 ug/1 95-50-1 o-Dichlorobenzene ND 600 0.50 ug/I 106-46-7 p-Dichlorobenzene ND 75 0.50 ug/I ND = Not detected J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 141) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® 6 of 22 Accutest Laboratories Report of Analysis Page 2 of Client Sample ID: 291C OAKLAND ROAD Lab Sample ID: M73763-1 Date Sampled: 05/23/08 Matrix: DW-Drinking Water Date Received: 05/27/08 Method: EPA 524.2 REV 4.1 Percent Solids: n/a Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT VOA List CAS No. Compound Result MCL RL Units Q 156-60-5 trans-1,2-Dichloroethylene ND 100 0.50 ug/1 15 6-59-2 cis-1,2-Dichloroethylene ND 70 0.50 ug/1 10061-02-6 trans-1,3-Dichloropropene ND 0.50 ug/1 100-41-4 Ethylbenzene ND 700 0.50 ug/1 87-68-3 Hexachlorobutadiene ND 0.50 ug/1 98-82-8 Isopropylbenzene ND 0.50 ug/I 99-87-6 p-Isopropyltoluene ND 0.50 ug/I 75-09-2 Methylene chloride ND 5.0 0.50 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/1 91-20-3 Naphthalene ND 0.50 ug/1 103-65-1 n-Propylbenzene ND 0.50 ug/1 100-42-5 Styrene ND 100 0.50 ug/1 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/I 71-55-6 1,1,1-Trichloroethane ND 200 0.50 ug/I 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ug/1 79-00-5 1,1,2-Trichloroethane ND 5.0 0.50 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/1 96-18-4 1,2,3-Trichioropropane ND 0.50 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 70 0.50 ug/I 95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/I 108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l 127-18-4 Tetrachloroethylene ND 5.0 0.50 ug/1 108-88-3 Toluene ND 1000 0.50 ug/I 79-01-6 Trichloroethylene ND 5.0 0.50 ug/I 75-69-4 Trichlorofluoromethane ND 0.50 ug/1 75-01-4 Vinyl chloride ND 2.0 0.50 ug/l m,p-Xylene ND 0.50 ug/1 95-47-6 o-Xylene ND 0.50 ug/1 1330-20-7 Xylenes (total) ND 10000 0.50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 2199-69-1 1,2-Dichlorobenzene-d4 90% 70-130% 460-00-4 4-Bromofluorobenzene 78% 70-130% ND = Not detected J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 141) B = Indicates analyte found in associated method blank E = Indicate&xalne_exceeds calibration range N = Indicates presumptive evidence of a compound Min 7 of 22 QA.tCt.,!TESV' M73763 :. Accutest Laboratories Report of Analysis Page 1 of 2 Client Sample ID: 291D OAKLAND ROAD Lab Sample ID: M73763-2 Date Sampled: 05/23/08 Matrix: DW-Drinking Water Date Received: 05/27/08 Method: EPA 524.2 REV 4.1 Percent Solids: n/a Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT File ID DF Analyzed By Prep Date Prep'Batch Analytical Batch Run#1 R5009.1) 1 06/06/08 AA n/a n/a MSR191 Run#2 Purge Volume Run#1 5.0 ml Run#2 VOA List CAS No. Compound Result MCL RL Units Q 71-43-2 Benzene ND 5.0 0.50 ug/1 108-86-1 Bromobenzene ND 0.50 ug/1 74-97-5 Bromochloromethane ND 0.50 ug/1 75-27-4 Bromodichloromethane ND 0.50 ug/1 75-25-2 Bromoform ND 0.50 ug/1 74-83-9 Bromomethane ND 0.50 ug/1 104-51-8 n-Butylbenzene ND 0.50 ug/1 135-98-8 sec-Butylbenzene ND 0.50 ug/1 98-06-6 tert-Butylbenzene ND 0.50 ug/1 108-90-7 Chlorobenzene ND 100 0.50 ug/1 75-00-3 Chloroethane ND 0.50 ug/1 67-66-3 Chloroform ND 0.50 ug/1 74-87-3 Chloromethane ND 0.50 ug/I 95-49-8 o-Chlorotoluene ND 0.50 ug/I 106-43-4 p-Chlorotoluene ND 0.50 ug/1 56-23-5 Carbon tetrachloride ND 5.0 0.50 ug/I 75-34-3 1,1-Dichloroethane ND 0.50 ug/1 75-35-4 1,1-Dichloroethylene ND 7.0 0.50 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 ug/l 96-12-8 1,2-Dibromo-37chloropropane ND 0.20 0.50 ug/1 106-93-4 1,2-Dibromoethane ND 0.050 0.50 ug/1 107-06-2 1,2-Dichloroethane ND 5.0 0.50 ug/I 78-87-5 1,2-Dichloropropane ND 5.0 0.50 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 ug/1 124-48-1 Dibromochloromethane ND 0.50 ug/I 74-95-3 Dibromomethane ND 0.50 ug/I 75-71-8 Dichlorodifluoromethane ND 0.50 ug/I 10061-01-5 cis-1,3-Dichloropropene ND 0.50 ug/1 541-73-1 m-Dichlorobenzene ND 0.50 ug/I 95-50-1 o-Dichlorobenzene ND 600 0.50 ug/1 106-46-7 p-Dichlorobenzene ND 75 0.50 ug/1 ND = Not detected J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 141) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound am 1012 8of22 QAX=UTEfi 1. M73763 ..'- --,... _, Accutest Laboratories Report of Analysis Page 2 of Client Sample ID: 291D OAKLAND ROAD Lab Sample ID: M73763-2 Date Sampled: 05/23/08 Matrix: DW-Drinking Water Date Received: 05/27/08 Method: EPA 524.2 REV 4.1 Percent Solids: n/a Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT VOA List CAS No. Compound Result MCL RL Units Q 156-60-5 trans-1,2-Dichloroethylene ND 100 0.50 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 70 0.50 ug/1 10061-02-6 trans-1,3-Dichloropropene ND 0.50 ug/I 100-41-4 Ethylbenzene ND 700 0.50 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 ug/I 98-82-8 Isopropylbenzene ND 0.50 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 ug/I 75-09-2 Methylene chloride ND 5.0 0.50 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/1 91-20-3 Naphthalene ND 0.50 ug/I 103-65-1 - n-Propylbenzene ND 0.50 ug/I 100-42-5 Styrene ND 100 0.50 ug/1 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/1 71-55-6 1,1,1-Trichloroethane ND 200 0.50 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ug/I 79-00-5 1,1,2-Trichloroethane ND 5.0 0.50 ug/I 87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/I 96-18-4 1,2,3-Trichloropropane ND 0.50 ug/1 120-82-1 1,2,4-Trichiorobenzene ND 70 0.50 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/1 127-18-4 Tetrachloroethylene ND 5.0 0.50 ug/1 108-88-3 Toluene ND 1000 0.50 ug/I 79-01-6 Trichloroethylene ND 5.0 0.50 ug/I 75-69-4 Trichlorofluoromethane ND 0.50 ug/I 75-01-4 Vinyl chloride ND 2.0 0.50 ug/I m,p-Xylene ND 0.50 ug/I 95-47-6 o-Xylene ND 0.50 ug/1 1330-20-7 Xylenes (total) ND 10000 0.50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 2199-69-1 1,2-Dichlorobenzene-d4 85% 70-130% 460-00-4 4-Bromofluorobenzene 88% 70-130% ND = Not detected J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 141) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound all 9of22 New England 'B EB • i v Section 4 P Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • RCP Form • Sample Tracking Chronicle ® 10 of 22 AGCU't'E M73763 "- - 0 - CHAIN OF CUSTODY 495 Tech Center West Bldg.I Marlboro,MA 01752 732-329.0200 FAX:732.329.3499/3480 Anutxn Jeex �� C9ent/Re rtin Information Fee-oityinfor,reto, Analytical information EXXONMOBIL CORPORATION•Regional Lab tory Pro ram Northeast Consultants Company Nam. Project Nama: Groundwater&Environmental Services Inc.-WNE Mobil-S.Windsor#Ot-QQA A""" a#" 4218 Hayden Station Road 249 Oakland Road city state zip City state Windsor Conncecticut 06095 South Windsor CT Prejaal ConMet: Enad iSuOnMOWIComace John Moss jai—&--pli.g.n Mary Caruso Samptanl's Nam.K - PxzonMoMl Contact Phon.N(609)596.4071�1 ors Phon.N Fox 1 Lotadon too Wasa soo 220-6119 860 688-9278 01-QQA AFEN PON 4509333735 url.N - Accutest Collection Preservation Sample# 'of a Field ID I Point of Collection Data Tore sa ea by Mainz lotu. _ 291C Oakland Road Y3 O?' FS' MA DL/ 3 291D Oakland Road 0 1 0 55' 1✓ '� 3 7umaround Tine Bu.lnesa da Date D.41—ble Em ECommantalRamaNw aid.10BusinessDays IPpro—tsyuwe! C--.tal'A- =F'ULLCLP 8 Day Rush ❑Comm.retal-B- 0 NYASP CRIogwy A Please follow RCP protocol for a GA groundwater classification - .Day RUSH n NJ Rsduced NYA8P category 6 3 Day EMERGENCY ❑NJ Fug state Forme ©2Day EMERGENCY Other F-1 EDO Formal 1 Day EMERGENCY Other Coin 1.1"A—Reaufta Ony --ff!!^^y1• Emer en T/A data available VIA Lablink Sample Cmtody must be doe merited below each time samples cha a Ion,Includingcou13 rier tlet o z ky z $ Y: usl nMry sp S • C .Y173763: Clain of Custody Page 1 of 2 ® 11 of 22 REST M73763 ,. ',, PROJECT COMMUNICATION FORM Client Name:• ExxonMobil Proiect Name.South Windsor ProiectNumber:01-QQA ProiectManaeer:John Moss Contact Info:(800)220-6119 x3540 Field Manager: Sample Matrix: ❑groundwater or surface water,❑soil,❑sediment,X drinking water,❑air,❑other Constituents of Concern:Please note any known or suspected contaminants in high concentrations or any non-standard analytes not contained in routine target lists(see notes). BTEX Reeulatory Criteria: ❑Residential Direct Exposure Criteria,❑ Industrial/Commercial Direct Exposure Criteria, ❑GA Pollutant Mobility Criteria,❑GB Pollutant Mobility Criteria,❑Other: ❑Groundwater Protection Criteria,❑ Surface Water Protection Criteria,❑Aquatic Life Criteria(specify applicable criteria below)X Other: EPA MCL's;CTDPH Action Levels Quality Control Requirements:Indicate if your project will have Project specific field quality control samples.Check all that apply.Also specify if special QAIQC site requirements exist:i.e.,Q,4PP ❑Matrix Spike,❑Matrix Spike Duplicate,X Trip Blank(s), ❑Other Field QC: ❑Project QAPP(send appropriate section(s)to lab) Report Deliverables Requirements:Indicate any reporting requirements other than routine lab data sheets such as electronic formats: ❑Excel Tables,❑GISKey,❑Envirodata,X GES Format,X RCP,❑Other: Expected Sampling Date(s):Indicate expected number ofsampling events or duration May,August,November Total Number of Samples and Expected Sample Load Per Day:(indicate number of each matrix ifapplicable) W Sample Pick UP: X office(s),❑site(address),❑other ^ Special Instructions: ❑ Report TICS 0'w w I a Notes: If requesting non-routine compounds that have no regulatory criteria,indicate required Meortin _ limit for each compound. ;; 0 Reasonable Confidence Protocol Laboratory Analysis QA/QC Certification Form p. N Laboratory Name: Accutest New England Client: Exxon Mobil Project Location: GESCT:01-QQA 249 Oakland Rd.,South Project Number: PO#4509333735 WBS#08 Windsor CT Sampling Date(s): 5/23/2008 Laboratory Sample ID(s): M73763-1,M73763-2 Methods: EPA 524.2 REV 4.1 For each analytical method referenced in this laboratory report package, were all specified QA/QC performance criteria followed,including the requirement to explain any 1 criteria falling outside of acceptable guidelines,as specified in the CTDEP method- Yes No specific Reasonable Confidence Protocol documents)? 1A Where all the method specified preservation and holding time requirments met? Yes No f 1 B VPH and EPH mehods only: Was the VPH or EPH method conducted without Yes No significant modifications (See section 11.3 of respective methods) NA f✓ Were all samples received by the laboratory in a condition consistent with 2 that described on the associated chain-of-custody document(s)? Yes 1-7 No 3 Were samples received at an appropriate temperature(<6°C)? Yes No Were all QA/QC performance criteria specified in the CTDEP Reasonable r 4 Confidence Protocol documents achieved? Yes No 5 a)Were reporting limits specified or referenced on the chain-of-custody? Yes I✓ No b)Were these reporting limits met? Yes f- No ° For each analytical method referenced in this laboratory report package, 6 were results reported for all constituents identified in the method-specific Yes No analyte lists presented in the Reasonable Confidence Protocol documents? 7 Are project-specific matrix spikes and laboratory duplicates included in this Yes No fL data set? Note:For all questions to which the response was"No" (with the exception of question#7),additional information must be provided in an attached narrative. If the answer to question#1,#1A or#1B is"No",the data package does not meet the requirements for"Reasonable Confidence". I,the undersigned,attest under pains and penalties of perjury that,to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report,such information is accurate and complete. Authorized Signature: Position: Lab Director Printed Name: Reza Tand Date: 6/1 412 0 0 8 Accutest New England Li 13of22 G M73763 Accutest Laboratories Internal Sample Tracking Chronicle w ExxonMobil Job No: M73763 GESCT:01-QQA 249 Oakland Rd., South Windsor CT Project No: PO#4509333735 WBS#08 Sample Number Method Analyzed By Prepped By Test Codes M73763'1 Collected: 23-MAY-09 09:55 By: KGA Received: 27-MAY-08 By: 291C OAKLAND ROAD M73763-1 EPA 524.2 REV 4.1 06-JUN-08 20:34 AA V524STD M73763-2 Collected: 23-MAY-08 1055 By KGA Received: 27-MAY-08 By: 291D OAKLAND ROAD M73763-2 EPA 524.2 REV 4.1 06-JUN-08 21:01 AA V524STD Page 1 of 1 ® 14 of 22 M73763 New England t Section 5 GC/MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ® 15 of 22 M73763 ,-;p Method Blank Summary Page 1 of 2 Job Number: M73763 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-MB R5000.1) 1 06/06/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 PP g M73763-1, M73763-2 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 0.50 ug/I 108-86-1 Bromobenzene ND 0.50 ug/l 74-97-5 Bromochloromethane ND 0.50 ug/l 75-27-4 Bromodichloromethane ND 0.50 ug/l 75-25-2 Bromoform ND 0.50 ug/l 74-83-9 Bromomethane ND 0.50 ug/1 104-51-8 n-Butylbenzene ND 0.50 ug/1 135-98-8 sec-Butylbenzene ND 0.50 ug/l 98-06-6 tert-Butylbenzene ND 0.50 ug/l 108-90-7 Chlorobenzene ND 0.50 ug/l 75-00-3 Chloroethane ND 0.50 ug/1 67-66-3 Chloroform ND 0.50 ug/l 74-87-3 Chloromethane ND 0.50 ug/1 95-49-8 o-Chlorotoluene ND 0.50 ug/1 106-43-4 p-Chlorotoluene ND 0.50 ug/l 56-23-5 Carbon tetrachloride ND 0.50 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 ug/I 75-35-4 1,1-Dichloroethylene ND 0.50 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 ug/l 124-48-1 Dibromochloromethane ND 0.50 ug/l 74-95-3 Dibromomethane ND 0.50 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 ug/l 541-73-1 m-Dichlorobenzene ND 0.50 ug/1 95-50-1 o-Dichlorobenzene ND 0.50 ug/l 106-46-7 p-Dichlorobenzene ND 0:50 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 ug/l 100-41-4 Ethylbenzene ND 0.50 ug/l ® 16 of 22 M73763 a.'. . - , Method Blank Summary Page 2 of Job Number: M73763 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-MB R5000.1) 1 06/06/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73763-1, M73763-2 CAS No. Compound Result RL Units Q 87-68-3 Hexachlorobutadiene ND 0.50 ug/l 98-82-8 Isopropylbenzene ND 0.50 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 ug/1 75-09-2 Methylene chloride ND 0.50 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/1 91-20-3 Naphthalene ND 0.50 ug/1 103-65-1 n-Propylbenzene ND 0.50 ug/I 100-42-5 Styrene ND 0.50 ug/1 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/I 71-55-6 1,1,1-Trichloroethane ND 0.50 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ug/1 79-00-5 1,1,2-Trichloroethane ND 0.50 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/1 127-18-4 Tetrachloroethylene ND 0.50 ug/I 108-88-3 Toluene ND 0.50 ug/I 79-01-6 Trichloroethylene ND 0.50 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 ug/1 75-01-4 Vinyl chloride ND 0.50 ug/1 m,p-Xylene ND 0.50 ug/1 95-47-6 o-Xylene ND 0.50 ug/1 1330-20-7 Xylenes (total) ND 0.50 ug/1 CAS No. Surrogate Recoveries Limits 2199-69-1 1,2-Dichlorobenzene-d4 96% 70-130% 460-00-4 4-Bromofluorobenzene 82% 70-130% CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q Total TIC, Volatile 0 ug/1 ® 17 of 22 A xZU'1€'FEST. M73763 Blank Spike Summary Page 1 of Job Number: M73763 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-BS R4998.1) 1 06/06/08 AA n/a n/a MSR191 cn The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73763-1, M73763-2 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits 71-43-2 Benzene 5 7.3 146* a 70-130 108-86-1 Bromobenzene 5 4.8 96 70-130 74-97-5 Bromochloromethane 5 5.7 114 70-130 75-27-4 Bromodichloromethane 5 5.8 116 70-130 75-25-2 Bromoform 5 4.3 86 70-130 74-83-9 Bromomethane 5 5.8 116 70-130 104-51-8 n-Butylbenzene 5 5.7 114 70-130 135-98-8 sec-Butylbenzene 5 5.5 110 70-130 98-06-6 tert-Butylbenzene 5 5.4 108 70-130 108-90-7 Chlorobenzene 5 5.6 112 70-130 75-00-3 Chloroethane 5 7.1 142* a 70-130 67-66-3 Chloroform 5 6.8 136*a 70-130 74-87-3 Chloromethane 5 7.4 148* a 70-130 95-49-8 o-Chlorotoluene 5 5.7 114 70-130 106-43-4 p-Chlorotoluene 5 5.7 114 70-130 56-23-5 Carbon tetrachloride 5 5.9 118 70-130 75-34-3 1,1-Dichloroethane 5 7.6 152* a 70-130 75-35-4 1,1-Dichloroethylene 5 6.3 126 70-130 563-58-6 1,1-Dichloropropene 5 6.9 138*a 70-130 96-12-8 1,2-Dibromo-3-chloropropane 5 5.3 106 70-130 106-93-4 1,2-Dibromoethane 5 5.2 104 70-130 107-06-2 1,2-Dichloroethane 5 6.6 132*a 70-130 78-87-5 1,2-Dichloropropane 5 6.9 138*a 70-130 142-28-9 1,3-Dichloropropane 5 6.2 124 70-130 594-20-7 2,2-Dichloropropane 5 7.0 140* a 70-130 124-48-1 Dibromochloromethane 5 5.0 100 70-130 74-95-3 Dibromomethane 5 6.4 128 70-130 75-71-8 Dichlorodifluoromethane 5 3.5 70 70-130 10061-01-5 cis-1,3-Dichloropropene 5 6.3 126 70-130 541-73-1 m-Dichlorobenzene 5 5.5 110 70-130 95-50-1 o-Dichlorobenzene 5 5.1 102 70-130 106-46-7 p-Dichlorobenzene 5 5.5 110 70-130 156-60-5 trans-1,2-Dichloroethylene 5 7.4 148* a 70-130 156-59-2 cis-1,2-Dichloroethylene 5 6.6 132* a 70-130 10061-02-6 trans-1,3-Dichloropropene 5 6.6 132* a 70-130 100-41-4 Ethylbenzene 5 6.0 120 70-130 ® 18 of 22 12 ACC IL T EST. ........ .......... .... M73763 :.,. . ...... Blank Spike Summary Page 2 of 2 Job Number: M73763 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR191-BS R4998.1) 1 06/06/08 AA n/a n/a MSR191 The QC reported here applies to the following samples: Method: EPA 524.2 REV 4.1 M73763-1, M73763-2 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits 87-68-3 Hexachlorobutadiene 5 4.1 82 70-130 98-82-8 Isopropylbenzene 5 5.6 112 70-130 99-87-6 p-Isopropyltoluene 5 5.0 100 70-130 75-09-2 Methylene chloride 5 6.4 128 70-130 1634-04-4 Methyl Tert Butyl Ether 5 6.1 122 70-130 91-20-3 Naphthalene 5 4.1 82 70-130 103-65-1 n-Propylbenzene 5 5.8 116 70-130 .100-42-5 Styrene 5 5.1 102 70-130 630-20-6 1,1,1,2-Tetrachloroethane 5 5.0 100 70-130 71-55-6 1,1,1-Trichloroethane 5 ' 6.2 124 70-130 79-34-5 1,1,2,2-Tetrachloroethane 5 5.6 112 70-130 79-00-5 1,1,2-Trichloroethane 5 5.3 106 70-130 87-61-6 1,2,3-Trichlorobenzene 5 4.3 86 70-130 96-18-4 1,2,3-Trichloropropane 5 5.1 102 70-130 120-82-1 1,2,4-Trichlorobenzene 5 4.4 88 70-130 95-63-6 1,2,4-Trimethylbenzene 5 5.2 104 70-130 108-67-8 1,3,5-Trimethylbenzene 5 5.5 110 70-130 127-18-4 Tetrachloroethylene 5 5.5 110 70-130 108-88-3 Toluene 5 6.5 130 70-130 79-01-6 Trichloroethylene 5 6.3 126 70-130 75-69-4 Trichlorofluoromethane 5 5.2 104 70-130 75-01-4 Vinyl chloride 5 6.5 130 70-130 m,p-Xylene 10 11.7 117 70-130 95-47-6 o-Xylene 5 5.7 114 70-130 1330-20-7 Xylenes (total) 15 17.4 116 70-130 CAS No. Surrogate Recoveries BSP Limits 2199-69-1 1,2-Dichlorobenzene-d4 80% 70-130% 460-00-4 4-Bromofluorobenzene 96% 70-130% (a) Outside control limits. Associated samples are non-detect for this compound. 19 of 22 M ACCtJTEST< M73763 -, _ .... ., Duplicate Summary Page 1 of Job Number: M73763 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73920-11)UP R5018.D 1 06/07/08 AA n/a n/a MSR191 M73920-1 R5017.13 1 06/07/08 AA n/a n/a MSR191 i� The C reported here applies to the following samples: Method: EPA 524.2 REV 4.1 Q P PP g P M73763-1, M73763-2 M73920-1 DUP CAS No. Compound ug/l Q ug/l Q RPD Limits 71-43-2 Benzene ND ND nc 30 108-86-1 Bromobenzene ND ND nc 30 74-97-5 Bromochloromethane ND ND nc 30 75-27-4 Bromodichloromethane ND ND nc 30 75-25-2 Bromoform ND ND nc 30 74-83-9 Bromomethane ND ND nc 30 104-51-8 n-Butylbenzene ND ND nc 30 135-98-8 sec-Butylbenzene ND ND nc 30 98-06-6 tert-Butylbenzene ND ND nc 30 108-90-7 Chlorobenzene ND ND nc 30 75-00-3 Chloroethane ND ND nc 30 67-66-3 Chloroform ND ND nc 30 74-87-3 Chloromethane ND ND nc 30 95-49-8 o-Chlorotoluene ND ND nc 30 106-43-4 p-Chlorotoluene ND ND nc 30 56-23-5 Carbon tetrachloride ND ND nc 30 75-34-3 1,1-Dichloroethane ND ND nc 30 75-35-4 1,1-Dichloroethylene ND ND nc 30 563-58-6 1,1-Dichloropropene ND ND nc 30 96-12-8 1,2-Dibromo-3-chloropropane ND ND nc 30 106-93-4 1,2-Dibromoethane ND ND nc 30 107-06-2 1,2-Dichloroethane ND ND nc 30 78-87-5 1,2-Dichloropropane ND ND nc 30 142-28-9 1,3-Dichloropropane ND ND nc 30 594-20-7 2,2-Dichloropropane ND ND nc 30 124-48-1 Dibromochloromethane ND ND nc 30 74-95-3 Dibromomethane ND ND nc 30 75-71-8 Dichlorodifluoromethane ND ND nc 30 10061-01-5 cis-1,3-Dichloropropene ND ND nc 30 541-73-1 m-Dichlorobenzene ND ND nc 30 95-50-1 o-Dichlorobenzene ND ND nc 30 106-46-7 p-Dichlorobenzene ND ND nc 30 156-60-5 trans-1,2-Dichloroethylene ND ND nc 30 156-59-2 cis-1,2-Dichloroethylene ND ND nc 30 10061-02-6 trans-1,3-Dichloropropene ND ND nc 30 100-41-4 Ethylbenzene ND ND nc 30 20 of 22 12ACC:C U 1"EST M73763 :-' - Duplicate Summary Page 2 of 2 Job Number: M73763 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73920-1DUP R5018.1) 1 06/07/08 AA n/a n/a MSR191 M73920-1 R5017.1) 1 06/07/08 AA n/a n/a MSR191 en The C reported here applies to the following samples: Method: EPA 524.2 REV 4.1 Q P PP g P M73763-1, M73763-2 M73920-1 DUP CAS No. Compound ug/l Q ug/l Q RPD Limits 87-68-3 Hexachlorobutadiene ND ND nc 30 98-82-8 Isopropylbenzene ND ND nc 30 99-87-6 p-Isopropyltoluene ND ND nc 30 75-09-2 Methylene chloride ND ND nc 30 1634-04-4 Methyl Tert Butyl Ether ND ND nc 30 91-20-3 Naphthalene ND ND nc 30 103-65-1 n-Propylbenzene ND ND nc 30 100-42-5 Styrene ND ND nc 30 630-20-6 1,1,1,2-Tetrachloroethane ND ND nc 30 71-55-6 1,1,1-Trichloroethane ND ND nc 30 79-34-5 1,1,2,2-Tetrachloroethane ND ND nc 30 79-00-5 1,1,2-Trichloroethane ND ND nc 30 87-61-6 1,2,3-Trichlorobenzene ND ND nc 30 96-18-4 1,2,3-Trichloropropane ND ND nc 30 120-82-1 1,2,4-Trichlorobenzene ND ND nc 30 95-63-6 1,2,4-Trimethylbenzene ND ND nc 30 108-67-8 1,3,5-Trimethylbenzene ND ND nc 30 127-18-4 Tetrachloroethylene 0.56 0.65 15 30 108-88-3 Toluene ND ND nc 30 79-01-6 Trichloroethylene ND ND nc 30 75-69-4 Trichlorofluoromethane ND ND nc 30 75-01-4 Vinyl chloride ND ND nc 30 m,p-Xylene ND ND nc 30 95-47-6 o-Xylene ND ND nc 30 1330-20-7 Xylenes (total) ND ND nc 30 CAS No. Surrogate Recoveries DUP M73920-1 Limits 2199-69-1 1,2-Dichlorobenzene-d4 97% 104% 70-130% 460-00-4 4-Bromofluorobenzene 98% 108% 70-130% ® 21 of 22 ® UTES T. M73763 -- r Volatile Surrogate Recovery Summary Page I of I Job Number: M73763 Account: MOBILSS ExxonMobil Project: GESCT:01-QQA 249 Oakland Rd., South Windsor CT Method: EPA 524.2 REV 4.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 S2 M73763-1 R5008.1) 90.0 78.0 M73763-2 R5009.D 85.0 88.0 M73920-1DUP R5018.1) 97.0 98.0 MSR191-BS R4998.1) 80.0 96.0 MSR191-MB R5000.1) 96.0 82.0 Surrogate Recovery Compounds Limits S1 = 1,2-Dichlorobenzene-d4 70-130% S2 = 4-Bromofluorobenzene 70-130% ® 22 of 22 M73763